PUREPATH 100+KIT A with Mechanically Refrigerated Cold Traps

Includes Installation in U.S. (excludes AK, HI)

Cascade’s PUREPATH 100 + KIT A is a 4″ wiped film distillation system with mechanically refrigerated cold traps optimized for viscous crude refinement.

0.1m2 Evaporation surface area
Approx 2-4L/per hour thru-put
Mechanically refrigerated dual glass cold traps by Huber (-100°C & -20°C)
System is professionally delivered & installed on mobile rack
Fused electrical box allows system to run on single 120V – 240V 1PH 50AMP service
Modular & expandable at any time into more automated temperature and control
All tubing, fluids, connections included
NRTL listed components

KIT A: Integrated Mechanically Refrigerated Cold Traps:

Huber MiniChill 600 (-20°C Recirculating Bath) Chills Glass Condensing Coil Trap, includes 5 gal. BioFrost Coolant
Huber TC100 (-100°C Immersion Coil) Chills Glass Trap Insert
UL Listed
2 each 8′ Insulated Hoses

The PUREPATH Difference

There are a number of different distillation systems on the market. Cascade’s PUREPATH 100 + KIT A has a few marked differences.

1) Temperature Delta Of Asahi Glass Helps Minimize Breakage
The truth is – glass breaks and the distillation glassware is expensive to replace. The Asahi glass on the PUREPATH has an industry leading 110°C temperature delta. This means the Asahi glass on the PUREPATH can withstand the temperature shocks associated with rapid, hot to cold temperature changes that could occur with extreme temperature ranges – or when cold ethanol is introduced into the system to clean.

2) Keep It Clean! The Vacuum Integrity Of The Asahi Glass Is Exceptional – Seals And Joints Do Not Require Grease
Many products manufactured in a distillation system are destined for human consumption. The PUREPATH seals and joints are super smooth, which not only means exceptional vacuum integrity, but that you won’t have to introduce grease into the system in order to maintain vacuum. Lesser quality glass will often slightly leak – reducing performance/output and increase labor efforts chasing down small vacuum leaks.

3) The Vacuum Pumping System – Deep, Protected From Contamination & Real Time Graphical Data
The vacuum system features a UL Listed Agilent DS302 Rotary Vane Pump Since the vacuum integrity of the AGI Glass is so strong, it clears the way for the vacuum pump to get deeper to its ultimate pressure of 2×10^-3 mbar. We protect and keep processing clean with a foreline trap on the inlet and an oil mist return.

4) Rodaviss® Couplings For Easy, Safe Disconnect Of Receiving Flasks
Cascade’s PUREPATH minimizes another potential glass break point by utilizing Rodaviss couplings.

5) Professional on-site installation and training. Our installation and training crew is a team of technicians from Cascade Sciences, Asahi Glass and seasoned industry veterans.

Straight Talk About Thru-Put

There are many variables that dictate thru put of any wiped film system. Crude oil will run through at different rates. Depending on initial potency test numbers, expect 2-3 Liters per hour.

To produce quality distillate, crude oil typically must run through the system twice.

• 1st Run strips terpenes and volatiles (Heads)

• 2nd Run distills heavy flower (Body)

Benefits of the PUREPATH 100 include:

• High Evaporation Efficiency
• Minimum Thermal Decomposition
• Gas and Vacuum Tight
• Uniform Thin Film
• Jacketed Evaporator for Easy Viewing
• Uniform Rotating Wiper System (Up to 300°C Option)
• Grease-less Magnetic Sealed Bearing, Valve and Joints
• Perfect for Heat Sensitive Materials
• Short Residence Time

Precision Glass by Asahi
Jacketed Evaporator ID 100mm with evaporation surface area of 0.1m2
Receiver 2000ml, Borosilicate Glass 3.3
Temperature range of glass –90°C to +230°C
Delta of Glass 110°C (the temperature change the glass can withstand without breaking)

External Condenser: Thermal transfer area 0.2m2 with 2 water connectors
Magnetic Seal with Cover –torque 1.1Nm / Cover SS316
Wiper PTFE Wiper +200°C
Overall Design Operating Pressure 0.1 mbar
Cold Finger: Dry Ice capacity of up to 475ml
Temperature Control by Huber
Huber 202 Heating Feed Vessel with Temperature Probe
General information & temperature controller
Temperature range	45°C to 200 °C
Temperature stability	±0.02 °C
Temperature control	TAC, self-optimizing (True Adaptive Control)
Controller	Pilot ONE (E-grade “Basic”)
Safety class	III / FL
Protection class	IP20
Dimensions:	(W x D x H) 178 x 260 x 355 mm
Weight	8 kg
Heating / cooling capacity
Heating capacity	2 kW
Circulation pump
Pressure pump max.	27 l/min ; 0,7 bar
Suction pump max.	22 l/min ; 0,4 bar
Pump connection	M16x1 AG male
Connections
Pt100 connection	Pt100
Digital interface	RS232, Ethernet, USB Device, USB Host
Operating data
Permissible ambient temp.	5°C to 40°C
Bath opening WxD/BD	Ø = 25 / 150 mm
Bath volume	2L
Power supply	230V 1~ 50/60Hz
Current max.	10A
Huber 125 Ministat Cooling Main Body Condenser General information & temperature controller
Temperature range	-25°C to 150°C
Temperature stability	±0.02°C
Temperature control	TAC, self-optimizing (True Adaptive Control)
Controller	Pilot ONE (E-grade “Basic”)
Safety class	III / FL
Protection class	IP20
Dimensions (W x D x H)	225 x 370 x 429 mm
Weight	25kg
Heating / cooling capacity
• Heating capacity	1.5 kW
• Cooling capacity	100 20 0 -10 -20 °C 0.3 0.3 0.21 0.15 0.05 kW
• Cooling machine	air-cooled
• Refrigerant	R290 (0.1 kg)
Circulation pump
• Pressure pump max.	22 lpm ; 0.7 bar \| 5.81 gpm ; 10.15 psi
Suction pump max.	16 lpm ; 0.4 bar \| 4.23 gpm ; 5.8 psi
Pump connection	M16x1 AG male
Permissible viscosity	50 mm²/s
Connections
Pt100 connection	Pt100
Digital interface	RS232, Ethernet, USB Device, USB Host
Operating data
Permissible ambient temp.	5°C to 35°C
Noise Level	47dB(A)
Bath opening W x D / BD	178 x 80 / 120 mm
Bath volume	2.75 Liters
Filling volume min.	2 Liters
Power supply	115V 1~ 50/60Hz
Current max.	11.5 A
Huber 304 Heating Main Body Jacket
General information & temperature controller
Temperature range	28°C to 300 °C
Temperature stability	±0.02 °C
Temperature control	TAC, self-optimizing (True Adaptive Control)
Controller	Pilot ONE (E-grade “Basic”)
Safety class	III / FL
Protection class	IP20
Dimensions	(W x D x H) 210 x 335 x 392 mm
Weight	14kg
Heating / cooling capacity
Heating capacity	3kW
Circulation pump
Pressure pump max.	25 l/min ; 0,7 bar
Suction pump max.	18.5 l/min ; 0,4 bar
Pump connection	M16x1 AG male
Permissible viscosity	50 mm²/s
Connections
Pt100 connection	Pt100
Digital interface	RS232, Ethernet, USB Device, USB Host
Operating data
Permissible ambient temp.	5°C to 40 °C
Bath opening WxD/BD	130 x 100 / 155mm
Bath volume	5 Liters
Filling volume minimum	3.2 litres
Power supply	230V 1~ 50/60Hz
Current max.	14A
Fusing	16A
Vacuum Power by Agilent
Agilent DS302 8.2 CFM
Pump Type	Oil, Rotary Vane
Pumping Speed	8.2 CFM
Ultimate Pressure	2 × 10-3 mbar
Power	120V / 1ph (220V available)
Intake Connection	KF-25
Dimensions	(L x W x H) 19.33” x 5.27” x 8.34”
Weight	53 lbs
Vacuum Gauges, Connection Hardware included
KIRK-1 FEATURES
● Auto Off
● On/Off soft switch
● Battery level indication
● Good/Bad sensor (tube) indication
● Self test mode
● Field replaceable sensor
● 3 different graphical displays of vacuum pressure (pump-down, line, or bar graph)
● Vacuum analytics for leak, outgassing and pump-down
Unit Size
• Length	28″
• Width	83″
• Height	83″
KIT A Equipment
Huber Minichiller 600 OLÉ General Information & Temperature Controller
Temperature Range	-20°C to 40°C
Temperature Stability	±0,5°C
Temperature Display	OLED Display
Display Resolution	0.1°C
Alarm Message	optical, acoustical
Controller	OLÉ
Safety Class	I / NFL
Protection Class	IP20
Dimensions	(W x D x H) 280 x 490 x 424 mm
Weight	35 kg
Heating / Cooling Capacity
Cooling Capacity	15 0 -10 -20 °C 0.6 0.5 0.35 0.15 kW
Cooling	machine air-cooled
Refrigerant	R290 (0,085 kg)
Circulation Pump
Pressure Pump Max.	24 l/min ; 0,7 bar
Suction Pump Max.	18 l/min ; 0,4 bar
Pump Connection	M16x1 AG male
Connections
Digital Interface	USB, RS232
Operating Data
Permissible Ambient Temp.	5°C to 40°C
Noise Level	63 dB(A)
Filling Volume Min.	2.8 Liters
Volume of Expansion	2.2 Liters
Power Supply	230V 1~ 50/60Hz
Current max.	4 A
Huber TC100
Temperature Range	-100°C to 40°C
Controller	ON-OFF-Regler
Safety Class	I / NFL
Dimensions	(W x D x H) 295 x 500 x 570 mm
Weight	61 kg
Heating / Cooling Capacity
Cooling Capacity	0 -20 -50 -60 -80 -90 -100 °C 0.16 0.15 0.13 0.12 0.12 0.07 0.01 kW
Cooling	machine air-cooled
Refrigerant 1. Stage	R1270 (0,114 kg)
Refrigerant 2. Stage	R1150
Operating Data
Permissible Ambient Temp.	5°C to 40°C
Power Supply	230V 1~ 50/60Hz
Current Max.	6.5 A

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