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Tef-Flex PTFE / EPDM Unitized Sanitary Tri-Clamp Gasket
Tef-Flex Sanitary Tri-Clamp Gasket Tef-Flex: A Tef-Flex sanitary gasket’s contact surface is a layer of PTFE grafted to an EPDM rubber inner core. This totally bonded construction provides an exceptionally pure and incredibly flexible seal. By grafting the elastomer with a layer of PTFE, Tef-Flex will behave like an elastomer but will prevent product contamination, service interruptions and clean-up costs associated with traditional elastomer seals. The PTFE grafted elastomer in a Tef-Flex sanitary gasket will maintain I.D. without re-torquing or leaking. Key Features: Excellent resistance to almost all chemicals Excellent Temperature Range Excellent Cleanability due to PTFE (Teflon) Excellent Flexibility Sizes Available: 0.5" 0.75" 1" 1.5" 2" 2.5" 3" 4" 6" 8" 10" 12" Chemical Compatibility: Butane A - Excellent Propane (liquified) A - Excellent Alcohols: Amyl A - Excellent Benzyl A - Excellent Butyl A - Excellent Diacetone A - Excellent Ethyl A - Excellent Hexyl A - Excellent Isobutyl A - Excellent Isopropyl A - Excellent Methyl A - Excellent Octyl A - Excellent Propyl A - Excellent Disclaimer: BVV Recommends no more than a -40F Operating Temperature and is not responsible for the user running their system with incompatible chemicals.
$18.00 - $38.00
Thermocouple Plus | 531 Equivalent Vacuum Sensor - .001 to 6 Torr Accuracy
531 Thermocouple Plus Use for applications that require a better accuracy than others gauges can provide. Excellent for dirty applications where a replaceable sensor is desirable. Design for years of use Applications for Freeze-drying, low pressure distillations, fore line monitoring, and transformer dry out. Weight 1 lbs Shipping Dimensions 6 x 4 x 4 in Isolated no Vacuum Reference Absolute Display No Units Torr, mbar, bar, kPa, inches of Hg, mm Hg, millitorr, microns, inches of water, PSI, Pa Total Range .001-760 Range with Accuracy .001 – 6.0 Torr Sensor Type Thermocouple
$110.00
Glass Vac™ 8" Diameter LID
Glass Vac 8" Diameter LID Our patented gasket #9475627 Disclaimer: This item Includes Lid and Gasket Only This is a Replacement Lid for the following Vacuum Chambers: Glass Vac 1 Gallon Tall Stainless Steel Vacuum Chamber Glass Vac 1.5 Gallon Tall Stainless Steel Vacuum Chamber
$54.00
XL Refinement Filter
XL Refinement Filter The BVV™ XL Refinement Filter is a stainless steel filtration system that provides industrial scale, high flow filtering, with greatly improved functionality compared to a traditional Buchner filter. Utilizing a collection base for vacuum assistance and storage of material, the XL Refinement Filter allows for industrial filtration with a longer lifespan and ease of use. Key Features: Stainless steel design for greater thermal conductivity and improved lifespan Easy to clean and disassemble with Tri-Clamp stainless steel parts Mobile Rack mounted with wide mouth design **Rack #2 option has extra space to mount additional filters or heat exchangers Secondary collection vessel for vacuum and storage of material Liquid dip tube for direct injection into rotary evaporator after filling Key Specifications: Large 12" Diameter x 24" Long Fully Jacketed Column Massive 20LB (23.5 Gallons / 89 Liters) Fully Jacketed Collection Base 5 micron Sintered Stainless Steel Filter Disc 100 Pack of Qualitative Cellulose Filter Paper Dedicated 3/8" Vacuum Valve Dedicated 3/8" Dip Tube Valve Silicone gaskets with high alcohol resistance 3/8" Stainless steel hose barb connections Polycarbonate sights for easy viewing Jacketed Filter for temperature stability Quick Start Operation Instructions: Before beginning filtration, pre-chill refinement filter for best thermal conductivity Secure ashless filter paper with compression ring connect tubing from refinement filter to a vacuum pump Attach vacuum system to the dedicated vacuum valve Begin to pour solution into filter Close dedicated dip tube valve and start vacuum Once solution has been completely filtered, stop vacuum system and disconnect from dedicated vacuum valve Connect dedicated dip tube valve to injection valve on rotovap Begin rotovap procedure Open dedicated dip tube valve and begin injecting filtered solution into rotovap
$3,050.00 - $4,860.00
5L Main Condenser
Main condenser for 5L Best Value Rotary Evaporator. *Photo does NOT represent the actual part. Photo Coming soon, inquire for photos if you need to order this item please. *Notice to customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. **Glassware Safety Disclaimer: BVV™ is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.**
$320.00
50L Neocision ETL Lab Certified Rotary Evaporator
50L Neocision ETL Lab Certified Rotary Evaporator The 50L Neocision ETL Lab Certified Rotary Evaporator is a full-scale system meant to fulfill the needs of large volume production and meet the requirements of a certified laboratory with its ETL certification standards. Featuring an electric lift bath and all PTFE valves for extreme chemical resistance, the 50L Neocision gives users the ability to recover large amounts of solvent in a smaller footprint with highly improved functionality. All Neocision rotovaps feature high-efficiency valves and drain ports making it easy to directly inject solution continuously without the need to stop the system or release vacuum to drain. The temperature and rotation speed are easily controlled from a single digital interface. Our rotovaps are a fraction of the price of more costly systems with the same functionality and evaporation efficiency. To keep your bath heating properly, this unit should only be used with RO or DI water. 10-50L NEO and ECO Rotary Evaporator Diagram Features: ETL Certified for Lab use. Digital temperature and speed control with simple user interface Electric Bath Lift Teflon Coated Bath for corrosion resistance High-efficiency drain port and injection valves Smaller footprint for improved workspace allocation Mobility with locking casters Shorter vapor path for faster evaporation and condensation Direct injection capability for continuous feeding of solution Continuous draining capability without the need to release vacuum or stop the system 1-year warranty on all mechanical parts. Does not include glassware/moving parts Specifications: Model 50L NEOCISION Rotary Evaporator Optimum Ambient Temperature 5~25C / 41~105.8F Glass Material GG-17 High Borosilicate Power (V/Hz) 220-240V 60Hz Single Phase Speed Regulation Digital Step-less Regulation Rotation Speed 0-120 RPM Set Temperature 0-99C / 0-210F Temperature Control Digital Temperature Control Maximum Vacuum Pressure -29.8 inHg Evaporating Flask Capacity 50L (20000ml) Receiving Flask Capacity 20L (10000ml) Condenser Style Main + Auxiliary Vertical Double Helix Evaporation Capacity Alcohol >/= 12 L/H Heater Max Current Draw (Amps) 25 Water Bath Material 304 Stainless Steel Water Bath Size 17.7 x 9.8 in. Lifting Function Electric Lifting Stroke 190mm / 7.5 in. Total Power Consumption (kW) 4.1 kW Dimensions 49 x 24 x 83 in. Weight 155 lbs Vacuum Connection 10mm / 3/8 in. Barb Condenser Connection 10mm / 3/8 in. Barb Warranty 1 Year Excluding: Moving Parts Glassware Certifications ETL Rotovap Quick Start Guide This guide gives basic quick start instructions for rotovaps. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs. Clean and assemble unit. Make sure all pieces are cleaned and sterilized using an alcohol solution. Connect chiller to condenser and set to 0C (32F). Always fill a rotovap condenser from the top down (chiller output to top of condenser, chiller input to bottom of condenser). Connect vacuum pump to cold trap and connect cold trap to vacuum port on rotovap. Turn on heat bath and set to 40C (113F). Once heat bath, chiller and cold trap have reached desired temperatures, turn on rotovap motor and set speed to approximately 100 RPM (does not have to be precise). Keep in mind, higher RPM’s will increase evaporation power but also increase heat load. Start vacuum pump and allow vacuum to pull down for a few minutes before injection. Once vacuum has been pulled to a sufficient level (does not have to be precise but should be below 100 Torr), using the injection valve, very slowly inject approximately 500 mL of solution into evaporating flask and then close the valve. Allow this small amount to begin evaporating. You may see the chiller begin to rise in temperature, this is called “priming” the rotovap. Once the temperature stops rising or all liquid is almost completely evaporated, open the injection valve again very slowly so that a small amount of liquid begins to enter the evaporating flask. Do not close injection valve this time but continue to allow solution to enter the evaporating flask. At this point you must try to match the input speed to the output speed. What this means is that you should be injecting the same amount of liquid into the rotovap that is equal to the amount of liquid dripping from the condenser into the receiving flask. You will know that the input speed and output speed are matched because the chiller will remain at a stable temperature. If the chiller begins to rise, then you are injecting too much liquid. Dial back the valve until the chiller stabilizes. Once everything is stabilized, you may walk away from the rotovap if necessary. Check every so often to make sure temperatures remain stable and evaporation continues efficiently. ***Note: All units are inspected for broken glass or parts before unit is shipped. If unit arrives damaged or glass is broken (this does not include minor imperfections or scuffs in glassware), Customer MUST contact BVV™ within 3 days of delivery to file a claim and receive a replacement part. If customer DOES NOT contact BVV™ within 3 days of delivery responsibility for replacement parts falls on the customer and they must pay for replacement pieces.*** ***Note: This item will ship by freight only.*** ***Glassware Safety Disclaimer: BVV™ is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.***.
$7,250.00
6" Pre-Built BIFLOW Hemispherical Lid with BVV 316SS Full Bore Valves
6" Pre-Built BIFLOW Hemispherical Lid with BVV 316SS Full Bore Valves (This Lid is fully assembled and Nitrogen Tested for Leaks at Best Value Vacs) This 6" Best Value Vacs Hemispherical lid is fully assembled and nitrogen tested for leaks at our warehouse. This lid comes with 3 BVV 316SS Full Bore Valves with (2)1/4" and (1)3/8" 37° JIC Flares, compound gauge and the 4th hole is plugged to allow for future expansion. These lids are made out of 304 stainless steel and have 3 1.5" Tri-Clamp ports with the middle port having an extended tube to control solvent flow. Key Features: Pre-built and Nitrogen Tested for Leaks BVV 316SS Full Bore Valves with 1/4" and 3/8" 37° JIC Flares -40F to 450F 304 High Polish Stainless Steel Compound Gauge (-30)-0-(150PSI) Specifications Lid Material 304 Stainless Steel Valve Material 316SS Full Encapsulated PTFE Core - 1/4 Turn Flare Size (2)1/4" and (1) 3/8" 37° JIC Tri-Clamp Size(s) (3) 1.5" Ports x 6" Tri-Clamp Nitrogen Tested Yes
$310.00
1" FNPT X 1.5" Tri-Clamp Top Cap
1" FNPT X 1.5" Tri-Clamp Top Cap These tri-clamp end caps: Have a 1" Female NPT connection Are made of 304 stainless steel
$16.00
HTP The Monster Press - 8 Ton
HTP The Monster Press - 8 Ton If you have a large amount of plant material and are looking for a quality press then the Monster Press is for you! These high-quality presses are built from Aircraft Aluminum and stainless steel designed to be used in conjunction with a unique heating process.The Monster Press exerts 8 Tons of pressure to output a maximum shape of 5”x 7” x 3” thick.High Tech Pipes make quality presses that are manufactured in the U.S.A. using American materials and labor. Each Press is assembled and individually inspected before shipping. Our Presses are designed to be heated to the ideal temperature which is an important aspect of the Pressing process. We design and build our products to stand the test of time and to become a permanent piece of equipment for the end user. We use aircraft aluminum which maintains heat as opposed to other Presses on the market which use steel that either quickly loses heat or heats up too fast thus destroying the material that is being pressed. Each Press comes with full step by step instructions and a video is available as well.
$934.95$895.00
Welch DryFast Collegiate Diaphragm Pump 2014
DryFast Collegiate Diaphragm Pump 2014 ***Note: This item has a possible 1-2 week lead time depending on stock availability*** Product Details Chemical Resistant Oil-Free Tuneable Vacuum Welch DryFastTM PTFE Diaphragm Vacuum Pumps enable precise vacuum control for organic evaporations with exclusive Advanced Vapor Management (AVM). Oil-Free, portable, chemical resistant, 1 head diaphragm design simplifies maintenance. Choose from seven dry PTFE vacuum pump models with flows up to 70 L / min and adjustable vacuum down to 2 Torr. Economical DryFastTM vacuum pumps are perfect for tough lab applications. Model Number 2014 Applications Vacuum Filtration, SPE, Rotary Evaporations (volatile solvents <80oC B.P., volume <2 liters), pumping harsh vapors & gases, general laboratory vacuum Type Laboratory Vacuum Pump Free Air Displacement cfm (l/min.) @60Hz 1.2(35) Free Air Displacement m3/hr (l/min.) @50Hz 1.75(29) Ultimate Pressure 40(53) Maximum Vacuum 28.3 Motor Horsepower (watts) 1/5(150) Adjustable Vac. / Gas Ballast Yes Tubing Needed 1/4(7) Intake Thread NPT M14(1/8) Overall Dimensions LxWxH in. (cm) 12x7.0x8.3 (30.5x 17.8x21.1) Ship Weight 19(8.6) Shipping Carton Dimensions LxWxH in. (cm) 21x14x15 (52x35x37) Adjustable Vacuum Knob
$1,602.00
Edwards E2M28 21 CFM Dual-Stage High Capacity Vacuum Pump
Edwards E2M28 21 CFM Dual-Stage High Capacity Vacuum Pump ***Note: This item Will Ship by Freight only*** The EM range of oil‑sealed rotary pumps – renowned for their high ultimate vacuum, rapid pumping speed, quiet operation and ability to handle vapor – have become the industry standard for laboratory and light industrial applications. The pump is a freestanding unit with the drive provided through a flexible coupling by either a single‑phase or three‑phase (four pole) air cooled motor.Each EM pump is supplied with 2 x 1 liter of Ultragrade 19 oil, O ring and centering ring, two Allen keys and spares seal for oil drain and filter plugs. For PFPE prepared FX pumps Fomblin® to be ordered separately. Technology The motor is totally enclosed and is cooled by the motor-cooling fan which directs air along the motor fins. The motors are fitted with a thermal overload device. When the motor is too hot, the thermal overload device switches off the pump. The thermal overload device has an automatic reset; when the motor cools down, the device resets and the motor will restart.An oil pressure system lubricates the pump shaft bearing surfaces and rotor sealing faces. The pump has an oil distribution valve which prevents discharge of oil to the pump interior after the pump stops. The pumping chambers are air-tight, so this arrangement also prevents suckback unless the gas ballast valve is open.You can inspect the level and condition of oil in the oil box reservoir through the oil sight-glass. An oil filler-plug is fitted to the top of the oil box. The pump has two oil drain-plugs to allow either gravity oil drain or pressure oil drain. Features and Benefits The pump is designed for reliable, long‑term operation. Thermal overload device prevents overheating (single phase only). The drive is provided through a flexible coupling by a single‑phase or three‑phase (four pole) motor. The motors are totally enclosed and are cooled by the motor cooling fan. Full height O ring sealed oil sight glass for easy checking of oil level and condition. Large sight glass and operating oil range. IE3 energy efficient 3 phase motor used with E2M28. Edwards E2M28 21 CFM Dual-Stage High Capacity Vacuum Pump. The EM range of oil-sealed rotary pumps - renowned for its high ultimate vacuum, rapid pumping speed, quiet operation and ability to handle vapour - has become the industry standard laboratory and light industrial applications. The E2M28 pump is a two-stage, direct drive, sliding vane pump. The pump is oil sealed and designed for reliable, long-term operation in both laboratory and industrial environments. The pump is a freestanding unit with the drive provided through a flexible coupling by either a single-phase or three-phase (four-pole) motor. Specifications Displacement 50Hz 32.2 m3h-1 / 19 ft3min-1 60Hz 38.9 m3h-1 / 22.3 ft3min-1 Speed (Pneurop 6602) 50Hz 27.5 m3h-1 / 16.2 ft3min-1 60Hz 33.0 m3h-1 / 19.5 ft3min-1 Ultimate vacuum (total pressure) without gas ballast 1 x 10-3 mbar / 7.5 x 10-4 Torr with gas ballast 1.5 x 10-2 mbar / 1.1 x 10-2 Torr with Fomblin® 1 x 10-2 mbar / 7.5 x 10-3 Torr Inlet connection NW25 flange Outlet connection** Nozzle 15 mm external Ø removable from 3/4 in BSP tapped hole Max allowed pressure at outlet 0.5 bar gauge / 7 psig Max water vapour pumping rate – GB II 220 gh-1 Max inlet pressure for water vapour 30 mbar / 23 Torr Max water vapour pumping rate 0.7 kg h-1 Operating temperature range 13 – 40 °C Nominal rotation speed 1440 / 1720 rpm Motor power 50 Hz 0.75 kW Motor power 60 Hz 0.90 kW Power Connector 1-ph* IEC EN60320 C19 Weight 44 kg / 97 lbs Noise 57 dB(A) @ 50 Hz Oil capacity - max 1.5 litre Oil capacity - min 1.2 litre Recommended oil (supplied) Ultragrade 19 * Pumps listed with IEC connector only ** The FX are supplied with NW25 outlet connection ** POWER CORD NOT INCLUDED. RECOMMEND FOR CUSTOMER TO WIRE PUMP TO OUTLET WITH EXACT LENGTH. DO NOT USE EXTENSIONS** **RECOMMEND FOR CUSTOMER TO HAVE ELECTRICIAN WIRE PUMP TO OUTLET WITH EXACT LENGTH** Pump Warranty Information Customers using solvents such as stabilization resins (MinWax™, Gator Venom™ etc.), alcohol and other polar solvents must use the vacuum pumps in conjunction with a cold trap for evacuations in excess of 5 minutes. (Excludes Cactus Juice™) If the consumer is using the pump for prolonged periods of time exceeding 5 minutes we require that a cold trap is used or the pump warranty is void. These stabilization resins have the ability to break down the internal components of the pump that are plastic resulting in a seized motor voiding all warranties. When evacuation exceeds 5 minutes these solvents begin to vaporize and then re-condense in the vacuum pump reservoir. Once enough solvent re-condenses in the pump displacing the oil the plastic internal components may begin to warp, melt or seize. The use of a cold trap will condense the vapors prior to making their way to the vacuum pump preventing pump damage due to excessive use. Furthermore, Minwax Wood Hardener™ is not to be used with any vacuum pumps, EVER. (A seized motor will result within the first use.) To prevent these issues from happening to your process, change the Oil after each vacuum pump use, Even if the use time is only 5min.
$8,653.00 - $10,402.00
Harvest Right Home Pro Freeze Dryer
Harvest Right™ Home Pro Freeze Dryer Fresh Food Per Batch18-27 lbs. Fresh Food Per YearUp to 5000 lbs. Tray Space1107 sq. inches Features Tray space: 1,107 square inches Freeze dry 18 to 27 lbs. fresh food per batch Freeze dry up to 5,000 lbs. fresh food per year (This would require a person to use the freeze dryer 4 times a week for 50 weeks a year) Dimensions Freeze dryer exterior dimensions: 21.3″ W x 27.5″ D x 31.3″ H Dimensions (without door or vacuum fitting): 20.25" W x 23.75" D x 31.3" H Perfect for counter top, cart, or table. Tray dimensions: 9″ W x 20.5″ x 0.75″ H Weight of freeze dryer: 143 lbs. 10 CFM industrial vacuum pump included/no extra cost ($895 value) Power 110 volt (NEMA 5-20) outlet. A dedicated 20 amp circuit is required Shipping Info The large freeze dryer ships in one package with a total weight of 243 lbs. Item will only be delivered to physical addresses. One freeze dryer package: 29″ W x 38″ D x 48″ H. Maintenance Replace vacuum pump oil every 20 to 30 batches (takes about two minutes) Clean freeze dryer as needed. Warranty Three year limited warranty. What's Included -Large Pro Freeze Dryer -Premier Industrial Vacuum Pump -Vacuum Pump Oil -Oil Filter -Stainless Steel Trays (set of 6) -Guide to Freeze Drying -Mylar Bags (50 ct) -Oxygen Absorbers (50 ct) -Impulse Sealer
$3,595.00 - $5,290.00
12" x (3) 2" x (2) 1/4 FNPT Endcap with Diptube
12" x (3) 2" x (2) 1/4 FNPT Endcap with diptube This End Cap come with a 11-5/16" long diptube, Two 1/4"-18 FNPT Threaded connection and Three 2" Tri-Clamp/ Tri Clover ferrule welded to the end cap with a sanitary weld with a 0.5" Tube Extension on center ferrule Below the Lid. They allow the user to adapt and connect a threaded connection to the 1/4" port on a Tri-Clamp lid and the 2" Tri-Clamp Connection. These 5 connections are welded on a 12" Tri-Clamp End Cap. Specification Material: 304 Stainless Steel Connection Type: 2" Tri-Clamp - 0.5" Tube Extension on center ferrule Below Lid 11-5/16" Diptube 12" Tri-Clamp 1/4" - 18 FNPT Standard: 3A
$245.00
6" x 4" x 3" x (2) 1/4" FNPT Tri-Clamp Skylight
Specifications: 304 Grade Stainless Steel Reducer 'Skylight' w/ High Polish interior 6" Triclamp x 4" Triclamp x 3" Triclamp (Can be used as viewport to see inside) x (2)1/4" FNPT 7" Tall
$175.00
24/29 Valve
24/29 Valve For 10L-50L Best Value Rotary Evaporators. *Notice to customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. **Glassware Safety Disclaimer: BVV™ is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.**
$35.00
20L Neocision Dual Short Path Distillation Turnkey System
20L Neocision Dual Short Path Distillation Turnkey System This unit carries a 2 day lead time. (Note: This kit does NOT include the stainless steel table.) The 20L Neocision Distillation Turnkey Setup features our Dual USA made P10V6 Distillation Heads. Every component in this distillation kit is made for precision, throughput, and repeatable results. You will also receive Dual Dewar Style Ribbed Glass Cold Traps to keep all volatiles and solvents out of your vacuum system. This Turnkey Setup gives you everything needed to perform distillation at the highest level. The 20L Neo Kit Includes: 20L Neocision Kit with glassware, labware, and Dual P10V6 Distillation Heads. BVV 15 Liter Advanced Digital Heated Circulator Choice of Vacuum Pump KF-25 Bellow Y Manifold Dual Ribbed Dewar Style Glass Cold Trap Non-Mercury Glass Thermometers 20L Digital Heating and Stirring Mantle Distillation Quick Start Guide This guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs, Before beginning distillation, ensure the following steps have been taken: Vacuum Pump is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed. All glass components are in good working order and ready to be assembled A winterization and degassing procedure has been done to prepare oil for distillation The unit's max internal temperature cannot exceed 380C. The recommended max set temperature should not exceed 250C Once all three of these steps have been completed, you are ready to begin distilling. Begin by placing stir bar in the boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer. Assemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware Attach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation. Connect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system. Connect receiving cow to cold trap. Connect cold trap to manifold. Connect vacuum gauge to manifold. At this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process. Turn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability. Start stir slower and increase speed with temperature. Once you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C. You will see your first fraction somewhere between 180C and 190C or slightly before. This is the “heads” fraction. You will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to “self-clean” the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your “main body” fraction. You will see temps between 190-220C during this fraction. Continue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed. The final “tails” fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The “tails” fraction has an obvious color change and will be darker than the “main body” fraction. You will see temps between 200-250C during this fraction. As fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well. Once process is complete, stop heat, stop stir, and stop vacuum. Let atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation. ***Note: This entire setup will ship via motor freight.*** *Notice to Customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. BVV™ is not responsible for the failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail, which can cause bodily harm or damage to the surrounding area.
$13,000.00 - $17,000.00
P2V4 Neocision Distillation Head - USA Made
P2V4 Neocision Distillation Head P2V4 Short Path Distillation Head includes 4 sets of Vigreux with 24/40 Joints and GL-14 Barb Connections. Key Features: MADE IN THE USA Designed for 1 & 2 Liter Flasks Set of 4 Vigreux to allow for better seperation of fractions without packing material Larger vacuum jacket allows for less heat loss during distillations Larger vapor path to allow for gas/vapor phase flow Increased internal diameter for faster, more efficient fractioning as well as packing and unpacking of media Increased condenser length and diameter for more efficient condensation of vapor with zero clogging *Notice to customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. **Glassware Safety Disclaimer: BVV™ is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.**
$800.00
Dry Utility Vacuum/Pressure Gauge - Center Back Mount
Dry Utility Vacuum/Pressure Gauge - Center Back Mount 1/8" MNPT brass Connection
$12.00$7.00
Economy Recirculating Heater Kit
Economy Recirculating Heater Kit The Economy Recirculating Heater Kit is designed to provide efficient heating and circulation at an affordable price. The kit includes a submersible water pump for fluid circulation, an LX or MX immersion heater, and all tubing and hose clamps needed to pair with your system. The tubing is 1/2" ID x 5/8" OD and the pump fitting is 1/2". The pump will circulate up to 594 GPH. Economy Recirculating Heater Kit Includes: Polyscience LX or MX Immersion Circulator EcoPlus Eco 633 Fixed Flow Submersible/Inline Pump 594 GPH 5 Gallon Aluminum Pot 10 Feet of 1/2" Silicone Tubing 10 Pack of Adjustable Stainless Steel Tubing Clamps
$1,700.00
5L BVV™ Rotary Evaporator Glass Axis
Glass axis for 5L BVV™ Rotary Evaporator *Notice to customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. **Glassware Safety Disclaimer: BVV™ is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.**
$50.00
Welch 6.1 cfm Full Chemical-Resistant 8-Head Diaphragm Pump
Welch 6.1 cfm Full Chemical-Resistant 8-Head Diaphragm Pump The Welch 6.1CFM Full Chemical-Resistant 8-Head Diaphragm Pump is the ideal choice for 50L Rotary Evaporators and large oven systems. This high capacity, full chemical resistant pump gives users the ability to vac down large capacity spaces quickly, efficiently, and cleanly without worrying about contamination of pump oil. The inner diaphragm is lined with PTFE making it highly chemical resistant and long lasting. It is one of the quietest and cleanest running vacuum pumps on the market. Key Features: Fully Chemical-Resistant Oil-less diaphragm style vacuum pump High capacity vacuum capability Specifications: Electrical Requirements: 110v 60Hz single phase Pumping Rate: 6.1cfm / 174L/min Gasket Material: All-PTFE Ultimate Vacuum level: 6 torr / 8 mbar Maximum Vacuum: 29.9 inHg Inlet / Outlet: KF16 Flange Adjustable vac. / gas ballast: No Unit dimensions (LxWxH in): 21x10x12 in Shipping dimensions (LxWxH in): 28x15x20 in Shipping weight (lbs): 90 Technical Data Free Air Displacement @ 60 Hz, cfm (L/min) 6.1 (173) Ultimate Pressure, torr 6 Motor Power, HP (kW) at 60 Hz Motor Power, HP (kW) at 60 Hz Inlet (Exhaust) Connection Thread NPT NW16 - 1/4" NPT Tubing Needed, I.D. in. (mm) Hose Connector Available Weight, lbs (kg) 72.3 (32.8) Dimensions, LxWxH, in (mm) 21x11x12 (530x280x310) 115V Order Number 2064B-01 ***Note: Purchase of this pump is subject to End User Verification. A certification form must be filled out before completion of purchase.***
$5,864.00
5L Short Path Distillation Kit with P5 Distillation Head
5L Short Path Distillation Kit with P5 Distillation Head This unit carries a 2 day lead time. The 5L Distillation Kit includes everything needed to perform distillation excluding the vacuum pump and chiller. This kit features our USA made P5 Distillation Head, as well as USA, made glass. This Kit is designed for high volume production with the highest quality components for precise, repeatable results time and again. This Kit Does NOT include a vacuum pump or chiller. Please see the below recommendations for both as well as recommended add-ons. Recommended Vacuum Pumps: Pro Series 11.3CFM Corrosion Resistant Two Stage Vacuum Pump (recommended option) Just Better 6 CFM 2 Stage Deep Vacuum Pump (economy option) Recommended Chillers: Polyscience 7 Liter MX Heated Circulator (economy option) Polyscience 7 Liter Refrigerated Circulator (premium option with chilling capability) Recommended Add-Ons: Glass Dewar Style Cold Trap (recommended cold trap) Bullseye Precision Vacuum Gauge (premium vacuum gauge for measuing depth) CT40 or CT80 Electronic Cold Trap (electronic cold trap, dry ice replacement) J-KEM Digital Vapor Temp Monitor (digital vapor temp monitor with data-logging capabilites) Specifications: Boiling Flask Size: 5L Receiving Flask Size: 2x 500mL, 1000mL Batch Capacity approximate: 1000-2500 grams Run time: 4 to 8 hours dependent upon material composition and throughput Distillation Temperature Range: 140-250C (Do not exceed 250C) Recommended Condenser Temperature: 40-50C This Kit Includes: Glass components: 5L Boiling Flask P5V6 Distillation Head Triple Neck Cow 2x 500mL Receiving Flask 1L Receiving Flask 120mm Glass Funnel Accessories: PTFE Magnetic Stir Bar Retriever 5 Pack of Metal Keck Clips Dow Corning High Vacuum Silicone Grease Tripod Stand 5L Digital Heating and Stirring Mantle 3-Finger Adjustable Clamp 0-77mm 6" x 6" Scissor Jack 500-1000mL Cork Stand 2x 24/40 ChemglassPTFE Thermometer Inlet Adapter 10ft of Gum Rubber Vacuum Hose 10ft of Silicone Chiller Hose 1/4" Vacuum Manifold Traceable Kangaroo Thermometer - Digital 10 Pack of Adjustable Stainless Steel Tubing Clamps Fiberglass Insulation Rope 10 Feet 1.5 Gallon Cold Trap (2QT Tank) Dry Ice, Liquid Nitrogen w/ 2x 1/4" Barb Adapters Distillation Quick Start Guide This guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs, Before beginning distillation, ensure the following steps have been taken: Vacuum Pump is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed. All glass components are in good working order and ready to be assembled A winterization and degassing procedure has been done to prepare oil for distillation The unit's max internal temperature cannot exceed 380C. The recommended max set temperature should not exceed 250C Once all three of these steps have been completed, you are ready to begin distilling. Begin by placing stir bar in boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer. Assemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware Attach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation. Connect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system. Connect receiving cow to cold trap. Connect cold trap to manifold. Connect vacuum gauge to manifold. At this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process. Turn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability. Start stir slower and increase speed with temperature. Once you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C. You will see your first fraction somewhere between 180C and 190C or slightly before. This is the “heads” fraction. You will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to “self-clean” the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your “main body” fraction. You will see temps between 190-220C during this fraction. Continue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed. The final “tails” fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The “tails” fraction has an obvious color change and will be darker than the “main body” fraction. You will see temps between 200-250C during this fraction. As fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well. Once process is complete, stop heat, stop stir, and stop vacuum. Let atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation. *Notice to Customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. BVV™ is not responsible for the failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail, which can cause bodily harm or damage to the surrounding area.
$2,200.00
Upgraded TRS21 Compressor Head Complete, Stainless Fittings, Viton
Upgraded TRS21 Compressor Head Complete, Stainless Fittings, Viton Upgrade your TRS21 by purchasing a new Compressor Head with Viton O-rings for butane and propane gas compatibly and stainless steel fittings to meet FDA guidelines on handling of consumable products. This head is assembled here in the USA and is a direct replacement for any TRS21 Compressor Head.
$195.00
Glycerin Filled Vacuum Gauge with 1/4" NPT Back Mount -30inHg-0Psi
BVV -30inHg-0Psi BVV™ Glycerin filled vacuum gauge has a 1/4" MNPT brass connection with a readout of (-30) inHg - 0 PSI. The outer diameter of the gauge measures 2.25" We provide adapters to fit your setup in MNPT, FNPT, MJIC, FJIC, and standard compression tubing.
$18.00
BVV™ 8 Ton 304SS Puck Press
BVV™ 8 Ton 304SS Puck Press This BVV™ 8 Ton 304SS Puck Press allows users to compress material into an easily manageable puck. Specifications: 304 Stainless Steel Components (Excludes Jack) External Dimensions - 7-1/8" x 7-1/8" x 14" Internal Puck Mold Diameter - 3.75" Mold Height - 3-1/4" Weight - 34LBS
$315.00
Bore Through 1/2" Compression Fitting x 1/2" MJIC
Bore Through 1/2" Compression Fitting x 1/2" MJIC made out of 304 stainless steel.
$12.00
7.5CF BVV™ Neocision ETL Lab Certified Vacuum Oven
7.5CF BVV™ Neocision Certified Lab Vacuum Oven, 5 Individually Heated Shelves, LED's - 3 Year Warranty Disclaimer: This unit is intended for LEGAL purposes only, to be used in accordance with local laws and ordinances. Use only in well-ventilated areas! Introduction Our vacuum ovens are purpose-built to perform degassing / purging of light hydrocarbon solvents. Using the technique of cold boiling, the oven applies a gentle heat under reduced pressure conditions to expedite solvent degassing while simultaneously preserving color, aroma, and overall solute quality. We've applied our extensive vacuum expertise and industry experience to produce a series of ovens designed exactly for your needs: low consumption, high-throughput, and reliable operation. Performance Capabilities At Best Value Vacs, we make every effort to provide oven performance capabilities in a standardized format. We're not interested in juking our stats to make a sale. Instead, our goal is to provide quality, transparent production capabilities that meet the demands of our professional customers. Temperature Stability: ±1.0° Temperature Uniformity: within 4% of the temperature setpoint. Heat-Up Time: 20 minutes. Ultimate Vacuum: <500 µmHg / mTorr / micron. Time to Vacuum: 10 minutes to 29"Hg using our VE Series 12cfm Dual Stage Vacuum Pump. Vacuum Hold: guaranteed to lose less than 1"Hg (25.4 torr) in 24 hours. Technical Data Electrical Voltage 120V Frequency 60Hz Power 1960W Current 20A Plug IEC C13 (unit ships with detachable NEMA 5-20 cable) Internal Chamber Heating Individual direct-heat shelves Chamber Material Stainless Steel Dimensions (LxWxH) 22" x 23.25" x 25.25" Vacuum Gauge Style Glycerin-filled for accuracy and longevity Range (units) -30 to 0 (inHg) / -1 to 0 (bar) Shelving Ships With 5 Heated Shelves Shelf Dimensions (LxW) 21.5" x 21.5" Shelf Capacity 462 in2 Total Shelf Capacity 2311 in2 / 16.1 ft2 Safety Seal Silicone on Tempered Glass Window Dimensions (LxH) 20.25" x 23.75" Lights 4 strips of LEDs provide a clear, bright view of the interior Handle No plastic, all metal parts for lifetime durability Exterior Dimensions (LxWxH) 35" x 33" x 34.5" Weight 430 lbs Support Locking Casters Safety Electrical Built-in, resettable, overcurrent circuit breaker Thermal Automatic overtemperature shutoff Compliance CE CE Listing Recognized ISO ISO 9001:2015 ETL Certified Conforms to ANSI/UL STD.61010-1, 61010-2-010 -- Certified to CAN/CSA STD. C22.2 NO.61010-1, 61010-2-010 Connections Vacuum Inlet KF25 / NW25, quarter-turn valve Purge Inlet 5/16" Barbed, 10-turn valve Atmospheric Release Quick-release dial Contains Ships With KF25 x 1/4" JIC Flare with 1/4" vacuum hose User Manual Included Vacuum Pump Sold Separately. Warranty 3 Years Capacity and Throughput Planning Oven capacity requirements vary widely by the producer. We wanted to create a method to assist in determining the best oven match for your operation, based on a few of the parameters of your extraction and of your desired purge. We based this formula on an expected extraction yield of 25%, with an extract-density of 1 g/in2. Using the following variables, this formula is designed to provide an estimate of your required shelving capacity: Size = Extraction Batch Size (lbs) Number = Runs per 24h Period Purge = Your desired purging duration (hours) Area Required (ft2) = [(Size) * (Number) * (Purge+1)] / 122 Area Required (in2) = (Size) * (Number) * (Purge+1) * 1.18 Note: This item is a freight ship item and will ship Via UPS Ground Freight. Expedited freight can only be calculated by calling customer service 331-281-0154. All orders with expedited freight through the website will not be honored and will need to be re-quoted. A valid Phone Number IS REQUIRED to ship, Otherwise UPS freight Cannot Contact you for a delivery setup window. Freight Time is 2-5 Days. West Coast 5 Days, Midwest 2 days, East Coast 3-4 days.
$8,100.00
Best Value Vacs 1 Gallon Flat Stainless Steel Vacuum Chamber W/GLASS LID
1 Gallon Shatter Vac Flat Stainless Steel Vacuum Chamber W/ GLASS LID (Comes with 2 Year Limited warranty) This is a complete BestValueVac® vacuum chamber setup designed built and 100% tested in Naperville, Illinois. With our unique patent pending gasket design (Patent #9475627) this chamber is sure to last 10,000 uses with proper care and maintenance. The gasket itself is reversible (doubling the life of our system) allowing customers to instantly take it off and flip it over. Every chamber is tested prior to shipping to lose no more than 2.5Hg/24hrs. -Please Refer to these charts for vacuum specifications at altitude and conversions: Vacuum at Altitude Chart Vacuum Conversion Chart Key Features: High Strength Stainless Steel Chamber Highly Durable and Reversible Silicone Gasket Glycerin filled vacuum gauge User friendly vacuum connections that fit most vacuum pumps on the market 50 Micron Air filter for reducing airborne contaminants when releasing the vacuum Silicone vacuum pad 5' of vacuum rated HVAC hose to pull a vacuum. Specification Chamber Material 304 Stainless Steel Gasket Material Silicone Lid Material Glass Internal Dimensions (ID) 3" Tall x 10.25" Diameter Vacuum Gauge (Glycerin Filled) InHG (0)-(-30) Manifold Connections 1/4" SAE and 1/4" FNPT Temperature Rating 150°F (65°C) Additional Included Items 5' Purple Vacuum Rated HVAC Hose Platinum Cured Silicone Pad Black 50 Micro Air Filter Compatibility Explanation: BestValueVac® Chambers are not compatible with stabilization resin (i.e. Cactus Juice™, Gator Venom™, Minwax™ etc.), alcohol, ethanol, acetone and acrylic based monomers or polymers.The lid may only be cleaned with soapy water. DOES NOT APPLY TO GLASS LID VERSION ShatterVac® chambers are not compatible with stabilization resin (i.e. Cactus Juice™, Gator Venom™, Minwax™ etc.), acetone, acrylic based monomers or polymers. The lid may be cleaned with soapy water and low strength cleaning agents. GlassVac® chambers are compatible with all solvents and stabilization resins. We only recommend and warranty GlassVac® chambers for resin infusion and wood stabilization.The lid may be cleaned with any solvent or cleaning agent. See FAQ at the top for product safety warnings. Pump Warranty Information: Customers using solvents such as stabilization resins (MinWax™, Gator Venom™ etc.), alcohol and other polar solvents must use the vacuum pumps in conjunction with a cold trap for evacuations in excess of 5 minutes. (Exludes Cactus Juice™) If the consumer is using the pump for prolonged periods of time exceeding 5 minutes we require that a cold trap is used or the pump warranty is void. These stabilization resins have the ability to break down the internal components of the pump that are plastic resulting in a seized motor voiding all warranties. When evacuation exceeds 5 minutes these solvents begin to vaporize and then re-condense in the vacuum pump reservoir. Once enough solvent re-condenses in the pump displacing the oil the plastic internal components may begin to warp, melt or seize. The use of a cold trap will condense the vapors prior to making their way to the vacuum pump preventing pump damage due to excessive use. Furthermore, Minwax Wood Hardener™ is not to be used with any vacuum pumps, EVER. (A seized motor will result within the first use.) To prevent these issues from happening to your process, change the Oil after each vacuum pump use, Even if the use time is only 5min. For shipping info including Import/Export details visit our Shipping link at the bottom of the page.
$135.00
Dry Ice Condenser for 2L Electric Lift Rotary Evaporator
Dry Ice Condenser for 2L Best Value Electric Lift Rotary Evaporators. *Notice to customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. **Glassware Safety Disclaimer: BVV™ is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.**
$375.00
1L Standard Distillation Turnkey Setup
1L Standard Distillation Turnkey Setup The Standard Distillation Turnkey Setup includes all the components necessary to successfully perform distillation at an entry level price point. The Standard Turnkey Setup Includes: 1L Distillation Kit 1/4" Flare x 1/4" Barb Adapter BVV™ 5L Heated Circulator BVV™ V9D 9CFM Two Stage Vacuum Pump Distillation Quick Start Guide This guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs, Before beginning distillation, ensure the following steps have been taken: Vacuum Pump is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed. All glass components are in good working order and ready to be assembled A winterization and degassing procedure has been done to prepare oil for distillation Once all three of these steps have been completed, you are ready to begin distilling. Begin by placing stir bar in boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer. Assemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware Attach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation. Connect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system. Connect receiving cow to cold trap. Connect cold trap to manifold. Connect vacuum gauge to manifold. At this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process. Turn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability. Start stir slower and increase speed with temperature. Once you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C. You will see your first fraction somewhere between 180C and 190C or slightly before. This is the “heads” fraction. You will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to “self-clean” the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your “main body” fraction. You will see temps between 190-220C during this fraction. Continue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed. The final “tails” fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The “tails” fraction has an obvious color change and will be darker than the “main body” fraction. You will see temps between 200-250C during this fraction. As fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well. Once process is complete, stop heat, stop stir, and stop vacuum. Let atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation. ***Note: This entire setup will ship via motor freight.*** *Notice to Customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. BVV™ is not responsible for the failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail, which can cause bodily harm or damage to the surrounding area.
$2,100.00 - $2,350.00
P10V6 Neocision Distillation Head - USA Made
P10V6 Distillation Head P10V6 Distillation Head has 6 sets of vigreux in the distillation column with 45/50 lower joint, 24/40 Thermometer Joint, and a 34/45 side joint and includes GL-14 barb connections. MADE IN THE USA Designed for 10 Liter Flasks Set of 6 vigreux to allow for packing media Larger vacuum jacket allows for less heat loss during distillations Larger vapor path to allow for gas/vapor phase flow Increased internal diameter for faster, more efficient fractioning as well as packing and unpacking of media Increased condenser length and diameter for more efficient condensation of vapor with zero clogging *Notice to customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. **Glassware Safety Disclaimer: BVV™ is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.**
$825.00
Best Value Vacs 2 Gallon Aluminum Vacuum Chamber W/GLASS LID
2 Gallon Vacuum & Degassing Chamber W/GLASS LID (Comes with 2 yr Limited Warranty) This is a complete BestValueVac® vacuum chamber setup designed built and 100% tested in Naperville, Illinois. With our unique patent pending gasket design (Patent #9475627) this chamber is sure to last 10,000 uses with proper care and maintenance. The gasket itself is reversible (doubling the life of our system) allowing customers to instantly take it off and flip it over. Every chamber is tested prior to shipping to lose no more than 2.5Hg/24hrs. -Please Refer to these charts for vacuum specifications at altitude and conversions: Vacuum at Altitude Chart Vacuum Conversion Chart Key Features: Aluminum Vessel Highly Durable and Reversible Silicone Gasket Glycerin filled vacuum gauge User friendly vacuum connections that fit most vacuum pumps on the market 50 Micron Air filter for reducing airborne contaminants when releasing the vacuum Silicone vacuum pad 5' of vacuum rated HVAC hose to pull a vacuum. Specification Chamber Material 3004 Aluminum Gasket Material Silicone Lid Material Glass Internal Dimensions (ID) 6.5" Tall x 10" Diameter Vacuum Gauge (Glycerin Filled) InHG (0)-(-30) Manifold Connections 1/4" SAE and 1/4" FNPT Temperature Rating 150°F (65°C) Additional Included Items 5' Purple Vacuum Rated HVAC Hose Platinum Cured Silicone Pad Black 50 Micron Air Filter Compatibility Explanation: BestValueVac® Chambers are not compatible with stabilization resin (i.e. Cactus Juice™, Gator Venom™, Minwax™ etc.), alcohol, ethanol, acetone and acrylic based monomers or polymers.The lid may only be cleaned with soapy water. ShatterVac® chambers are not compatible with stabilization resin (i.e. Cactus Juice™, Gator Venom™, Minwax™ etc.), acetone, acrylic based monomers or polymers. The lid may be cleaned with soapy water and low strength cleaning agents. GlassVac® chambers are compatible with all solvents and stabilization resins. We only recommend and warranty GlassVac® chambers for resin infusion and wood stabilization.The lid may be cleaned with any solvent or cleaning agent. See FAQ at the top for product safety warnings. Pump Warranty Information: Customers using solvents such as stabilization resins (MinWax™, Gator Venom™ etc.), alcohol and other polar solvents must use the vacuum pumps in conjunction with a cold trap for evacuations in excess of 5 minutes. (Exludes Cactus Juice™) If the consumer is using the pump for prolonged periods of time exceeding 5 minutes we require that a cold trap is used or the pump warranty is void. These stabilization resins have the ability to break down the internal components of the pump that are plastic resulting in a seized motor voiding all warranties. When evacuation exceeds 5 minutes these solvents begin to vaporize and then re-condense in the vacuum pump reservoir. Once enough solvent re-condenses in the pump displacing the oil the plastic internal components may begin to warp, melt or seize. The use of a cold trap will condense the vapors prior to making their way to the vacuum pump preventing pump damage due to excessive use. Furthermore, Minwax Wood Hardener™ is not to be used with any vacuum pumps, EVER. (A seized motor will result within the first use.) To prevent these issues from happening to your process, change the Oil after each vacuum pump use, Even if the use time is only 5min. For shipping info including Import/Export details visit our Shipping link at the bottom of the page.
$124.00
Glass Vac™ 16.75" Diameter LID
Glass Vac 16.75" Diameter LID Our patented gasket #9475627 Disclaimer: This item Includes Lid and Gasket Only This is a Replacement Lid for the following Vacuum Chambers: Glass Vac 15 Gallon Aluminum Vacuum Chamber
$213.00
Glass Vac 1.5 Gallon TALL Stainless Steel Vacuum Chamber and Vacuum Pump Kit
Glass Vac 1.5 Gallon TALL Stainless Steel Vacuum Chamber and Vacuum Pump Kit (Chamber comes with 2 yr. limited warranty) This is a complete BestValueVac® vacuum chamber setup designed built and 100% tested in Naperville, Illinois. With our unique patent pending gasket design (Utility Patent #14/533,548) this chamber is sure to last 10,000 uses with proper care and maintenance. The gasket itself is reversible (doubling the life of our system) allowing customers to instantly take it off and flip it over. Every chamber is tested prior to shipping to lose no more than 2.5Hg/24hrs. Please refer to these charts for vacuum specifications at altitude and conversions: Vacuum at Altitude Chart Vacuum Conversion Chart This Kit Includes: Glass Vac 1.5 Gallon TALL Stainless Steel Vacuum Chamber VE115 3CFM Single Stage Vacuum Pump or V4D 4CFM Two Stage Vacuum Pump 2 year limited warranty on the chamber 1 year limited warranty on the pump Key Features: High Strength Stainless Steel Chamber Highly Durable and Reversible Silicone Gasket Glycerin filled vacuum gauge User friendly vacuum connections that fit most vacuum pumps on the market 50 Micron Air filter for reducing airborne contaminants when releasing the vacuum Silicone vacuum pad 5' of vacuum rated HVAC hose to pull a vacuum. Specification Chamber Material 304 - 2B Stainless Steel Gasket Material Silicone Lid Material Glass Internal Dimensions (ID) 8-5/8" Tall x 7-1/8" Diameter Vacuum Gauge (Glycerin Filled) InHG (0)-(-30) Manifold Connections 1/4" SAE and 1/4" FNPT Temperature Rating 150°F (65°C) Additional Included Items 5' Purple Vacuum Rated HVAC Hose Platinum Cured Silicone Pad Black 50 Micro Air Filter Models BVV4D BVV7S BVV9D Stage 2 1 2 Ultimate Vacuum (Microns) 15 75 15 Refrigerant Classes A1 Non-Toxic, Non Flammable Dimensions (in) 12.4 x 4.8 x 10.16 12.4 x 4.8 x 10.16 15 x 6.3 x 11.22 Weight (lbs) 19.4 16.5 32 Free Air Displacement 4.3 CFM 6.4 CFM 8.5 CFM Motor Size (HP) RPM 1 HP 3440 RPM Oil Capacity 10oz / 300ml 14.5oz / 410ml 24oz / 680ml Voltage 110V 60 Hz Power Cord Hard Wired 3m / 9.8' Power Cord Power Switch Standard On / Off Operating Temperature Range 32F to 125 F (0C to 52C) Gas Ballast Valve Yes No Yes Intake Fittings Stainless Steel Inlet Fitting with 1/4" SAE & 3/8" JIC Male Ports VE115 Specification Free Air Displacement - (CFM) 3CFM # Of Stages 1 Voltage 110v / 60Hz Ultimate Vacuum 5 Pa HP 1/4 Oil Capacity 280ml Weight 15LB Intake Connection 1/4" SAE & JIC Compatibility Explanation: BestValueVac® chambers are not compatible with stabilization resin (i.e. Cactus Juice™, Gator Venom™, Minwax™ etc.), alcohol, ethanol, acetone and acrylic based monomers or polymers. The lid may only be cleaned with soapy water. SVac® chambers are not compatible with stabilization resin (i.e. Cactus Juice™, Gator Venom™, Minwax™ etc.), acetone, acrylic based monomers or polymers. The lid may be cleaned with soapy water and low strength cleaning agents. GlassVac® chambers are compatible with all solvents and stabilization resins. We only recommend and warranty GlassVac® chambers for resin infusion and wood stabilization. The lid may be cleaned with any solvent or cleaning agent. See FAQ at the top for product safety warnings. Pump Warranty Information: Customers using solvents such as stabilization resins (MinWax™, Gator Venom™ etc.), alcohol and other polar solvents must use the vacuum pumps in conjunction with a cold trap for evacuations in excess of 5 minutes. (Excludes Cactus Juice™) If the consumer is using the pump for prolonged periods of time exceeding 5 minutes we require that a cold trap is used or the pump warranty is void. These stabilization resins have the ability to break down the internal components of the pump that are plastic resulting in a seized motor voiding all warranties. When evacuation exceeds 5 minutes these solvents begin to vaporize and then re-condense in the vacuum pump reservoir. Once enough solvent re-condenses in the pump displacing the oil the plastic internal components may begin to warp, melt or seize. The use of a cold trap will condense the vapors prior to making their way to the vacuum pump preventing pump damage due to excessive use. Furthermore, Minwax Wood Hardener™ is not to be used with any vacuum pumps, EVER. (A seized motor will result from the first use.) To prevent these issues from happening to your process, change the Oil after each vacuum pump use, Even if the use time is only 5min. For shipping info including Import/Export details visit our Shipping link at the bottom of the page.
$288.00 - $457.00
Teleflex USA High Pressure Smooth Bore PTFE Braided Stainless Steel Hose
Teleflex Lightweight high-pressure hose is specially constructed for applications requiring strength, reliability and long-term performance along with low profile and flexibility. Added to this is the wide temperature range in which these hoses operate. These advantages combine to make Teleflex hose the choice for hot oils, phosphate esters, industrial gases and chemicals and many more. This hose is constructed of a smooth innertube of PTFE impregnated with carbon black to provide conductivity for status dissipations. The outer braids unique bunch braid design made with 300 series stainless steel. Properties of PTFE Tensile Strength @ 73F 1500-3000lb./sq. in. Elongation @ 73F 100-200% Stiffness @ 73F 60,000 lb./sq. in. Impact Strength, Izod 70F 2.0 ft. - lb./in. 73F 3.5 ft. - lb./in. 170F 6.0 ft. - lb./in Hardness Durometer D55-D70 Compressive Stress at 1% Deformation @ 73F 600 lb./sq. in. @ 1% Offset @ 73F 1000 lb./sq. in Deformation Under Load @ 122°F 1200 lb./sq. in., 24 hrs. 4-8% 2000 lb./sq. in., 24 hrs. 25% Heat-Distortion Temperature, 66 lb./sq. in. 250°F Coefficient of Linear Thermal Expansion Per °F, 77-140°F 5.5x10-5 Thermal Conductivity, 0.18 in. 1.7 B.T.U./hr./sq.ft./°F/in. Specific Heat 0.25 B.T.U./lb./°F Water Absorption 0.0° Flammability Nonflammable Specific Gravity 2.1-2.3 Useful Conversions 1 p.s.i. = 0.0689 bar 1 Atms = 14.70 p.s.i. 1 bar = 14.5035 p.s.i. 1 Atms = 29.92 in. mercury 1 p.s.i. = 0.0703 Kg/sq.cm 1 m. = 3.281 ft. 1 Kg/sq.cm = 14.22 p.s.i. 1 ft. = 0.3048 m.
$60.00 - $79.00
ASME Certified 50L Jacketed Solvent Tank 304L with Diptube
ASME Certified 50L Jacketed Solvent Tank 304L with Diptube This is a custom manufactured USA made ASME Certified 50LB Jacketed Collection base with UM Stamp and made out of 304L Stainless Steel. This base is designed to be configured to any application and can even be used as a solvent tank. This tank comes preconfigured as a collection base with dip tube and SSP Valves, sight glasses, 1/2" Hose Barbs and will hold around 50LBS of liquid butane and is able to have fluid circulated around the outer jacket to increase recovery speeds in the extraction system. **This Item will ship Via FREIGHT ONLY. Specifications Material 304L Stainless Steel Certification: ABILITY ENGINEERING TECHNOLOGY INC. ASME / UM / NB MAWIWP 350 PSI at 150°F MAWEWP N/A MIN TEMP -20°F at 350PSI Butane Capacity ~50LBS Connection Sizes: 6" Tri-Clamp (2) 1" NPT (2) 1/2" NPT - Outer Jacket Ports (2) 3/8" NPT Weight 146LBS Outer Dimensions: 32-7/8" Tall 14" Diameter Inner Dimensions: 24" Tall 12" Diameter
$4,250.00
Best Value Vacs 3 Gallon Stainless Steel Vacuum Chamber W/GLASS LID
3 Gallon Stainless Steel Vacuum & Degassing Chamber W/GLASS LID (Comes with 2 Year Limited warranty) This is a complete BestValueVac® vacuum chamber setup designed built and 100% tested in Naperville, Illinois. With our unique patent-pending gasket design (Patent #9475627) this chamber is sure to last 10,000 uses with proper care and maintenance. The gasket itself is reversible (doubling the life of our system) allowing customers to instantly take it off and flip it over. Every chamber is tested prior to shipping to lose no more than 2.5Hg/24hrs. -Please Refer to these charts for vacuum specifications at altitude and conversions: Vacuum at Altitude Chart Vacuum Conversion Chart Key Features: High Strength Stainless Steel Chamber Highly Durable and Reversible Silicone Gasket Glycerin filled vacuum gauge User-friendly vacuum connections that fit most vacuum pumps on the market 50 Micron Air filter for reducing airborne contaminants when releasing the vacuum Silicone vacuum pad 5' of vacuum rated HVAC hose to pull a vacuum. Specification Chamber Material 304 Stainless Steel Gasket Material Silicone Lid Material Glass Internal Dimensions (ID) 10-7/8" Tall x 9" Diameter Vacuum Gauge (Glycerin Filled) InHG (0)-(-30) Manifold Connections 1/4" SAE and 1/4" FNPT Temperature Rating 150°F (65°C) Additional Included Items 5' Purple Vacuum Rated HVAC Hose Platinum Cured Silicone Pad Black 50 Micro Air Filter Compatibility Explanation: BestValueVac® Chambers are not compatible with stabilization resin (i.e. Cactus Juice™, Gator Venom™, Minwax™ etc.), alcohol, ethanol, acetone and acrylic-based monomers or polymers.The lid may only be cleaned with soapy water. DOES NOT APPLY TO GLASS LID VERSION ShatterVac® chambers are not compatible with stabilization resin (i.e. Cactus Juice™, Gator Venom™, Minwax™ etc.), acetone, acrylic-based monomers or polymers. The lid may be cleaned with soapy water and low strength cleaning agents. GlassVac® chambers are compatible with all solvents and stabilization resins. We only recommend and warranty GlassVac® chambers for resin infusion and wood stabilization. The lid may be cleaned with any solvent or cleaning agent. See FAQ at the top for product safety warnings. Pump Warranty Information: Customers using solvents such as stabilization resins (MinWax™, Gator Venom™, etc.), alcohol and other polar solvents must use the vacuum pumps in conjunction with a cold trap for evacuations in excess of 5 minutes. (Excludes Cactus Juice™) If the consumer is using the pump for prolonged periods of time exceeding 5 minutes we require that a cold trap is used or the pump warranty is void. These stabilization resins have the ability to break down the internal components of the pump that are plastic resulting in a seized motor voiding all warranties. When evacuation exceeds 5 minutes these solvents begin to vaporize and then re-condense in the vacuum pump reservoir. Once enough solvent re-condenses in the pump displacing the oil the plastic internal components may begin to warp, melt or seize. The use of a cold trap will condense the vapors prior to making their way to the vacuum pump preventing pump damage due to excessive use. Furthermore, Minwax Wood Hardener™ is not to be used with any vacuum pumps, EVER. (A seized motor will result within the first use.) To prevent these issues from happening to your process, change the Oil after each vacuum pump use, Even if the use time is only 5min. For shipping info including Import/Export details visit our Shipping link at the bottom of the page.
$152.00
Best Value Vacs 3 Gallon Aluminum Vacuum Chamber W/GLASS LID
Best Value Vacs 3 Gallon Aluminum Vacuum Chamber W/GLASS LID Comes with 2 yr Limited Warranty This is a complete BestValueVac® vacuum chamber setup designed built and 100% tested in Naperville, Illinois. With our unique patent pending gasket design (Patent #9475627) this chamber is sure to last 10,000 uses with proper care and maintenance. The gasket itself is reversible (doubling the life of our system) allowing customers to instantly take it off and flip it over. Every chamber is tested prior to shipping to lose no more than 2.5Hg/24hrs. *Please Refer to these charts for vacuum specifications at altitude and conversions: Vacuum at Altitude Chart Vacuum Conversion Chart Key Features: Aluminum Vessel Highly Durable and Reversible Silicone Gasket Glycerin filled vacuum gauge User friendly vacuum connections that fit most vacuum pumps on the market 50 Micron Air filter for reducing airborne contaminants when releasing the vacuum Silicone vacuum pad 5' of vacuum rated HVAC hose to pull a vacuum. Specification Chamber Material 3004 Aluminum Gasket Material Silicone Lid Material Glass Internal Dimensions (ID) 9" Tall x 10" Diameter Vacuum Gauge (Glycerin Filled) InHG (0)-(-30) Manifold Connections 1/4" SAE and 1/4" FNPT Temperature Rating 150°F (65°C) Additional Included Items 5' Purple Vacuum Rated HVAC HosePlatinum Cured Silicone PadBlack 50 Micro Air Filter Compatibility Explanation: BestValueVac® Chambers are not compatible with stabilization resin (i.e. Cactus Juice™, Gator Venom™, Minwax™ etc.), alcohol, ethanol, acetone and acrylic based monomers or polymers.The lid may only be cleaned with soapy water. DOES NOT APPLY TO GLASS LID VERSION ShatterVac® chambers are not compatible with stabilization resin (i.e. Cactus Juice™, Gator Venom™, Minwax™ etc.), acetone, acrylic based monomers or polymers. The lid may be cleaned with soapy water and low strength cleaning agents. GlassVac® chambers are compatible with all solvents and stabilization resins. We only recommend and warranty GlassVac® chambers for resin infusion and wood stabilization.The lid may be cleaned with any solvent or cleaning agent. See FAQ at the top for product safety warnings. Pump Warranty Information: Customers using solvents such as stabilization resins (MinWax™, Gator Venom™ etc.), alcohol and other polar solvents must use the vacuum pumps in conjunction with a cold trap for evacuations in excess of 5 minutes. (Exludes Cactus Juice™) If the consumer is using the pump for prolonged periods of time exceeding 5 minutes we require that a cold trap is used or the pump warranty is void. These stabilization resins have the ability to break down the internal components of the pump that are plastic resulting in a seized motor voiding all warranties. When evacuation exceeds 5 minutes these solvents begin to vaporize and then re-condense in the vacuum pump reservoir. Once enough solvent re-condenses in the pump displacing the oil the plastic internal components may begin to warp, melt or seize. The use of a cold trap will condense the vapors prior to making their way to the vacuum pump preventing pump damage due to excessive use. Furthermore, Minwax Wood Hardener™ is not to be used with any vacuum pumps, EVER. (A seized motor will result within the first use.) To prevent these issues from happening to your process, change the Oil after each vacuum pump use, Even if the use time is only 5min. For shipping info including Import/Export details visit our Shipping link at the bottom of the page.
$135.00
P5 Distillation Head - USA Made
P5 Distillation Head P5 Packable Distillation Head with 34/45 lower joint and 24/40 upper and side joints. Includes GL-14 Barb Connections. Recommended packing media: Raschig Rings, Porcelain Berl Saddles, Glass Beads, Pro-Pak, or Stainless Steel Wool. Key Features: MADE IN THE USA Designed for 5 Liter Flasks Single set of lowered vigreaux to allow for packing media Larger vacuum jacket allows for less heat loss during distillations Larger vapor path to allow for gas/vapor phase flow Increased internal diameter for faster, more efficient fractioning as well as packing and unpacking of media Increased condenser length and diameter for more efficient condensation of vapor with zero clogging *Notice to customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. **Glassware Safety Disclaimer: BVV™ is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.**
$850.00
50L Solvent Pro Series Glass Axis
50L Solvent Pro Series Glass Axis. *Notice to customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. **Glassware Safety Disclaimer: BVV™ is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.**
$90.00
Harvest Right Premier Vacuum Pump
Harvest Right Premier Vacuum Pump Technical Specifications Oil: Robinair Premium High Vacuum Pump Oil or JB Industries Black Gold Vacuum Pump Oil Only DC Motor Energy Efficient Voltage: Standard, 110v, 60Hz Dimensions: 16.3″ x 6″ x 12.1″ Weight: 32lbs Noise: 52 decibels Product Comparison: Premier Oil Pump vs Standard Oil Pump Oil Changes: This new Premier Pump rarely needs to have the oil changed or filtered. The pump has a gas ballast feature that makes it so water does not stay in the oil. Because of this, the oil in the pump will be pristine and clear, even after 30 or more batches. You simply won’t need to change the oil until you have run 20 or more batches. Whereas, the oil in the Standard Vacuum Pump needs to be changed and filtered every 4 or 5 batches (when using the new 3/8 inch vacuum hose). You should only replace the oil in this pump with Robinair Premium High Vacuum Pump Oil (or with JB Industries Black Gold Vacuum Pump Oil). These may be purchased from Harvest Right, Amazon, and other locations. Do not use Dairyland vacuum pump oil in the Premier pump. Vacuum Pressure: Under cold and hot conditions the Premier Pump will pull a deeper vacuum than the Standard Pump. Under cold conditions the difference is .05 Pascal for the Premier Pump and .08 Pascal for the Standard Pump. Whereas, under warm conditions the difference is much greater: .05 Pascal for the Premier Pump and 2.05 Pascal for the Standard Pump.Hence, the Premier Pump is especially not affected by warm, ambient conditions. When temperatures rise, it will pull a vacuum far better than the Standard Pump. The Premier Pump is just not affected by outside heat. It pulls the same deep vacuum even when it is in a warm environment. Noise: The Premier Pump is substantially quieter than the Standard Pump, 52 decibels versus 64 decibels. The Industrial Pump at 52 decibels is about the same as a refrigerator. Oil Mist Filter: Both pumps come with an oil mist filter. However, the Premier Pump’s oil mist filter allows for no oil spray at all and it will last much longer. Power Use: The Premier Pump uses less power than the Standard Pump (187 watts versus 218 watts). Amperage: Under hot conditions at ultimate vacuum pressure the Standard Pump pulls 2.1 amps while the Premier Pump only pulls 1.7 amps. Hence, the Premier Pump is more efficient. Weight: The Premier Pump is easier to move around as it weighs 5 pounds less than the Standard Pump (32 lbs. versus 37 lbs.) Life: The Premier Pump is more durable and will last longer than the Standard Pump.
$795.00
Harvest Right PHARMACEUTICAL PRO Freeze Dryer - Medium
Harvest Right™ PHARMACEUTICAL PRO Freeze Dryer - Medium 7 TRAYS 6.5 sq ft tray space 4 LITERS OF ICE CAPACITY Key Features & Benefits - The freeze dryer has built in intelligence. It automatically and perfectly manages the freeze drying process - The ideal vacuum pressure and drying temperature is maintained for each material – preserves freshness and potency - 6.5 square feet of tray space - Shelving unit holds 7 trays (each tray 7.5″ W x 18″ L x 0.75″ H) - 4 liters of ice capacity - Weight: 127 lbs. Warranty 3 year limited warranty Dimensions Overall product dimensions: 18″ W x 21.25″ D x 28.5″ H Perfect for a counter top, cart or table. Power 110 volt outlet. Shipping Info - The medium freeze dryer ships in one package with a total weight of 216 lbs. - Item will be delivered to physical addresses, no PO boxes. - One freeze dryer package: 26″W x 36″D x 45″H. Maintenance Simply filter and replace oil. Takes one or two minutes. Industrial Grade Design High quality, super high vacuum High evacuation performance Light, fast, energy efficient Technical Specifications Oil: Harvest Right Oil, Robinair Premium High Vacuum Pump Oil or JB Industries Black Gold Vacuum Pump Oil Only DC Motor Energy Efficient Voltage: Standard, 115v, 60Hz Dimensions: 16.3″ x 6″ x 12.1″ Weight: 32 lbs Noise: 52 decibels Product ComparisonIndustrial Oil Pump vs Standard Oil Pump Oil ChangesThis new Industrial Pump rarely needs to have the oil changed or filtered. The pump has a gas ballast feature that makes it so water does not stay in the oil. Because of this, the oil in the pump will be pristine and clear, even after 30 or more batches. You simply won’t need to change the oil until you have run 25 to 40 batches. Whereas, the oil in the standard vacuum pump needs to be changed and filtered every 4 or 5 batches (when using the new 3/8 inch vacuum hose). Vacuum PressureUnder cold and hot conditions the Industrial Pump will pull a deeper vacuum than the Standard Pump. Under cold conditions the difference is .05 Pascal for the Industrial Pump and .08 Pascal for the Standard Pump. Whereas, under warm conditions the difference is much greater: .05 Pascal for the Industrial Pump and 2.05 Pascal for the Standard Pump.Hence, the Industrial Pump is especially not affected by warm, ambient conditions. When temperatures rise, it will pull a vacuum far better than the Standard Pump. The Industrial Pump is just not affected by outside heat. It pulls the same deep vacuum even when it is in a warm environment. NoiseThe Industrial Pump is substantially quieter than the Standard Pump, 52 decibels versus 64 decibels. The Industrial Pump at 52 decibels is about the same as a refrigerator. Oil Mist FilterBoth pumps come with an oil mist filter. However, the Industrial Pump’s oil mist filter allows for no oil spray at all and it will last much longer. Power UseThe Industrial Pump uses less power than the Standard Pump (187 watts versus 218 watts). AmperageUnder hot conditions at ultimate vacuum pressure the Standard Pump pulls 2.1 amps while the Industrial Pump only pulls 1.7 amps. Hence, the Industrial Pump is more efficient. WeightThe Industrial Pump is easier to move around as it weighs 5 pounds less than the Standard Pump (32 lbs. versus 37 lbs.) LifeThe Industrial Pump is more durable and will last longer than the Standard Pump.
$3,295.00 - $4,790.00
MAXTRAP105 -105°C Vacuum Cold Trap, 120V
MAXTRAP105 -105°C Vacuum Cold Trap, 120V Cascade’s MAXTRAP105 is not an ordinary lab-grade cold trap. Cascade has integrated features necessary for time-sensitive, high-throughput, production-focused vacuum purging or drying applications. MAXTRAP105 Cold Trap Includes: Cascade’s COLDWELL 304 Stainless Steel Trap Insert (Patent pending baffle system) 3 Quart Capacity (2839 ml) Viton Gasket for Vacuum Integrity Labconco -105°C Refrigerated Base Green CFC / HFC Free Refrigerants Power Cord 3mm Neoprene Insulator Cap Requires 800ml (~ 3.5 cups) of a transfer fluid such as ethanol. Not Included. Cascade recommends: ethanol, glycol, cryo-cool fluids Quality Made in USA 1 Year Warranty Connection Lines and hardware: 4′ of 1″ Diameter Vacuum Tubing with KF-25 Flanges on each side. KF-25 clamps, centering rings for the connection tube MAXTRAP Tips: Safety At very cold temperatures, solvents and even oxygen can re-condense back into liquid. This is potentially explosive. Liquid oxygen is a light blue color and can condense into a cold trap if a pump has sucked air through the trap when the trap is very cold. Always follow your standard operating procedures and safety guidelines. Don’t Stop: Keep Processing while trap is being reclaimed, cleaned, refreshed Cold traps can become full or the captured material freezes and blocks flow. For high moisture, outgassing, 24 hour processing/vacuum purging consider adding a second, spare COLDWELL trap. The secondary COLDWELL can be dropped into place so processing continues while the full trap is cleaned, defrosted. Quick Start Up Tips: Remove shipping foam from reservoir bottom prior to use Fill reservoir with 800ml (+/-3.5 cups) ethanol to marked line Monitor ethanol levels inside reservoir Allow at least 30 mins for trap to cool Keep side vents clear. Allow at least 4″ for airflow Monitor interior of stainless trap for clogging Short tube – attach to vacuum pump Tall tube – attach to vacuum oven MAXTRAP105 Differences: The key to quality cold trap performance is: time, surface area, and temperature. Time: Most cold traps have very narrow inlets and outlets, slowing down your process. Not Cascade’s MAXTRAP105! Full KF25 inlet and outlet connections never reduce flow. Surface Area: Most cold traps have glass or a smaller surface area to collect the matter your vacuum pump would otherwise ingest. Cascade’s MAXTRAP105 surface area is a patent pending series of filter baffles inside the COLDWELL stainless trap. Specifications Coldwell Stainless Trap KF25 Inlet & Outlet 3 Quart Capacity (2839 mliters) Viton Gasket Neoprene Insulator Cap Labconco -105°C Mechanical Base 115V / 1ph / 3 AMP (60Hz) Cord Included CFC / HCFC Free Refrigerants Dimensions inches 24.1 W x 23.9 D x 12.6 H cm 34.3 x 59.7 x 30.5 *Requires approximately 800ml (~ 3.5 cups) of transfer fluid(ethanol, glycol, cryo-cool fluids) Connections 1 each 4′ KF-25 flanged vacuum rated line 1 each KF-25 Centering Ring 1 each KF-25 Clamp Weight COLDWELL Stainless Trap: 14 lbs Mechanical Base: 139 lbs Shipping Weight: 190 lbs Additional Resources: Download Specs Download Supplemental Manual NTRL Certifications -105C Refrigerated Base Safety Certification
$9,950.00
5L Neocision Short Path Distillation Turnkey Kit
5L Neocision Short Path Distillation Turnkey Kit This unit carries a 2 day lead time. The 5L Premium Distillation Turnkey Setup features our 5L Distillation Kit with P5 Distillation Head and USA made glass. Every component in this turnkey is made for precision, throughput, and repeatable results. Also included is our Pro Series Corrosion Resistant Two Stage Vacuum Pump giving you extreme power and depth with a long lifespan, the Bullseye Precision Vacuum Gauge from Digivac which is the most rugged and dependable vacuum gauge on the market, and a BVV 19L Heated Circulator for maximum condensation of vapors. You will also receive a Dewar Style Glass Cold Trap to keep all volatiles and solvents out of your vacuum system. This Turnkey Setup gives you everything needed to perform distillation at the highest level. The Premium Turnkey Kit Includes: 5L Neocision Kit with P5 Distillation Head KF-25 x 1/4" Barb Adapter Dewar Style Glass Cold Trap Bullseye Precision Vacuum Gauge BVV 19L MX Heated Circulator Pro Series 21.2CFM Corrosion Resistant Two Stage Vacuum Pump Distillation Quick Start Guide This guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs, Before beginning distillation, ensure the following steps have been taken: Vacuum Pump is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed. All glass components are in good working order and ready to be assembled A winterization and degassing procedure has been done to prepare oil for distillation Once all three of these steps have been completed, you are ready to begin distilling. Begin by placing stir bar in boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer. Assemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware Attach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation. Connect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system. Connect receiving cow to cold trap. Connect cold trap to manifold. Connect vacuum gauge to manifold. At this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process. Turn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability. Start stir slower and increase speed with temperature. Once you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C. You will see your first fraction somewhere between 180C and 190C or slightly before. This is the “heads” fraction. You will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to “self-clean” the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your “main body” fraction. You will see temps between 190-220C during this fraction. Continue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed. The final “tails” fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The “tails” fraction has an obvious color change and will be darker than the “main body” fraction. You will see temps between 200-250C during this fraction. As fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well. Once process is complete, stop heat, stop stir, and stop vacuum. Let atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation. ***Note: This entire setup will ship via motor freight.*** ***Note: All units are inspected for broken glass or parts before unit is shipped. If unit arrives damaged or glass is broken (this does not include minor imperfections or scuffs in glassware), Customer MUST contact BVV™ within 3 days of delivery to file a claim and receive a replacement part. If customer DOES NOT contact BVV™ within 3 days of delivery responsibility for replacement parts falls on the customer and they must pay for replacement pieces.*** ***Glassware Safety Disclaimer: BVV™ is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.***
$10,500.00 - $14,750.00
1/2" Fractional Tube Fitting Hose
1/2" Fractional Tube Fitting Hose These chemically resistant PTFE braided hoses are a necessity when dealing with harsh chemicals or solvents and high-pressure applications. They provide a uniquely rugged, durable, and chemically resistant combination of Stainless Steel and PTFE by having an inner core of PTFE and protecting that with a braided stainless steel outer sleeve. These hoses have a tube stub on each end that fits a standard compression fitting. ***Note: Do not exceed the specified hose bend radius or the inner PTFE liner will kink and the hose integrity will become compromised and should not be used. Specifications: Connection Type(s): 1/2" Tube Stub Liner Material PTFE (Teflon) Braid Material 304 Stainless Steel Swivel Material 304 Stainless Steel Temperature Rating -94°F to 500°F (-70°C - 260°C) Pressure Rating 1500 PSI Chemical Resistance Excellent Max Bend Radius 5 1/2"
$47.50 - $88.00
Stainless Steel Laboratory Scissor Jacks
Stainless Steel Scissor Jacks Adjustable height laboratory scissor jack. The platform is 4"/6"/8" & the durable 304 stainless steel heavy-duty lab lifts with very little effort necessary! Specifications: 304 Stainless Steel Platform size: 4" x 4" / 6" x 6" / 8" x 8"
$29.00 - $49.00
BVV™ Stackable Diamond Miner V2
BVV™ Stackable Diamond Miner V2 The Stackable Diamond Miner V2 Diamond miner eliminates the need for glass jars and adds safety to your degassing procedure. Allowing you to see your Diamond growth through the top sight glass and by pulling up the Stackable Diamond Miner Tray once the process is completed. This diamond miner comes rack-mounted with a fully jacketed column and high-pressure clamps.
$2,250.00
3 Way Ball Valve - Fractional Tube Fitting
SSP - 3 Way Ball Valve - Fractional Tube Fitting SSP Instrumentation Flolok® manually operated three-way ball valves accept media through the bottom port and allow selection of flow through a selected port. Features: Directional handle indicates flow direction Panel Mountable 180-degree actuation Directional flow path Micro-finished ball provides positive seal Free-floating ball design provides compensation for seat wear for repetitive sealing Blow-out proof ball & stem Standard Product Testing - Every ball valve is assembled and tested @ 1000 psi (68.9 bar) with Nitrogen Specifications Body Material 316 Stainless Steel Pressure Rating @ 100F 3000 PSIG @37C 208 BAR @300F 2500 PSIG @148C 172 BAR Connection Type 1 Duolok Tube Fitting Connection Size 1 Specified by User Connection Type 2 Duolok Tube Fitting Connection Size 2 Specified by User Connection Type 3 Duolok Tube Fitting Connection Size 3 Specified by User Handle Type Nylon-Stainless Steel Insert Handle Color Black Packing Material PTFE SSP proudly makes Duolok®, TruFit®, FloLok® and hundreds of other products 100% in the USA!
$150.00 - $230.00
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