Meta Purification
2 Neck Offset Round Heavy Wall Bottom Flask - USA Made
2 Neck Offset Round Bottom Heavy Wall Flask This USA made 2 Neck Offest flask is designed specifically for Short Path Distillation units and offsets the distillation head and cow so there is more clearance from the heating mantle. These flasks are made of heavy walled borosilicate and both have a 24/40 Female joint at a 20° Angle perfect for a heating mantle probe. Specifications Material Heavy Wall Borosilicate Sizes Available: 2000ml - 24/40 Joints 5000ml - 24/40 20° Angled Joint and 34/45 Offset Joint 10000ml - 24/40 20° Angled Joint and 45/50 Center Joint MADE in the USA *Notice to customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. **Glassware Safety Disclaimer: BVV™ is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.**
$200.00 - $1,100.00
2L Standard Short Path Distillation Turnkey Setup
2L Standard Short Path Distillation Turnkey Setup The Standard Distillation Turnkey Setup includes all the components necessary to successfully perform distillation at an entry-level price point. Crossbar pictured is not included. We recommend purchasing multiple lab stands to accommodate your specific needs. The Standard Turnkey Setup Includes: 2L Distillation Kit 1/4" Flare x 1/4" Barb Adapter BVV™ 5L Heated Circulator BVV™ V9D 9CFM Two Stage Vacuum Pump High quality and durable Borosilicate 3.3 glass Vacuum-jacketed distillation adapter 3-way cow adapter, accommodating up to 3 pcs of 500mL flasks GCT-01 cold trap guarding from damage of vapors Kangaroo Traceable Digital Thermometer Flexible Gum Rubber Vacuum Tubing and Silicone Tubing for Flow Distillation Quick Start Guide This guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs, Before beginning distillation, ensure the following steps have been taken: Vacuum Pump is in good working order. The pump should be run against the dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed. All glass components are in good working order and ready to be assembled A winterization and degassing procedure has been done to prepare oil for distillation The unit's max internal temperature cannot exceed 380C. The recommended max set temperature should not exceed 250C Once all three of these steps have been completed, you are ready to begin distilling. Begin by placing stir bar in boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer. Assemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware Attach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation. Connect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system. Connect receiving cow to cold trap. Connect cold trap to manifold. Connect vacuum gauge to manifold. At this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process. Turn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability. Start stir slower and increase speed with temperature. Once you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C. You will see your first fraction somewhere between 180C and 190C or slightly before. This is the “heads” fraction. You will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to “self-clean” the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your “main body” fraction. You will see temps between 190-220C during this fraction. Continue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed. The final “tails” fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The “tails” fraction has an obvious color change and will be darker than the “main body” fraction. You will see temps between 200-250C during this fraction. As fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well. Once the process is complete, stop heat, stop stir, and stop vacuum. Let the atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation. ***Note: This entire setup will ship via motor freight.*** *Notice to Customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. BVV™ is not responsible for the failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail, which can cause bodily harm or damage to the surrounding area.
$2,600.00
Variety Pack - Small - 24ct - Rosin Filter Bags
"DISCLAIMER: This unit is intended for LEGAL purposes only, to be used in accordance with local laws and ordinances Rosin Filter Bag Variety Pack Improve your yields with our Rosin Bags!- With no bag, product flattens and spreads out as it's squeezed- Our bags will keep your product packed tightly together and provide higher PSI- Our Rosin Filter Bags are made from woven, sewn Nylon: our weave pattern offers superior strength to help prevent blowouts.- Easy use: Simply pick up and toss bag when done. No need to manually separate material and product.- Safe: We use sewn bags, not glued. No messy glue residue to worry about! This is a variety sample pack of our Rosin Filter Bags. Each pack contains a total count of 24 mesh bags, in 8 different sizes:- (3) 25μm mesh bags, 2.5"" x 3.25""- (3) 45μm mesh bags, 2.5"" x 3.25""- (3) 73μm mesh bags, 2.5"" x 3.25""- (3) 90μm mesh bags, 2.5"" x 3.25""- (3) 120μm mesh bags, 2.5"" x 3.25""- (3) 160μm mesh bags, 2.5"" x 3.25""- (3) 190μm mesh bags, 2.5"" x 3.25""- (3) 220μm mesh bags, 2.5"" x 3.25"" "
$20.00
1L Distillation Kit
1L Distillation Kit The 1L Distillation Kit is a simple, easy to use system designed for small personal use. It includes all stands, clamps, clips, and tubing needed to begin distilling immediately. This Kit Does NOT include a vacuum pump or circulator. Please see the below recommendations for both as well as recommended add-ons. Or check out our 1L Standard Distillation Turnkey Setup which includes vacuum pump and circulator. Recommended Vacuum Pumps: Pro Series 5.6CFM Corrosion Resistant Two Stage Vacuum Pump (premium option) Just Better 6 CFM 2 Stage Deep Vacuum Pump (USA made economy option) Best Value Vacs VE280 9CFM Two Stage Vacuum Pump (economy option) Recommended Circulator: Polyscience 7 Liter MX Heated Circulator (economy option) Polyscience 7 Liter MX Refrigerated Circulator (premium option with chilling capability) Recommended Add-Ons: Glass Dewar Style Cold Trap (recommended cold trap) Bullseye Precison Vacuum Gauge (premium vacuum gauge for measuring depth) CT40 or CT80 Electronic Cold Trap (electronic cold trap, dry ice replacement) Specifications: Boiling Flask Size: 1L Receveiving Flask Size: 250ml Batch Capacity approximate: 200-400 grams Run time: 4 to 8 hours dependent upon material composition and throughput Distillation Temperature Range: 140-250C (Do not exceed 250C) Recommended Condenser Temperature: 40-50C This Kit Includes: Glass Components: 1L 2-Neck Boiling Flask Short Path Head Triple Neck Cow Receiving Flask 3x 250ml Single Neck Round Bottom Flask 14/20 Thermometer Adapter 24/40 Thermometer Adapter 120mm Glass Funnel 14/20 Stopper 24/40 Stopper Accessories: Magnetic PTFE Stirring Bar Retriever 5 Pack of Metal Keck Clips Dow Corning High Vacuum Silicone Grease Tripod Stand 1L Analog Heating and Stirring Mantle 3 Finger Clamp Adjustable 0-70mm Boss Head -13mm 6" x 6" Scissor Jack 250-500ml Cork Stand 10ft of Vacuum Hose 10ft of Chiller Hose 1/4" Vacuum Manifold Traceable Kangaroo Thermometer - Digital 10 Pack of Adjustable Stainless Steel Tubing Clamps Fiberglass Insulation Rope 10 Feet 1.5 Gallon Cold Trap (2QT Tank) Dry Ice, Liquid Nitrogen w/ 2x 1/4" Barb Adapters Distillation Quick Start Guide This guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs, Before beginning distillation, ensure the following steps have been taken: Vacuum Pump is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed. All glass components are in good working order and ready to be assembled A winterization and degassing procedure has been done to prepare oil for distillation Once all three of these steps have been completed, you are ready to begin distilling. Begin by placing stir bar in boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer. Assemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware Attach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation. Connect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system. Connect receiving cow to cold trap. Connect cold trap to manifold. Connect vacuum gauge to manifold. At this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process. Turn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability. Start stir slower and increase speed with temperature. Once you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C. You will see your first fraction somewhere between 180C and 190C or slightly before. This is the “heads” fraction. You will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to “self-clean” the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your “main body” fraction. You will see temps between 190-220C during this fraction. Continue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed. The final “tails” fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The “tails” fraction has an obvious color change and will be darker than the “main body” fraction. You will see temps between 200-250C during this fraction. As fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well. Once process is complete, stop heat, stop stir, and stop vacuum. Let atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation. *Notice to Customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. BVV™ is not responsible for the failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail, which can cause bodily harm or damage to the surrounding area.
$1,000.00
20L Collection Base
The 20 Liter Collection Base allows for vacuum assistance during filtration. It works most efficiently when paired with the Refinement Filter but can be used as a standalone unit. It includes a dedicated vacuum valve and deidcated liquid dip tube valve which allows for direct injection into a rotovap. Key Features: Stainless steel design for greater thermal conductivity and improved lifespan Easy to clean and disassemble with Tri-Clamp stainless steel parts Collection vessel for vacuum and storage of material Liquid dip tube for direct injection into rotary evaporator after filling Key Specifications: 20 Liter Collection Base (12"x12" Welded Bottom Spool w/ 12" Lid) Dedicated Vacuum Valve Dedicated Dip Tube Valve Silicone gaskets with high alcohol resistance 1/4" and (2)3/8" Stainless steel barb connections Polycarbonate sights for easy viewing
$850.00
BVV™ 5L Digital Heating Mantle Probe
BVV™ 5L Digital Heating Mantle Probe This is a replacement probe for the BVV™ 5L Digital Heating Mantle. the probe measures 15.5" in length with an overall length of 60.5"
$98.00
Distillation Head
BVV™ Distillation Head BVV™ Brand Distillation head is made out of 3.3 Boro and comes with (2) 24/40 Ground Male Joints and a 14/20 Female thermometer joint at the top of the head. This head features 2x GL-14 barbs for the condenser and an extended drip tip for the receiving cow. The head measures 8.5" from the bottom 24/40 joint to the top of the head and the condenser is 3.5" long. The head has 2 sets of quad Vigreux and is bent at a 20-degree angle. *Notice to customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. **Glassware Safety Disclaimer: BVV™ is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.**
$200.00
Porcelain Buchner Funnel Kit
This porcelain buchner funnel kit includes a 3.3 borosilicate non-jointed conical flask with side port hose barb, porcelain buchner funnel in either 1000 or 2000ml and a 9 piece rubber cones set to create the seal between the flask and the funnel. Each kits includes the following: 1000ML: (1) - 1000ml Porcelain Buchner Funnel (1) - 2500ml Conical Flask Filtering with Internal Side Arm (1) - Rubber Cones Set of 9 2000ML: (1) - 2000ml Porcelain Buchner Funnel (1) - 5000ml Conical Flask Filtering with Internal Side Arm (1) - Rubber Cones Set of 9
$125.00 - $140.00
Valved Vacuum Adapter 2.0 - Made in USA
Valved Vacuum Adapter 2.0 This Valved Vacuum Adapter allows the user to isolate the vacuum in a short path distillation system from the cow or receiving flasks of the system to allow the easy swap of the flasks and allows for a full bore vapor flow. These adapters have a 24/40 male joint having a grease-less Viton O-ring seal which reduces the grease mess for each fraction. It also includes GL-14 Cap for venting vacuum and also comes with a PTFE threaded valve with Viton Seals. Sizes: 24/40 Joint - All 3 Joints are 24/40 with GL-14 Cap 34/45 Joint - 2 34/45 Joints and 24/40 lower O-ring Joint with GL-14 Cap *Notice to customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. **Glassware Safety Disclaimer: BVV™ is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.**
$450.00
475L Centrifuge Bags
This nylon bag is designed to fit in our BVV brand centrifuges to contain material and be easily swappable after runs to speed up processing times. These bags come with 2 zippers and come in 1, 10, 50, 100, and 200 micron filtration levels. For use with 475L Centrifuges Appx. Size : 47.25" Diameter x 16.75" Height Specifications SKU Appx. Diameter In. Appx. Height in. CFB-45L-XXX 17.5" 11.75" CFB-160L-XXX 32.25" 13" CFB-280L-XXX 39.25" 14" CFB-475L-XXX 47.25" 16.75"
$245.00 - $499.00
Cold Trap 2" Stainless Steel
Cold Trap 2" Stainless Steel This Stainless Steel Cold is designed and intended for use with the Polyscience IP60 Cold Finger (Can also be used with dry Ice) to create a cold trap that can achieve extremely frigid temperatures. These cold traps have 2 1/4" FNPT ports with one having a dip tube to the bottom of the trap to achieve higher vapor condensing rates with the 2" Diameter Center opening for the IP60. This Cold trap also has an insulating vacuum jacket around the entire container to maintain the subzero temperatures and help achieve the maximum minimal temperature of the IP60. Unlike many cold Traps on the market, this one is also made out of 304 Stainless steel and the internal parts are resistant to most chemicals and easily cleaned due to the Tri-Clamp lid design. Specifications Material 304 Stainless Steel Temperature Rating -200 to 200°C Ultimate Vacuum <100millitorr / microns Cold Finger Internal Dimensions 1.85" x 11.75" (Fits Polyscience IP60) Trap Internal Dimensions 5.85" x 10" Outside Dimensions 8" x 14" x 15" (Includes jacket gauge and valve hardware) Weight 28LBS
$465.00 - $508.00
Certified Jacketed Diamond Miner
Certified Jacketed Diamond Miner Introducing BVV's Certified Jacketed Diamond Miner, peer review by PRV Engineers, the ultimate tool for precise and efficient crystallization procedures. Take control of your crystallization process like never before with our Certifed Jacketed Diamond Miner. Designed to accelerate crystal growth, this miner allows for precise heating or cooling through its jacketed base, ensuring optimal conditions for crystal formation. Our Certified Jacketed Diamond miner comes fully loaded with all the features you could ask for in a diamond miner including 2X 1/4" JIC Lid Valves, 1X 1/2" JIC Lid Valves for exceptional versatility, 2X Certified Borosilicate Sight Glasses for optimized process viewing, 1X -30hg-250PSI Compound Pressure Gauge for precise process monitoring, and 1X 100 PSI ASME Safety Valve for insured safety and peace of mind. With the capability to maintain precise temperature control, you can achieve consistent and high-quality crystals for a wide range of applications. Whether you're looking to produce large crystals or control the size and shape of your crystal output, our Jacketed Diamond Miner provides the flexibility and accuracy you need to meet your specific requirements. Upgrade your crystallization process into compliance today and elevate the quality, and efficiency of your crystal production with BVV's Certified Jacketed Diamond Miner. *Certified versions require infield verification by PRV engineers to ensure compliance prior to certification being issued. Certification includes Jurisdiction specific peer review document, Field inspection letter for the unit, & a field certificate approving its use.* Specifications: 2X Certified Borosilicate Sight Glasses (FJDM-6: 1.5"/FJDM-12: 2") 1X 100 PSI ASME Safety Valves 1X -30hg-250PSI Compound Pressure Gauge 2X 1/4" JIC Lid Valves 1X 1/2" JIC Lid Valve with 1X 1/2" JIC Cap for Seeding 2X 1/2" Barb Jacket Valves Available Size/Type: 6"Non-Certified 12"Non-Certified 6" Infield Certified 12"Infield Certified
$950.00 - $2,180.00
Bullseye Precision Gauge | Portable Vacuum Gauge | .001 to 2 Torr Accuracy
Bullseye Precision Gauge | Portable Vacuum Gauge | .001 to 2 Torr Accuracy The Bullseye Precision Gauge is the ideal portable vacuum gauge to serve many applications. This patented vacuum gauge offers Graphical Displays and graphics supporting real-time analytics (Leak, Pump, Outgas, Stable) Visual graphing feature right on the display Display pinpoints the root of the problem so you get it right the first time Put it anywhere with its magnet and kickstand Options: Rugged carrying case designed for instrument, back-up sensor and these adapters that can change the NPT to a KF25 or KF16 vacuum interface adapters Sensor (Probe) Replacements: This gauge is paired with the Thermocouple Plus/531 Equivalent Sensor, but works with Agilent 531 or 536 sensors as well if you are looking for a more robust sensor option Numeric & Graphical Displays See vacuum readings in either numbers or easy-to-read graphs Calibrated & Precise Delivered pretested and calibrated with thermocouple sensor under actual vacuum against a NIST standard. Extended Battery Lifespan Solid state electronics are built into the Bullseye Precision Gauge. The portable vacuum gauge operates using AA batteries and lasts 70 hours. Applications Vacuum pump monitoring, vacuum pump testing, baseline vacuum pump performance, & transformer dry-out, distillation monitoring Bullseye Precision Gauge Accuracy Remember to choose your vacuum gauge that gives you the accuracy you need for your application. This Bullseye comes with a thermocouple sensor, which has better accuracy in the millitorr up to 6 Torr. If you need your Bullseye Gauge to have CE rating then choose either the Bullseye with 531 or Bullseye with 536 KF25 1 to 99 millitorr +/- 2 millitorr or 20% 100 to 2000 millitorr +/- 10% 2 to 6 Torr +/- 25% Above 6 Torr Continuous and monotonic (increasing reading indicates increasing pressure) Units Torr, mbar, bar, kPa, inHg, mm Hg, millitorr, microns, inches of water, PSI, Pa Control Range 1E-4 – 1000 Torr Range with Accuracy .001 – 5 Torr Sensor Type SEN-VGT500, Thermocouple Plus Dimensions 6.2”H x 3.7”W x 1.3”D Certifications ROHS and CE
$543.25$530.00
Analog Heating and Stirring Mantle
Analog Heating and Stirring Mantle is used to heat up a glass round bottom flask and stir the contents inside. Heating and stirring functions are analog and sizes range from 500ml to 2000ml. (Mantle's are tested in house and may show slight discoloration on the heating surface.) Certifications: CE Approval Warranties: 500ml - 30 Day Limited Warranty 1000/2000ml - 90 Day Limited Warranty.
$135.00 - $175.00
Glass Cold Trap - Ribbed (Made in USA)
BVV™ Glass Cold Trap - Ribbed This dewar style glass is designed to increase surface area for maximum vapor condensation and it also has 24/40 or 34/45 jointed connections to increase vapor flow. Note: The bottom joint will always be 24/40. *Notice to customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement.
$500.00
4" Stainless Steel Buchner Funnel
4 Inch Stainless Steel Buchner Funnel 4” Buchner Funnel Kit: This buchner funnel kit adapts to any vessel with a 24/40 joint. The included adapter makes it possible to pull vacuum and use large vessels as a collection. Max internal volume of the buchner funnel is 0.82L, but can be adapted with a larger spool for higher capacity. This kit features: 4” x 4” 304SS spool with a capacity of 0.82L 4” Tri-Clamp Single Hinge Clamp 4”x1.5” 304SS Hemispherical Reducer 1.5” Tri-Clamp Double Hinged Clamp 4” 5 Micron 304SS Sintered Disc Filter 4” 304SS Filter Plate V2 1.5”x24/40 304SS Adapter 24/40 Glass Inlet Straight Adapter with hose connection Recommended items: 110MM sized filter paper, 24/40 jointed glass conical flask. For additional information or questions regarding this kit contact our customer support line.
$370.00
5L Premium Short Path Distillation Turnkey Setup
5L Premium Distillation Kit This unit carries a 2 day lead time. The 5L Premium Short Path Distillation Turnkey Setup features our 5L Distillation Kit with P5 Distillation Head and USA made glass. Every component in this turnkey is made for precision, throughput, and repeatable results. Also included is our Pro Series 11.3CFM Corrosion Resistant Two Stage Vacuum Pump giving you extreme power and depth with a long lifespan, the Bullseye Precision Vacuum Gauge from Digivac which is the most rugged and dependable vacuum gauge on the market, and a BVV 19L Heated Circulator for maximum condensation of vapors. You will also receive a Dewar Style Glass Cold Trap to keep all volatiles and solvents out of your vacuum system. This Turnkey Setup gives you everything needed to perform distillation at the highest level. The Premium Short Path Distillation Turnkey Kit Includes: 5L Distillation Kit with P5 Distillation Head KF-25 x 1/4" Barb Adapter Dewar Style Glass Cold Trap Bullseye Precision Vacuum Gauge Polyscience 7L MX Heated Circulator Pro Series 14.1CFM Corrosion Resistant Two Stage Vacuum Pump Short Path Distillation Quick Start Guide This guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs, Before beginning distillation, ensure the following steps have been taken: Vacuum Pump is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed. All glass components are in good working order and ready to be assembled A winterization and degassing procedure has been done to prepare oil for distillation Once all three of these steps have been completed, you are ready to begin distilling. Begin by placing stir bar in boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer. Assemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware Attach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation. Connect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system. Connect receiving cow to cold trap. Connect cold trap to manifold. Connect vacuum gauge to manifold. At this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process. Turn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability. Start stir slower and increase speed with temperature. Once you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C. You will see your first fraction somewhere between 180C and 190C or slightly before. This is the “heads” fraction. You will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to “self-clean” the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your “main body” fraction. You will see temps between 190-220C during this fraction. Continue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed. The final “tails” fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The “tails” fraction has an obvious color change and will be darker than the “main body” fraction. You will see temps between 200-250C during this fraction. As fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well. Once the process is complete, stop heat, stop stir, and stop vacuum. Let atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation. ***Note: This entire setup will ship via motor freight.*** ***Note: All units are inspected for broken glass or parts before unit is shipped. If unit arrives damaged or glass is broken (this does not include minor imperfections or scuffs in glassware), Customer MUST contact BVV™ within 3 days of delivery to file a claim and receive a replacement part. If customer DOES NOT contact BVV™ within 3 days of delivery responsibility for replacement parts falls on the customer and they must pay for replacement pieces.*** ***Glassware Safety Disclaimer: BVV™ is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.***
$5,500.00
Pressure Filtration System - 6 x 28
This filter system is designed for high flow rates to filter unwanted precipitates from your oleoresin. The housing provides full enclosure of your filter bags, which are fully supported by the strainer basket within the housing to prevent blowouts. Pressure and high flow rates may be applied to get the fastest flow through filter bags. Using the housing allows full exhaustion of a bag prior to changing it without the sacrifice in filtering time.These filter bag housings use an eye-bolt clamp style to allow for high pressure without leakage, while still maintaining an easy to remove cover. When one filter bag gets filled, it can easily be swapped out by removing the lid while not under pressure and pulling the old bag out. The main seal on the housing is Buna-n rubber. The liquid pump is of 316 Stainless Steel Construction with PTFE seals and runs on compressed air or nitrogen. Built options Include: 1x 304 Stainless Steel Filter Bag Housing 1x 304 Stainless Steel Basket 1x 304 Stainless Steel Displacement Cylinder With Pump options Include: 1x 304 Stainless Steel Filter Bag Housing 1x 304 Stainless Steel Basket 1x 304 Stainless Steel Displacement Cylinder 1x 316 Stainless Steel Liquid pump Connecting hose or hardline tubing 4x Nomex Filter Bags (1μm, 5μm, 25μm, and 100μm) Specifications PFS-790-15 PFS-790-45 Flow Rate (GPM) ≤15 ≤45 Max Pressure (PSI) 100 @28 CFM Volume (in^3) 790 Working Temperature (°C) -40 - 100 Air Hose Connection ¼” JIC Flare ½” JIC Flare Filter Bag Housing Dimensions (LxWxH) 14” x 11” x 41” Filter Bag Trade Size #8 Included PVC Hose size ID ¾” 1” *This unit requires an air compressor for operation (not included)
$850.00 - $10,000.00
AFS 4" Tri-Clamp Inline Filter Housing for Disposable Color Remediation Cartridges
AFS Tri-Clamp Inline Filter Housing for Disposable Color Remediation Cartridges Note: Disposable cartridges sold separately. (Click Here for Cartridges) This inline housing allows for implementation of the AFS filters into many extraction systems. The AFS filter housing is 4" but comes with the adapter flanges for both ends to go inline with a standard 2" tri-clamp system. Kit Includes 2x 4" High Pressure Clamps 1x 4" Buna-N Gasket 2x Flat Reducers 4" to 2" Tri-Clamp 1x Cartridge Housing AFS Instruction Manual Download Here AFS SDS Sheet
$199.00$165.00
2L Short Path Distillation Kit
Short Path Distillation Setup Short path distillation is used for compounds that are not stable at high temperatures. It can also be used to purify small amounts of a compound. For those new to this type of distillation, our Short Path Kit includes everything you will need as you get started. All stands, clamps, clips, and tubing are included, which means it’s ready to start working straight out of the box. The cold trap, cow and vacuum grease can all be customized to meet your needs. The 2L Distillation Kit builds upon the same principal as the 1L Distillation Kit, giving users an easy to use system that will get them up and running at an affordable price. It includes all stands, clamps, clips, and tubing needed to begin distilling immediately. This Kit Does NOT include a vacuum pump or circulator. Please see the below recommendations for both as well as recommended add-ons. Or check out our 2L Standard Distillation Turnkey Setup which includes vacuum pump and circulator. Crossbar pictured is not included. We recommend purchasing multiple lab stands to accommodate your specific needs. Recommended Vacuum Pumps: Pro Series 5.6CFM Corrosion Resistant Two Stage Vacuum Pump (recommended option) Just Better 6 CFM 2 Stage Deep Vacuum Pump (economy option) Best Value Vacs VE280 9CFM Two Stage Vacuum Pump (economy option) Recommended Circulators: Polyscience 7 Liter MX Heated Circulator (economy option) Polyscience 7 Liter MX Refrigerated Circulator (premium option with chilling capability) Recommended Add-Ons: Glass Dewar Style Cold Trap (recommended cold trap) Bullseye Precison Vacuum Gauge (premium vacuum gauge for measuring depth) CT40 or CT80 Electronic Cold Trap (electronic cold trap, dry ice replacement) Short Path Distillation Kit Specifications: Boiling Flask Size: 2L Recieving Flask Size: 250ml Batch Capacity approximate: 2L = 400-1000 grams Run time: 4 to 8 hours dependent upon material composition and throughput Distillation Temperature Range: 140-250C (Do not exceed 250C) Recommended Condenser Temperature: 40-50C This Kit Comes Standard With The Following: Glass Components: 2L 2-Neck Boiling Flask Short Path Head Triple Neck Cow 3x 250mL Single Neck Receiving Flask 1/8" 14/20 PTFE Thermometer Adapter 1/4" 24/40 PTFE Thermometer Adapter 120mm Glass Funnel Accessories: Magnetic PTFE Stirring Bar Retriever 5 Pack of Metal Keck Clips Dow Corning High Vacuum Silicone Grease Tripod Stand 2L Digital Heating and Stirring Mantle 3 Finger Clamp Adjustable 0-70mm 6" x 6" Scissor Jack 250-500ml Cork Stand 10ft of Vacuum Hose 10ft of Chiller Hose 1/4" Vacuum Manifold Traceable Kangaroo Thermometer - Digital 10 Pack of Adjustable Stainless Steel Tubing Clamps Fiberglass Insulation Rope 10 Feet 1.5 Gallon Cold Trap (2QT Tank) Dry Ice, Liquid Nitrogen w/ 2x 1/4" Barb Adapters Distillation Quick Start Guide This guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs. Before beginning distillation, ensure the following steps have been taken: Vacuum Pump is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed. All glass components are in good working order and ready to be assembled A winterization and degassing procedure has been done to prepare oil for distillation The unit's max internal temperature cannot exceed 380C. The recommended max set temperature should not exceed 250C Once all three of these steps have been completed, you are ready to begin distilling. Begin by placing stir bar in boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer. Assemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware Attach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation. Connect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system. Connect receiving cow to cold trap. Connect cold trap to manifold. Connect vacuum gauge to manifold. At this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process. Turn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability. Start stir slower and increase speed with temperature. Once you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C. You will see your first fraction somewhere between 180C and 190C or slightly before. This is the “heads” fraction. You will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to “self-clean” the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your “main body” fraction. You will see temps between 190-220C during this fraction. Continue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed. The final “tails” fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The “tails” fraction has an obvious color change and will be darker than the “main body” fraction. You will see temps between 200-250C during this fraction. As fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well. Once process is complete, stop heat, stop stir, and stop vacuum. Let atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation. Learn more about short path distillation components and FAQs with this distillation guide. *Notice to Customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. BVV™ is not responsible for the failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail, which can cause bodily harm or damage to the surrounding area.
$1,275.00
Replacement Gasket for Dutch Weave Sintered Filter Disks - Silicone
Replacement Gasket for Dutch Weave Sintered Filter Disks This is a replacement Silicone gasket for dutch weave sintered filter disks.
$8.00 - $20.00
5 Gallon Refinement Filter
The BVV™ 5 Gallon Refinement Filter is a stainless steel filtration system that provides large scale, high flow filtering, with greatly improved functionality compared to a traditional Buchner filter. Utilizing a collection base for vacuum assistance and storage of material, the Refinement Filter allows for benchtop filtration with a longer lifespan and ease of use. Key Features: Stainless steel design for greater thermal conductivity and improved lifespan Easy to clean and disassemble with Tri-Clamp stainless steel parts Small tabletop footprint with wide mouth design Secondary collection vessel for vacuum and storage of material Liquid dip tube for direct injection into rotary evaporator after filling Key Specifications: Large 6" Diameter x 12" Long Dewaxing Column 20 Liter Collection Base 5 micron Sintered Stainless Steel Filter Disc 100 Pack of 6" Ashless Filter Paper (BIO-1-180) Dedicated 3/8" Vacuum Valve Dedicated 3/8" Dip Tube Valve Silicone gaskets with high alcohol resistance 3/8" Stainless steel hose barb connections Polycarbonate sights for easy viewing 2" Tri-Clamp Short Sight Glass for Flow Viewing Operation Instructions: Before beginning filtration, place refinement filter in freezer for best thermal conductivity Secure ashless filter paper with filter plate ring Place collection base on floor and connect tubing from refinement filter to to a vacuum pump Attach vacuum system to the dedicated vacuum valve Begin to pour solution into filter Close dedicated dip tube valve and start vacuum Once solution has been completely filtered, stop vacuum system and disconnect from dedicated vacuum valve Connect dedicated dip tube valve to injection valve on rotovap Begin rotovap procedure Open dedicated dip tube valve and begin injecting filtered solution into rotovap
$1,500.00
Diamond Sauce Separator for 1.9 ft³ Ovens and Larger
BVV Diamond Sauce Separator The BVV diamond sauce separator is a good compliment to any diamond miner. With this vessel you can easily strain and separate your diamonds from the sauce using the internal basket. You can clean your diamonds like never before with less work. DSS-9 12.25" Exact Height (Fits 1.9 ft³ Vacuum Ovens) 6" Deep Basket (100 micron mesh Dutch Weave) 3"x9" Main Body Spool DSS-12 15.25" Exact Height (Fits larger than 1.9 ft³ Vacuum Ovens) 9" Deep Basket (100 micron mesh Dutch Weave) 3"x12" Main Body Spool Replacement Top Gasket around the basket can be found Here.
$160.00 - $180.00
160L Centrifuge Bags
This nylon bag is designed to fit in our BVV brand centrifuges to contain material and be easily swappable after runs to speed up processing times. These bags come with 2 zippers and come in 1, 10, 50, 100, and 200 micron filtration levels. For use with 160L Centrifuges Appx. Size : 31.25" Diameter x 13" Height Specifications SKU Appx. Diameter In. Appx. Height in. CFB-45L-XXX 17.5" 11.75" CFB-160L-XXX 32.25" 13" CFB-280L-XXX 39.25" 14" CFB-475L-XXX 47.25" 16.75"
$187.00 - $350.00
Dewar Glass Cold Trap
BVV™ Dewar Glass Cold Trap This dewar style glass is designed for maximum vapor condensation and it also has a 24/40 bottom joint and (2) GL-14 8mm Hose Barbs *Notice to customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement.
$250.00$210.00
10L Digital Heating and Stirring Mantle
10L Digital Heating and Stirring Mantle Digital Heating and Stirring Mantles give the operator the most precise temperatures and readouts during distillations. These mantles autotune to specific user input to provide consistent results. Each mantle is equipped with large digital display that will give you readouts for both set temperature, actual temperature, and stirring speed. Each mantle also comes with a vertical brace bar and boss head as well as a temperature probe which plugs directly into the mantle. For first time use, the mantle should have an initial burn out done. This will burn off any residual oils used in the production of the insulation rope. The unit's max internal temperature cannot exceed 380C. The recommended max set temperature should not exceed 250C Specifications Capacity: 10L (10000mL) Power Supply: 220V 60Hz Adjustable Rotation Speed: 50-1800 RPM Motor Power: 40W, DC14-24V Heating Power 180-2200W Temperature Control Accuracy: +/- 1C Intelligent Temperature Control: Yes Temperature Range: RT+10-380C Insulation Material: Alkali-free Glass Fiber, temperature resistant up to 450C Shipping Dimensions: 23 x 23 x 16 in. Weight: 20 lbs
$1,150.00
P5V6 Neocision Distillation Head - USA Made
P5V6 Distillation Head P5V6 Distillation Head has 6 sets of vigreux in the distillation column with 34/45 lower joint and 24/40 upper and side joints and includes GL-14 barb connections. MADE IN THE USA Designed for 5 Liter Flasks Set of 6 vigreux to allow for packing media Larger vacuum jacket allows for less heat loss during distillations Larger vapor path to allow for gas/vapor phase flow Increased internal diameter for faster, more efficient fractioning as well as packing and unpacking of media Increased condenser length and diameter for more efficient condensation of vapor with zero clogging *Notice to customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. **Glassware Safety Disclaimer: BVV™ is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.**
$550.00
20L Digital Heating Mantle
20L DIGITAL HEATING AND STIRRING MANTLE Digital Heating and Stirring Mantles give the operator the most precise temperatures and readouts during distillations. These mantles autotune to specific user input to provide consistent results. Each mantle is equipped with large digital display that will give you readouts for both set temperature, actual temperature, and stirring speed. Each mantle also comes with a vertical brace bar and boss head as well as a temperature probe which plugs directly into the mantle. For first time use, the mantle should have an initial burn out done. This will burn off any residual oils used in the production of the insulation rope. The unit's max internal temperature cannot exceed 380C. The recommended max set temperature should not exceed 250C Specifications: Capacity: 20L (20000mL) Power Supply: 220V 60Hz (NEMA 6-20 plug) Adjustable Rotation Speed: 50-1800 RPM Motor Power: 40W, DC14-24V Heating Power 180-2200W Temperature Control Accuracy: +/- 1C Intelligent Temperature Control: Yes Temperature Range: RT+10-380C Insulation Material: Alkali-free Glass Fiber, temperature resistant up to 450C Shipping Dimensions: 25 x 25 x 18 in. Weight: 35 lbs
$1,200.00
Diamond Sauce Separator Basket Dutch Weave 100 Micron
BVV Diamond Sauce Separator Baskets for your Diamond Sauce Separator sold "A la Carte" The 6" long basket fit the BVV DSS-9 The 8.25" long basket fit the BVV DSS-12 The basket is a Dutch Weave all 304 Stainless Steel basket, and fits inside a 3" tri-clamp spool. The lip perfectly fits the tri clamp flange and works with our Dutch Weave product line gaskets.
$21.00 - $26.00
2L Short Path Distillation Kit with P2 Distillation Head
2L Short Path Distillation Kit with P2 Distillation Head The 2L Distillation Kit w/ P2 Distillation Head includes everything needed to perform distillation excluding the vacuum pump and chiller. This kit features our USA made P2 Distillation Head as well as USA made glass. It is designed with ease of use in mind and includes the highest quality components to ensure results are repeatable time and again. **This Kit Does NOT include a vacuum pump or circulator. Please see the below recommendations for both as well as recommended add-ons. Or check out our 2L Premium Turnkey Setup which includes vacuum pump and circulator.** Crossbar pictured is not included. We recommend purchasing multiple lab stands to accomodate your specific needs. Recommended Vacuum Pumps: Pro Series 5.6CFM Corrosion Resistant Two Stage Vacuum Pump (recommended option) Just Better 6 CFM 2 Stage Deep Vacuum Pump (USA made economy option) Welch 1400 DuoSeal 0.9 cfm 0.1 Micron Belt Drive Dual-Stage Pump Recommended Circulators: Polyscience 7 Liter MX Heated Circulator (economy option) Polyscience 7 Liter MX Refrigerated Circulator (premium option with chilling capability) Recommended Add-Ons: Glass Dewar Style Cold Trap (recommended cold trap) Bullseye Precison Vacuum Gauge (premium vacuum gauge for measuring depth) CT40 or CT80 Electronic Cold Trap (electronic cold trap, dry ice replacement) J-KEM Digital Vapor Temp Monitor (digital vapor temp monitor with data-logging capabilities) Specifications: Boiling Flask Size: 2L Receveiving Flask Size: 250mL Batch Capacity approximate: 2L = 400-1000 grams Run time: 4 to 8 hours dependent upon material composition and throughput Distillation Temperature Range: 140-250C (Do not exceed 250C) Recommended Condenser Temperature: 40-50C This Kit Includes: Glass components: 2L USA Made 2-Neck Boiling Flask P2 USA Made Distillation Head Triple Neck Cow 3x 250mL Receiving Flask 2x 24/40 Chemglass Thermometer Inlet Adapter 120mm Glass Funnel Accessories: Magnetic PTFE Stirring Bar Retriever 5 Pack of Metal Keck Clips Dow Corning High Vacuum Silicone Grease Tripod Stand 2L Digital Heating and Stirring Mantle 3 Finger Clamp Adjustable 0-70mm 6" x 6" Scissor Jack 250-500ml Cork Stand 10ft of Vacuum Hose 10ft of Chiller Hose 1/4" Vacuum Manifold Traceable Kangaroo Thermometer - Digital 10 Pack of Adjustable Stainless Steel Tubing Clamps Fiberglass Insulation Rope 10 Feet 1.5 Gallon Cold Trap (2QT Tank) Dry Ice, Liquid Nitrogen w/ 2x 1/4" Barb Adapters Distillation Quick Start Guide This guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs, Before beginning distillation, ensure the following steps have been taken: Vacuum Pump is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed. All glass components are in good working order and ready to be assembled A winterization and degassing procedure has been done to prepare oil for distillation The unit's max internal temperature cannot exceed 380C. The recommended max set temperature should not exceed 250C Once all three of these steps have been completed, you are ready to begin distilling. Begin by placing stir bar in boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer. Assemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware Attach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation. Connect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system. Connect receiving cow to cold trap. Connect cold trap to manifold. Connect vacuum gauge to manifold. At this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process. Turn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability. Start stir slower and increase speed with temperature. Once you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C. You will see your first fraction somewhere between 180C and 190C or slightly before. This is the “heads” fraction. You will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to “self-clean” the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your “main body” fraction. You will see temps between 190-220C during this fraction. Continue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed. The final “tails” fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The “tails” fraction has an obvious color change and will be darker than the “main body” fraction. You will see temps between 200-250C during this fraction. As fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well. Once process is complete, stop heat, stop stir, and stop vacuum. Let atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation. *Notice to Customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. BVV™ is not responsible for the failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail, which can cause bodily harm or damage to the surrounding area.
$2,200.00
Steam Distillation Kit
Steam Distillation Steam distillation is the separation of organic compounds at low temperatures by boiling water. It is widely used for essential oils and terpenes because it does not degrade the organic material as a traditional fractional distillation does. Alternatively, steam distillation can extract a diverse array of immiscible substances. You can use steam distillation for “steam stripping” in petroleum refineries and separate commercially important organic compounds, including fatty acids. Our system is composed of a 6-piece glass distillation set up paired with a separatory funnel. Simply fill the boiling flask with water and the material flask with your organic material, then use the heating mantle to boil the water and pass the steam through the material flask. There is a port above the material flask on the U-Tube to insert a thermometer to more closely monitor the process. The steam passing around the material will lower the boiling point on the surface of the plant material and cause the terpenes to boil off at low temperatures. After moving through the U-Tube the steam and terpenes will condense in the graham condenser and drain into the flask below. After filling the flask, simply swap it and drain the contents into the separatory funnel to remove all water. Steam Distillation is beneficial due to the lower boiling point being able to reduce the decomposition of temperature-sensitive compounds. Here’s a look at the key benefits of steam distillation. Key Benefits of Steam Distillation: Streamlined method produces organic solvent-free products Possesses large capacity for processing at the industrial scale Requires no subsequent separation steps Requires less fuel for the steam boiler for extraction of oils Due to its wide application and inexpensive equipment, steam distillation can be a cost-effective investment Kit Includes: 2L Analog Mantle 2L Boiling Flask 2L Material Flask U-Tube 24/40 Thermometer Adapter 24/40 Male Stopper Graham Condenser 500ml Flask 500ml Separatory Funnel BVV™ Lab Stand Three Finger Clamp Boss Head Please Note: for any replacement parts, please contact us. 2L Dual Neck Flask (SKU: STEAM-01-2000ml) 2L Material Flask (SKU: STEAM-02) U-Tube (SKU: STEAM-03) Graham Condenser (SKU: STEAM-04)
$495.00
P2 Distillation Head - USA Made
P2 Distillation Head P2 Packable Distillation Head with 24/40 Joints. Includes GL-14 Barb Connections. Recommended packing media: Raschig Rings, Porcelain Berl Saddles, Glass Beads, Pro-Pak, or Stainless Steel Wool. Key Features: MADE IN THE USA Designed for 1 & 2 Liter Flasks Single set of lowered vigreaux to allow for packing media Larger vacuum jacket allows for less heat loss during distillations Larger vapor path to allow for gas/vapor phase flow Increased internal diameter for faster, more efficient fractioning as well as packing and unpacking of media Increased condenser length and diameter for more efficient condensation of vapor with zero clogging *Notice to customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. **Glassware Safety Disclaimer: BVV™ is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.**
$600.00
Inline Strainer 304 Stainless Steel
Inline Strainer 304 Stainless Steel Inline Tri-Clamp strainers are used when filtering solids from liquids in fluid processing systems. The inside of the strainer is perforated with 2mm holes to collect larger solids when filtering and comes with (1) 3" Single pin clamp and (1) 3" silicone Tri-Clamp gasket. It is recommended that a strainer be placed after a pump, as the suction could damage the strainer core. Specifications Material 304 Stainless Steel Connection Type 1.5" Tri-Clamp Secondary Mesh Perforated Stainless Steel with 2mm Holes
$165.00
Color Remediation Column CRC w/ Bypass
Color Remediation Column w/ Bypass The CRC is a secondary column used as a filtration cartridge for hydrocarbon and ethanol extraction systems. Filter medias are packed in the column above a triple filtration stack, which aids in the removal of impurities from extracted oils. The CRC features a bypass path, allowing the operator to skip the column in case of a clog. The color remediation process is made simple by bundling the cartridge with the needed filter medias. We have paired the unit with suggested media, supplied in the proper ratio, and a standard operating procedure. The included procedure takes all the guesswork out of filtration, delivering the desired results the first try. Our CRC comes available with 1/4",3/8", and 1/2" MJIC connections, your choice of a 3",4", and 6" diameter spool with a 12" height, and rack mounting brackets standard to accommodate systems of any size. This Kit Includes: Color Remediation Column Rack Mounting Brackets 100 pack of 8 and 20-micron filter papers 1000g of Activated Alumina 1000g of Silica 60A 1000g of Pure-Flo® B80 (81, 5000, 6000 or Color Bleach)*Substitutes 1000g of Celite®545 Instruction Manual
$850.00 - $1,350.00
2L Premium Short Path Distillation Turnkey Setup with P2 Distillation Head
2L Premium Short Path Distillation Turnkey Setup with P2 Distillation Head The 2L Premium Distillation Turnkey Setup features our 2L Distillation Kit with P2 Distillation Head and USA made glass. Every component in this turnkey is made for precision, throughput, and repeatable results. Also included is our Pro Series 11.3CFM Corrosion Resistant Two Stage Vacuum Pump giving you extreme power and depth with long lifespan, the Bullseye Precision Vacuum Gauge from Digivac which is the most rugged and dependable vacuum gauge on the market, and a Polyscience 7L MX Heated Circulator for maximum condensation of vapors. You will also receive a Dewar Style Glass Cold Trap to keep all volatiles and solvents out of your vacuum system. This Turnkey Setup gives you everything needed to perform distillation at the highest level. The Premium Turnkey Kit Includes: 2L Distillation Kit w/ P2 Distillation Head KF-25 x 1/4" Barb Adapter Dewar Style Glass Cold Trap Bullseye precision Vacuum Gauge Polyscience 7L MX Heated Circulator Pro Series 14.1CFM Corrosion Resistant Two Stage Vacuum Pump Distillation Quick Start Guide This guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs, Before beginning distillation, ensure the following steps have been taken: Vacuum Pump is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed. All glass components are in good working order and ready to be assembled A winterization and degassing procedure has been done to prepare oil for distillation Once all three of these steps have been completed, you are ready to begin distilling. Begin by placing stir bar in boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer. Assemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware Attach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation. Connect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system. Connect receiving cow to cold trap. Connect cold trap to manifold. Connect vacuum gauge to manifold. At this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process. Turn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability. Start stir slower and increase speed with temperature. Once you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C. You will see your first fraction somewhere between 180C and 190C or slightly before. This is the “heads” fraction. You will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to “self-clean” the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your “main body” fraction. You will see temps between 190-220C during this fraction. Continue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed. The final “tails” fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The “tails” fraction has an obvious color change and will be darker than the “main body” fraction. You will see temps between 200-250C during this fraction. As fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well. Once the process is complete, stop heat, stop stir, and stop vacuum. Let the atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation. ***Note: This entire setup will ship via motor freight.*** ***Note: All units are inspected for broken glass or parts before unit is shipped. If unit arrives damaged or glass is broken (this does not include minor imperfections or scuffs in glassware), Customer MUST contact BVV™ within 3 days of delivery to file a claim and receive a replacement part. If customer DOES NOT contact BVV™ within 3 days of delivery responsibility for replacement parts falls on the customer and they must pay for replacement pieces.*** ***Glassware Safety Disclaimer: BVV™ is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.***
$6,000.00 - $7,650.00
280L Centrifuge Bags
This nylon bag is designed to fit in our BVV brand centrifuges to contain material and be easily swappable after runs to speed up processing times. These bags come with 2 zippers and come in 1, 10, 50, 100, and 200 micron filtration levels. For use with 280L Centrifuges Appx. Size : 39.25" Diameter x 14" Height Specifications SKU Appx. Diameter In. Appx. Height in. CFB-45L-XXX 17.5" 11.75" CFB-160L-XXX 32.25" 13" CFB-280L-XXX 39.25" 14" CFB-475L-XXX 47.25" 16.75"
$160.00 - $416.00
XL Refinement Filter
XL Refinement Filter The BVV™ XL Refinement Filter is a stainless steel filtration system that provides industrial scale, high flow filtering, with greatly improved functionality compared to a traditional Buchner filter. Utilizing a collection base for vacuum assistance and storage of material, the XL Refinement Filter allows for industrial filtration with a longer lifespan and ease of use. Key Features: Stainless steel design for greater thermal conductivity and improved lifespan Easy to clean and disassemble with Tri-Clamp stainless steel parts Mobile Rack mounted with wide mouth design **Rack #2 option has extra space to mount additional filters or heat exchangers Secondary collection vessel for vacuum and storage of material Liquid dip tube for direct injection into rotary evaporator after filling Key Specifications: Large 12" Diameter x 24" Long Fully Jacketed Column Massive 20LB (23.5 Gallons / 89 Liters) Fully Jacketed Collection Base 5 micron Sintered Stainless Steel Filter Disc 100 Pack of Qualitative Cellulose Filter Paper Dedicated 3/8" Vacuum Valve Dedicated 3/8" Dip Tube Valve Silicone gaskets with high alcohol resistance 3/8" Stainless steel hose barb connections Polycarbonate sights for easy viewing Jacketed Filter for temperature stability Quick Start Operation Instructions: Before beginning filtration, pre-chill refinement filter for best thermal conductivity Secure ashless filter paper with compression ring connect tubing from refinement filter to a vacuum pump Attach vacuum system to the dedicated vacuum valve Begin to pour solution into filter Close dedicated dip tube valve and start vacuum Once solution has been completely filtered, stop vacuum system and disconnect from dedicated vacuum valve Connect dedicated dip tube valve to injection valve on rotovap Begin rotovap procedure Open dedicated dip tube valve and begin injecting filtered solution into rotovap
$3,050.00 - $4,860.00
5L Short Path Distillation Kit with P5 Distillation Head
5L Short Path Distillation Kit with P5 Distillation Head This unit carries a 2 day lead time. The 5L Distillation Kit includes everything needed to perform distillation excluding the vacuum pump and chiller. This kit features our USA made P5 Distillation Head, as well as USA, made glass. This Kit is designed for high volume production with the highest quality components for precise, repeatable results time and again. This Kit Does NOT include a vacuum pump or chiller. Please see the below recommendations for both as well as recommended add-ons. Recommended Vacuum Pumps: Pro Series 11.3CFM Corrosion Resistant Two Stage Vacuum Pump (recommended option) Just Better 6 CFM 2 Stage Deep Vacuum Pump (economy option) Recommended Chillers: Polyscience 7 Liter MX Heated Circulator (economy option) Polyscience 7 Liter Refrigerated Circulator (premium option with chilling capability) Recommended Add-Ons: Bullseye Precision Vacuum Gauge (premium vacuum gauge for measuing depth) CT40 or CT80 Electronic Cold Trap (electronic cold trap, dry ice replacement) J-KEM Digital Vapor Temp Monitor (digital vapor temp monitor with data-logging capabilites) Specifications: Boiling Flask Size: 5L Receiving Flask Size: 2x 500mL, 1000mL Batch Capacity approximate: 1000-2500 grams Run time: 4 to 8 hours dependent upon material composition and throughput Distillation Temperature Range: 140-250C (Do not exceed 250C) Recommended Condenser Temperature: 40-50C This Kit Includes: Glass components: 5L Boiling Flask P5V6 Distillation Head Triple Neck Cow 2x 500mL Receiving Flask 1L Receiving Flask 120mm Glass Funnel Dewar cold trap Accessories: PTFE Magnetic Stir Bar Retriever 5 Pack of Metal Keck Clips Dow Corning High Vacuum Silicone Grease Tripod Stand 5L Digital Heating and Stirring Mantle 3-Finger Adjustable Clamp 0-77mm 6" x 6" Scissor Jack 500-1000mL Cork Stand 2x 24/40 ChemglassPTFE Thermometer Inlet Adapter 10ft of Gum Rubber Vacuum Hose 10ft of Silicone Chiller Hose 1/4" Vacuum Manifold Traceable Kangaroo Thermometer - Digital 10 Pack of Adjustable Stainless Steel Tubing Clamps Fiberglass Insulation Rope 10 Feet Distillation Quick Start Guide This guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs, Before beginning distillation, ensure the following steps have been taken: Vacuum Pump is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed. All glass components are in good working order and ready to be assembled A winterization and degassing procedure has been done to prepare oil for distillation The unit's max internal temperature cannot exceed 380C. The recommended max set temperature should not exceed 250C Once all three of these steps have been completed, you are ready to begin distilling. Begin by placing stir bar in boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer. Assemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware Attach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation. Connect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system. Connect receiving cow to cold trap. Connect cold trap to manifold. Connect vacuum gauge to manifold. At this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process. Turn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability. Start stir slower and increase speed with temperature. Once you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C. You will see your first fraction somewhere between 180C and 190C or slightly before. This is the “heads” fraction. You will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to “self-clean” the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your “main body” fraction. You will see temps between 190-220C during this fraction. Continue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed. The final “tails” fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The “tails” fraction has an obvious color change and will be darker than the “main body” fraction. You will see temps between 200-250C during this fraction. As fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well. Once process is complete, stop heat, stop stir, and stop vacuum. Let atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation. *Notice to Customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. BVV™ is not responsible for the failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail, which can cause bodily harm or damage to the surrounding area.
$2,200.00
1L Standard Distillation Turnkey Setup
1L Standard Distillation Turnkey Setup The Standard Distillation Turnkey Setup includes all the components necessary to successfully perform distillation at an entry level price point. The Standard Turnkey Setup Includes: 1L Distillation Kit 1/4" Flare x 1/4" Barb Adapter BVV™ 5L Heated Circulator BVV™ V9D 9CFM Two Stage Vacuum Pump Distillation Quick Start Guide This guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs, Before beginning distillation, ensure the following steps have been taken: Vacuum Pump is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed. All glass components are in good working order and ready to be assembled A winterization and degassing procedure has been done to prepare oil for distillation Once all three of these steps have been completed, you are ready to begin distilling. Begin by placing stir bar in boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer. Assemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware Attach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation. Connect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system. Connect receiving cow to cold trap. Connect cold trap to manifold. Connect vacuum gauge to manifold. At this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process. Turn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability. Start stir slower and increase speed with temperature. Once you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C. You will see your first fraction somewhere between 180C and 190C or slightly before. This is the “heads” fraction. You will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to “self-clean” the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your “main body” fraction. You will see temps between 190-220C during this fraction. Continue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed. The final “tails” fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The “tails” fraction has an obvious color change and will be darker than the “main body” fraction. You will see temps between 200-250C during this fraction. As fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well. Once process is complete, stop heat, stop stir, and stop vacuum. Let atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation. ***Note: This entire setup will ship via motor freight.*** *Notice to Customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. BVV™ is not responsible for the failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail, which can cause bodily harm or damage to the surrounding area.
$2,100.00 - $2,350.00
20L Neocision Dual Short Path Distillation Turnkey System
20L Neocision Dual Short Path Distillation Turnkey System This unit carries a 2 day lead time. (Note: This kit does NOT include the stainless steel table.) The 20L Neocision Distillation Turnkey Setup features our Dual USA made P10V6 Distillation Heads. Every component in this distillation kit is made for precision, throughput, and repeatable results. You will also receive Dual Dewar Style Ribbed Glass Cold Traps to keep all volatiles and solvents out of your vacuum system. This Turnkey Setup gives you everything needed to perform distillation at the highest level. The 20L Neo Kit Includes: 20L Neocision Kit with glassware, labware, and Dual P10V6 Distillation Heads. BVV 15 Liter Advanced Digital Heated Circulator Choice of Vacuum Pump KF-25 Bellow Y Manifold Dual Ribbed Dewar Style Glass Cold Trap Non-Mercury Glass Thermometers 20L Digital Heating and Stirring Mantle Distillation Quick Start Guide This guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs, Before beginning distillation, ensure the following steps have been taken: Vacuum Pump is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed. All glass components are in good working order and ready to be assembled A winterization and degassing procedure has been done to prepare oil for distillation The unit's max internal temperature cannot exceed 380C. The recommended max set temperature should not exceed 250C Once all three of these steps have been completed, you are ready to begin distilling. Begin by placing stir bar in the boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer. Assemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware Attach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation. Connect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system. Connect receiving cow to cold trap. Connect cold trap to manifold. Connect vacuum gauge to manifold. At this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process. Turn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability. Start stir slower and increase speed with temperature. Once you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C. You will see your first fraction somewhere between 180C and 190C or slightly before. This is the “heads” fraction. You will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to “self-clean” the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your “main body” fraction. You will see temps between 190-220C during this fraction. Continue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed. The final “tails” fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The “tails” fraction has an obvious color change and will be darker than the “main body” fraction. You will see temps between 200-250C during this fraction. As fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well. Once process is complete, stop heat, stop stir, and stop vacuum. Let atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation. ***Note: This entire setup will ship via motor freight.*** *Notice to Customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. BVV™ is not responsible for the failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail, which can cause bodily harm or damage to the surrounding area.
$13,000.00 - $17,000.00
Glas-Col Stirmantle
2L Glas-Col Stirmantle Glas-Col offers two types of StirMantles: Electromagnetic (50 to 750 rpm) and Motor Driven (100 to 1850 rpm). The maximum rpms available for each type depends on the viscosity of the solution being heated. Electromagnetic StirMantles are typically used with aqueous solutions like water, while the Motor Driven units use a powerful magnet for higher viscous solution like oils. StirMantles withstands 400°C internal operating temperature. EMS series include the heating mantle, speed control and stir-bar. WARNING: chemical spillage, overheating, overloading, and general misuse will greatly reduce service life! Note: The temperature probe this mantle comes with can only be used with a thermowell. If you are using it with BVV™ glassware you will need to add SKU: TK1/4-12 or TK1/4-18 depending on what mantle size is selected.
$1,050.00$600.00
Magnetic PTFE Stirring Bar - L Style - 70mm
Magnetic PTFE Stir Bar - L Style - 70mm Reduce stir bar jumping with the contoured shape of this L Style Magnetic PTFE Stir Bar. Ideal for round-bottom flask stirring applications. This 70mm L Style Magnetic Stir bar is great for round-bottom flasks above 5 liters in capacity. With its PTFE coating this Magnetic Stir Bar carries excellent solvent and temperature compatibility for a variety of applications. Specifications: L Style 70mm Length Material: High-temperature PTFE
$15.00
P2V4 Neocision Distillation Head - USA Made
P2V4 Neocision Distillation Head P2V4 Short Path Distillation Head includes 4 sets of Vigreux with 24/40 Joints and GL-14 Barb Connections. Key Features: MADE IN THE USA Designed for 1 & 2 Liter Flasks Set of 4 Vigreux to allow for better seperation of fractions without packing material Larger vacuum jacket allows for less heat loss during distillations Larger vapor path to allow for gas/vapor phase flow Increased internal diameter for faster, more efficient fractioning as well as packing and unpacking of media Increased condenser length and diameter for more efficient condensation of vapor with zero clogging *Notice to customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. **Glassware Safety Disclaimer: BVV™ is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.**
$750.00$550.00
ChemTek Large Fuge Bags - 50 Pack
ChemTek Large Fuge Bags - 50 Pack Centrifuge bags used for separations. Specifications: Size: 50-Pack Dimensions: H: 7” W: 6.5” Micron Size: 25 Micron Material: Food Grade Nylon
$50.00
Wireless Digital Vacuum Gauge 1~19,000 Microns
VGW-mini Wireless micron vacuum gauge measures vacuum via just one service port and with no loss of refrigerant. Its compact, robust and smart design support HVAC technicians with numerous intelligent features like the graphic display of measurement data in the Elitech Tools App. Its smart Bluetooth integration allows for data to be stored and evaluated reliably and efficiently, thus saving precious time and resources. Product Features High Accuracy The digital vacuum gauge achieves precise deep vacuum measurements down to single digit resolutions and provides notifications when the evacuation target is met. Smart APP Control Control your micron tester remotely and navigate through all measurement data via Smartphone or Tablet. Quickly and conveniently document your job, finalize your report and export - directly from the job site. Intelligent Judgement of H2O Status The vacuum meter automatically judges physical state of H2O by comparing ambient temperature and water saturation temperature corresponding to the vacuum in the system. Large, Easy-to-Read Display Continual digital readout of evacuation process can be viewed easily on the large, full-view LCD screen. Rechargeable Lithium Battery Built-in rechargeable lithium battery can work up to 20 hours per single full charge, saving troubles of frequent battery change. Product Specifications Measuring Range: 0-19000 micron Operating Temperature: -4℉~140℉ (-20°C~60°C) Interface: 1/4 SAE Accuracy: 1~10,000 microns: ±10% of readings ±10 microns10,000~19,000 microns: ±20% of readings Resolution: 0-400 1 Micron400-3000 10 Micron3000-10000 100 Micron10000-19000 250 Micron Vacuum Units microns, mTorr, in/hg, Pa, Torr, KPa, mbar and psia Battery rechargeable lithium battery (1,000mAh) Overload 27.5 bar Certification CE
$170.00
P10V6 Neocision Distillation Head - USA Made
P10V6 Distillation Head P10V6 Distillation Head has 6 sets of vigreux in the distillation column with 45/50 lower joint, 24/40 Thermometer Joint, and a 34/45 side joint and includes GL-14 barb connections. MADE IN THE USA Designed for 10 Liter Flasks Set of 6 vigreux to allow for packing media Larger vacuum jacket allows for less heat loss during distillations Larger vapor path to allow for gas/vapor phase flow Increased internal diameter for faster, more efficient fractioning as well as packing and unpacking of media Increased condenser length and diameter for more efficient condensation of vapor with zero clogging *Notice to customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. **Glassware Safety Disclaimer: BVV™ is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.**
$600.00
J-KEM DVR-200-EV Digital Vacuum Regulator
J-KEM DVR-200-EV Digital Vacuum Regulator The DVR-200-EV has the same stainless steel pressure transducer inside, but the vacuum valve is outside of the controller. The value of this design is that the vacuum valve can be cleaned or replaced much easier than the valve in the classic DVR-200. Some applications, like distillations or stripping large volumes of solvent, can leave residues inside the valve which causes it to fail. Replacing the vacuum valve is the most frequent repair that J-KEM performs on the DVR-200. Replacing the valve in the classic DVR-200 is difficult and must be returned to J-KEM for repair. With the EV version, the user can disassembled the valve and wash it out, or even replace it in under 5 minutes. For large distillations or botanical applications, J-KEM recommends the DVR-200-EV. No Mercury 100% digital pressure entry and control Wetted parts are 100% stainless steel and Teflon Vacuum ramping feature eliminates bumping Resists: All organic solvents Acids Bases Water Specifications: 100 watts. Vacuum fittings: 1/8″ NPTM. Warranty: Electronics 2 Years, Vacuum Valve 6 months (void if damaged by chemical buildup)
$1,665.00
P5 Distillation Head - USA Made
P5 Distillation Head P5 Packable Distillation Head with 34/45 lower joint and 24/40 upper and side joints. Includes GL-14 Barb Connections. Recommended packing media: Raschig Rings, Porcelain Berl Saddles, Glass Beads, Pro-Pak, or Stainless Steel Wool. Key Features: MADE IN THE USA Designed for 5 Liter Flasks Single set of lowered vigreaux to allow for packing media Larger vacuum jacket allows for less heat loss during distillations Larger vapor path to allow for gas/vapor phase flow Increased internal diameter for faster, more efficient fractioning as well as packing and unpacking of media Increased condenser length and diameter for more efficient condensation of vapor with zero clogging *Notice to customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. **Glassware Safety Disclaimer: BVV™ is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.**
$550.00$400.00
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