Meta Purification
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316L Stainless Dutch Weave Sintered Filter Disk 1 micron and up - BUNA-N
316L Dutch Weave Sintered Filter Disk **Note: This product comes with Filter Disk and Gasket ONLY. Filter Plate and Spool are NOT included. Recommended Filter plate click here. These 316L stainless steel dutch weave filter disks come with a custom made gasket to allow the user to insert filtration between clamping ends of any Tri-Clamp interface. The interface fits so snug, its inherent design prevents any blow-by. BVV™ 316L Dutch Weave Sintered Filter Disk - Data Sheet Pressure Ratings w/o any backing support; strait pipe connection: 1.5" 200PSI 2" 200PSI 3" 200PSI 4" 200PSI 6" 50PSI 8" 10PSI *Supporting Back Plate Required P# FP800-V3 10" 10PSI *Supporting Back Plate Required P# FP1000-V3 12" 10PSI *Supporting Back Plate Required P# FP1200-V3
$41.62 - $804.71
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Single Neck Round Bottom Flask
Single Neck Round Bottom Flask Single neck round bottom flasks can be used for a variety of applications such as capturing and collecting material and also used for boiling off material through distillation. These flasks are single neck with a ground 24/40 joint and require the application of vacuum grease to the ground surface when using the flasks in a vacuum application. When laying these flasks down it is always recommended to use a cork stand for the flask to prevent breakage and keep the flask upright. Sizes Available: 50ml - 24/40 Ground Joint 100ml - 24/40 Ground Joint 125ml - 24/40 Ground Joint 250ml - 24/40 Ground Joint 500ml - 24/40 Ground Joint 1000ml - 24/40 Ground Joint 2000ml - 24/40 Ground Joint *Notice to customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. **Glassware Safety Disclaimer: BVV™ is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.**
$12.49 - $52.72
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Cork Stand
Cork Stands Cork stands are used with laboratory glassware to help balance round bottom flasks or prevent damage or support a piece of glassware that is put on it. ***Note: Sizes correlate to round bottom flasks ml sizes. Sizes Available: 250-500ml 500-1000ml 1000-2000ml
$8.32 - $11.10
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Double Neck Round Bottom Flask
Double Neck Round Bottom Flask Double Neck Round Bottom Flasks can be used for a variety of applications such as capturing and collecting material and also used for boiling off material through distillation. These flasks are double neck with a ground 24/40 joint and require the application of vacuum grease to the ground surface when using the flasks in a vacuum application. The second neck of this flask can also be used for a thermometer port or for introducing material into the flask with a glass funnel. When laying these flasks down it is always recommended to use a cork stand for the flask to prevent breakage and keep the flask upright. Sizes Available: 500ml - 24/40 Ground Joint 1000ml - 24/40 Ground Joint 2000ml - 24/40 Ground Joint *Notice to customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. **Glassware Safety Disclaimer: BVV™ is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.**
$54.11 - $76.31
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6" Stainless Steel Diamond Miner
6" Stainless Steel Diamond Miner This 6" Diamond Miner is used for crystallizing botanical extracts into live resin terpene-rich sauce. This Diamond Miner eliminates the need for glass jars and makes your degassing procedure safer. The premium extractor lid is pre-assembled and nitrogen tested for leaks to ensure the customer receives a leak and worry-free part to use on their extraction system. These valves come with a 1-year manufacturer warranty against defects and are custom-built. Remove the 6" x 2" splatter platter to easily remove diamonds from your sauce mix. Glycerin filled compound gauge gives you an easy readout of pressure inside the vessel. Specifications: 304 Grade Stainless Steel 500-700ml Optimal Capacity (725ml) Max Fill 1.5" sight glass 6" splatter platter High-pressure clamps 316 Stainless Steel Valve with 1/4" Flare Connection Temp Range -40 to 230C Compound Gauge (-30)-(150) MAWP: 100 psi
$485.60 - $901.83
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Nylon Filter Bag Socks
Nylon Filter Bag Socks Nylon Filter Bag Socks make loading and unloading spools way faster and easier. Keep production costs down by hot-swapping socks and continuing to process material with less downtime. The 90 micron socks are made of nylon and the 53 micron socks are made of monofilament polyester, both of which won't react to solvents and are very durable. For the 90 micron socks, we recommend getting socks that are 2" larger in diameter than the spool size, which is how we've sized them. **NOTICE** Unlike the 53 micron socks, the 90 micron socks do not feature extra material around the top collar which can stretch around the top of the column, they will only fit inside the column. The only exception to this is the FILTERBAG-10X60IN-90M. ** Quality Materials: The 90 micron bags are made of high quality Nylon, and the 53 micron Filter bags are made of monofilament polyester, both of which are durable, stable, rust and corrosive resistance and good for long time use. Precise Design: The filter bag is designed to fit Spool. Wide Range of Applications: The filter bag is used to filter impurities during the reaction process is suitable for different media with working highest Temperature at 248℉. Resistant to many chemicals, unaffected by metal fatigue or corrosion, and have high tensile strength. Convenient organization and storage: 1PC Packed in a small plastic bag. The filter bag life depends on the working environment and the frequency of using, Check it Regularly for aging, damaged or hardening. SKU BAG SIZE (in) FITS SPOOL(in) (90m will not stretch over top of column) MESH (micron) FILTERBAG-6X60IN-90M 6X60 4 90 FILTERBAG-8X60IN-90M 8X60 6 90 FILTERBAG-10X60IN-90M 10x60 8 90 FILTERBAG-12X36IN-90M 12x36 10 90 FILTERBAG-12X60IN-90M 12x60 10 90 FILTERBAG-12X60IN-90M 12X60 8 90 FILTERBAG-3IDx12L-53M 5x14 3x12 53 FILTERBAG-4IDx24L-53M 8x28 4x24 53 FILTERBAG-4IDx48L-53M 8x52 4x48 53 FILTERBAG-6IDx24L-53M 10x30 6x24 53 FILTERBAG-6IDx48L-53M 10x54 6x48 53 FILTERBAG-8IDx48L-53M 14x56 8x48 53 Chemically Compatible with: Acetone Amyl Alcohol (only up to 70°F) Butane Butyl Alcohol Diacetone Alcohol (only up to 70°F) Dowtherm (only up to 70°F) Ethanol Ether Ethyl Acetate Ethylene Glycol Glycol Glycol Monoether (only up to 70°F) Isopropyl Acete Isopropyl Alcohol Methane (only up to 70°F) Methyl Acetate Methyl Alcohol Methyl Cellosolve (only up to 70°F) Methylene Chloride (only up to 100°F) Nitrogen Propane (only up to 250°F) Propylene Glycol Sodium Carbonate Sodium Chlorate (only up to 180°F) Sodium Chloride 10% Sodium Cyanide Sodium Peroxide (only up to 70°F) Steam (only up to 220°F) Sulfuric Acid 5% Sulfuric Acid 50% (only up to 70°F) Sulfuric Acid 96% (only up to 70°F) Sulfuric Acid Fuming Sulfurous Acid
$26.36 - $55.50
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Thermo Scientific Traceable Kangaroo Thermometer - Digital
Digital Thermometer Traceable Kangaroo™ Thermometer comes equipped with the 42-inch probe cable in a reel-compartment pouch in the back of the unit. As a perfect “carry-around” unit, this thermometer can fit easily in any pocket, or you can use the convenient flip-open stand to place upright. The dual-range digital thermometer measures temperature in test tubes, beakers, and other scientific laboratory equipment and is especially effective for rugged applications with high-impact ABS cases. Additionally, digital thermometers can measure the temperature of many substances from air to liquids to surfaces—all electronically. The best thing about this thermometer? It’s easy to use! Any user can record identical results with this intuitive unit. The range is –58.0 to 572°F and –50.0 to 300°C with a resolution of 0.1° (between –19.9 to 199.9°) otherwise 1° and an accuracy of ±1°C (between –30 and 250°C) otherwise ±2°C. This unit automatically captures and recalls minimum and maximum temperature readings over any time period. Its high and low alarm may be programmed in 1° increments. The alarm sounds every minute until temperature returns to non-alarm condition. Pressing the HOLD key freezes the display to record a current reading. To assure accuracy, an individually serial-numbered Traceable® Certificate is provided from its ISO 17025 calibration laboratory accredited by A2LA. It indicates traceability to standards provided by NIST (National Institute of Standards and Technology). The stainless-steel probe has a diameter of 0.14 inches x 7-1/2 inch length and is resistant to most chemicals. The supplied silver-oxide battery runs continuously for one year. Large 3/4-inch digits are readable from 20 feet. Compact size is 2-1/2 x 4-3/4 x 1/2 inches, and weight is 2-3/4 ounces. Each product goes through an intense vetting process before carrying the Traceable name, which means you’ll save both time and money by not having to calibrate separately. The Traceable Kangaroo Thermometer applies to various unique applications such as the storage, laboratory, and medical industries. Specifications: Temperature Range F: -58 - 572F Temperature Range C: -50 - 300C Temperature Resolution: 0.1C Temperature Accuracy: +/-1C Programmable High and Low Alarm ISO 17025 Calibration Stainless Steel Probe Diameter of Probe: 0.14 in Length of Probe: 7.5 in Size: 2.5x4.75x.5 in Weight: 2.75 ounces
$83.25
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2 Pack Magnetic PTFE Stirrer - L Style - 28mm
2 Pack Magnetic PTFE Stir Bar - L Style - 28mm Shop this 2 Pack Magnetic PTFE Stirring Bar to stir liquids in a closed container on BVV™! Used in short-path distillation. Find product details below. Specifications: L Style 28mm Length Material: High-temperature PTFE Quantity: 2
$9.71
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316L Stainless Dutch Weave Sintered Filter Disk 1 micron and up - Silicone
316L Dutch Weave Sintered Filter Disk **Note: This product comes with Filter Disk and Gasket ONLY. Filter Plate and Spool are NOT included. Recommended Filter plate click here. These 316L stainless steel dutch weave filter disks come with a custom made gasket to allow the user to insert filtration between clamping ends of any Tri-Clamp interface. The interface fits so snug, its inherent design prevents any blow-by. Sintered Filter Disk Technical Data Sheet Pressure Ratings w/o any backing support; strait pipe connection: 1.5" 200PSI 2" 200PSI 3" 200PSI 4" 200PSI 6" 50PSI 8" 10PSI *Supporting Back Plate Required P# FP800-V3 10" 10PSI *Supporting Back Plate Required P# FP1000-V3 12" 10PSI *Supporting Back Plate Required P# FP1200-V3
$41.62 - $804.71
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Dewar Style Glass Cold Trap Kit
Dewar Style Glass Cold Trap The Dewar Style Glass Cold Trap with GL-14 Barb Fittings allows the user to load dry ice into the inner portion of the cold trap from the top to allow maximum condensation temperatures. This protects your vacuum pump and captures any vapors that were lost during evaporation or distillation. Made in the USA. Dewar Style Glass Cold Traps includes the following: Metal Keck Clip Boss Head Lab Stand Chain Clamp 250ml Round Bottom Flask 24/40 Joint 250-500ml Cork Stand Specifications: USA Made 24/40 Male Ground Joint GL-14 8mm Barb Connections OD = 3.8" ID = 2.75" Height = 14.75" *Notice to customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. **Glassware Safety Disclaimer: BVV™ is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.**
$485.60
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2 Pack Magnetic PTFE Stirring Bar - B Style - 40mm
2 Pack Magnetic PTFE Stirring Bar - B Style - 40mm 2 Pack Magnetic PTFE Stirring Bar Specifications: B Style 40mm Length Material: High temperature PTFE Quantity: 2
$11.10
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Chain Clamp
Chain Clamp Chain clamp for use with tripod stands or other laboratory stands. Allows user to secure large diameter glassware, such as glass cold traps, to tripod or laboratory stands using boss head clips. Specifications: Chain Length = 15" Spring Loaded Tensioner Rod Length = 8.5" Rod Diameter = .475"
$29.14
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45L Centrifuge Bags
This nylon bag is designed to fit in our BVV brand centrifuges to contain material and be easily swappable after runs to speed up processing times. These bags come with 2 zippers and come in 1, 10, 50, 100, and 200 micron filtration levels. For use with 45L Centrifuges Appx. Size : 17.5" Diameter x 11.75" Height Specifications SKU Appx. Diameter In. Appx. Height in. CFB-45L-XXX 17.5" 11.75" CFB-160L-XXX 32.25" 13" CFB-280L-XXX 39.25" 14" CFB-475L-XXX 47.25" 16.75"
$159.55 - $414.84
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Inline CRC
Inline CRC Kit BVV's Inline CRC Kit can be utilized to adapt any 1.5", 2", 3", 4", or 6" diameter material column for inline adsorbent filtration. This kit includes a corresponding sized media column and a filter stack including a 5 micron & 1 micron Dutch Weave Sintered Filter Disc. This Inline color remediation kit is meant to be plumbed between your existing extractors material column and the existing hemispherical reducer of any closed loop hydrocarbon extractor.Assembly starts with placing the 1 micron sintered disk and gasket between the extracts hemispherical reducer and the included filter plate securing both with one of the included high-pressure clamps. Next, take the 5-micron sintered disk and the included ashless filter paper and rip around the circumference of the sintered disk, placing both atop the filter plate placing the sintered disc gasket and media column spool over top before securing both with the remaining high-pressure clamp. Since the spool secures the filter paper in place a filter plate ring is not required. Media can then be layered into the media column by weight before placing the loaded material column above the adsorbent filtration column and assembling the remainder of the extractor. For optimum filtering results utilize the following layer recipe from top to bottom: 30-50g per lb of biomass Silica 60A 75-100g per lb of biomass Bentonite Clay 30-50g per lb of biomass Neutral Activated Alumina This Kit includes: Media column Tri-clamp Spool V3 Filter Plate 5 Micron Sintered Disk 1 Micron Sintered Disk 2X Buna-N Sintered Disc Gaskets 2X High-pressure Clamps Fast Flow Ashless Filter Paper (100qty) *This video provides a visual assembly of the 3" Inline CRC which is applicable across all sizes*
$242.80 - $681.23
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2 Pack Magnetic PTFE Stirring Bar - B Style - 28mm
2 Pack Magnetic PTFE Stirring Bar - B Style - 28mm 2 Pack of Magnetic PTFE Stirring Bar. Specifications: B Style 28mm length Material: High temperature PTFE Quantity: 2
$11.10
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Porcelain Buchner Funnel Filtration Kit
Porcelain Buchner Funnel Filtration Kit This BVV™ Porcelain Buchner Funnel Filtration Kit was designed for continuous filtration of oils by using our large diameter porcelain Buchner funnel by increasing filtration area. Depending on the capacity needed you may select the size of the conical flask through a dropdown for 2500ml or 5000ml capacities. This Kit Includes the Following: (1) 1.5 Gallon Cold Trap with 1/4" Barbs (1) Rubber Cones, Set of 9 (1) Porcelain Buchner Funnel - 1000ml(When 2500ml Conical Flask is selected) or 2000ml(When 5000ml Conical Flask is selected) (1) BVV4D 4CFM Two Stage Vacuum Pump (1) Conical Flask with Filtering Side Arm - 2500ml or 5000ml (5') Gum Rubber Vacuum Tubing (1) HVAC hose (1) Ashless Filter Paper - 180mm Qualitative - Grade 1
$450.92 - $693.72
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5L Digital Heating and Stirring Mantle
5L Digital Heating and Stirring Mantle Digital Heating and Stirring Mantles give the operator the most precise temperatures and readouts during distillations. These mantles autotune to specific user input to provide consistent results. Each mantle is equipped with large digital display that will give you readouts for both set temperature, actual temperature, and stirring speed. Each mantle also comes with a vertical brace bar and boss head as well as a temperature probe which plugs directly into the mantle. For first time use, the mantle should have an initial burn out done. This will burn off any residual oils used in the production of the insulation rope. The unit's max internal temperature cannot exceed 380C. The recommended max set temperature should not exceed 250C Features: PID Temperature control Brushless magnetic magnetic stirrer motor Temperature protector Specifications: Capacity: 5L (5000mL) Power Supply: 110V 60Hz Adjustable Rotation Speed: 50-1800 RPM Motor Power: 40W, DC14-24V Heating Power 180-2200W Temperature Control Accuracy: +/- 1C Intelligent Temperature Control: Yes Temperature Range: RT+10-380C Insulation Material: Alkali-free Glass Fiber, temperature resistant up to 450C Shipping Dimensions: 20 x 15 x 14 in. Weight: 12 lbs
$1,179.32
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4" Stainless Steel Diamond Miner
4" Stainless Steel Diamond Miner The 4" Diamond miner eliminates the need for glass jars and adds safety to your degassing procedure. It also gives you multiple viewing angles to see your diamond growth. Remove the 4" x 2" splatter platter to easily remove diamonds from your sauce mix. A glycerin filled compound gauge gives you easy readout of pressure inside the vessel. Specifications: 304 grade stainless steel 500ml - 750ml Optimal Capacity 1.5" sight glass 4" sight glass 4" splatter platter High pressure clamps 316 Stainless Steel Valve with 1/4" Flare Connection Temp Range -40 to 230C MAWP: 100 psi
$624.35 - $985.08
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Cold Trap 4" Stainless Steel
Cold Trap 4" Stainless Steel This Stainless Steel Cold is designed and intended for use with the Polyscience IP100 Cold Finger (Can also be used with dry Ice) to create a cold trap that can achieve extremely frigid temperatures. These cold traps have 2 1/4" FNPT ports with one having a dip tube to the bottom of the trap to achieve higher vapor condensing rates with the 4" Diameter Center opening for the IP100. This Cold trap also has an insulating vacuum jacket around the entire container to maintain the subzero temperatures and help achieve the maximum minimal temperature of the IP60. Unlike many cold Traps on the market, this one is also made out of 304 Stainless steel and the internal parts are resistant to most chemicals and easily cleaned due to the Tri-Clamp lid design. Specifications Material 304 Stainless Steel Temperature Rating -200 to 200°C Ultimate Vacuum <100millitorr / microns Cold Finger Internal Dimensions 3.85" x 11.75" (Fits Polyscience IP100) Trap Internal Dimensions 7.85" x 10" Outside Dimensions 10" x 16" x 15" (Includes jacket gauge and valve hardware) Weight 38LBS
$763.09 - $832.46
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Large Refinement Filter
The BVV™ Large Refinement Filter is a stainless steel filtration system that provides large scale, high flow filtering, with greatly improved functionality compared to a traditional Buchner filter. Utilizing a collection base for vacuum assistance and storage of material, the Refinement Filter allows for benchtop filtration with a longer lifespan and ease of use. ***Note: Unit will come with 12" Single Pin Clamps for easier assembly/disassembly. Key Features: Stainless steel design for greater thermal conductivity and improved lifespan Easy to clean and disassemble with Tri-Clamp stainless steel parts Small tabletop footprint with wide mouth design Secondary collection vessel for vacuum and storage of material Liquid dip tube for direct injection into rotary evaporator after filling Key Specifications: Large 12" Diameter x 12" Height Funnel with 12" Filtration Plate 40 Liter Collection Base 5 micron Sintered Stainless Steel Filter Disc 100 Pack of Ashless Filter Paper Dedicated 3/8" Vacuum Valve Dedicated 3/8" Dip Tube Valve Silicone gaskets with high alcohol resistance 3/8" Stainless steel hose barb connections Polycarbonate sights for easy viewing 2" Tri-Clamp Short Sight Glass for Flow Viewing Operation Instructions: Before beginning filtration, place refinement filter in freezer for best thermal conductivity Secure ashless filter paper with compression ring Place collection base on floor and connect tubing from refinement filter to to a vacuum pump Attach vacuum system to the dedicated vacuum valve Begin to pour solution into filter Close dedicated dip tube valve and start vacuum Once solution has been completely filtered, stop vacuum system and disconnect from dedicated vacuum valve Connect dedicated dip tube valve to injection valve on rotovap Begin rotovap procedure Open dedicated dip tube valve and begin injecting filtered solution into rotovap
$3,191.10
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2 Pack Magnetic PTFE Stirring Bar - HL Style - 25mm
2 Pack Magnetic PTFE Stirring Bar - HL Style - 25mm 2 Pack Magnetic PTFE Stirring Bar Specifications: HL Style 25mm length Material: High temperature PTFE Quantity: 2
$11.10
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Refinement Filter
The BVV™ Refinement Filter is a stainless steel filtration system that provides large scale, high flow filtering, with greatly improved functionality compared to a traditional Buchner filter. This includes the Refinement Filter only. Does not include the 20L collection base. Please note, the Refinement filter alone does not have a vacuum port. You must pull vacuum through a secondary vessel if you are not using the 20L collection base. Key Features: Stainless steel design for greater thermal conductivity and improved lifespan Easy to clean and disassemble with Tri-Clamp stainless steel parts Small tabletop footprint with wide mouth design Wide base for stability while pouring Key Specifications: 216 cubic inches of liquid volume (3.5 Liters) Silicone gaskets with high alcohol resistance Drop-In Filter Plate with 100 Mesh Screen 3/8" Stainless steel barb connections Recommended Filter Paper: 180mm
$488.38 - $996.18
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2L Standard Short Path Distillation Turnkey Setup
2L Standard Short Path Distillation Turnkey Setup The Standard Distillation Turnkey Setup includes all the components necessary to successfully perform distillation at an entry-level price point. Crossbar pictured is not included. We recommend purchasing multiple lab stands to accommodate your specific needs. The Standard Turnkey Setup Includes: 2L Distillation Kit 1/4" Flare x 1/4" Barb Adapter BVV™ 5L Heated Circulator BVV™ V9D 9CFM Two Stage Vacuum Pump High quality and durable Borosilicate 3.3 glass Vacuum-jacketed distillation adapter 3-way cow adapter, accommodating up to 3 pcs of 500mL flasks GCT-01 cold trap guarding from damage of vapors Kangaroo Traceable Digital Thermometer Flexible Gum Rubber Vacuum Tubing and Silicone Tubing for Flow Distillation Quick Start Guide This guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs, Before beginning distillation, ensure the following steps have been taken: Vacuum Pump is in good working order. The pump should be run against the dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed. All glass components are in good working order and ready to be assembled A winterization and degassing procedure has been done to prepare oil for distillation The unit's max internal temperature cannot exceed 380C. The recommended max set temperature should not exceed 250C Once all three of these steps have been completed, you are ready to begin distilling. Begin by placing stir bar in boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer. Assemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware Attach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation. Connect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system. Connect receiving cow to cold trap. Connect cold trap to manifold. Connect vacuum gauge to manifold. At this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process. Turn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability. Start stir slower and increase speed with temperature. Once you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C. You will see your first fraction somewhere between 180C and 190C or slightly before. This is the “heads” fraction. You will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to “self-clean” the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your “main body” fraction. You will see temps between 190-220C during this fraction. Continue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed. The final “tails” fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The “tails” fraction has an obvious color change and will be darker than the “main body” fraction. You will see temps between 200-250C during this fraction. As fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well. Once the process is complete, stop heat, stop stir, and stop vacuum. Let the atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation. ***Note: This entire setup will ship via motor freight.*** *Notice to Customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. BVV™ is not responsible for the failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail, which can cause bodily harm or damage to the surrounding area.
$3,607.33
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1L Distillation Kit
1L Distillation Kit The 1L Distillation Kit is a simple, easy to use system designed for small personal use. It includes all stands, clamps, clips, and tubing needed to begin distilling immediately. This Kit Does NOT include a vacuum pump or circulator. Please see the below recommendations for both as well as recommended add-ons. Or check out our 1L Standard Distillation Turnkey Setup which includes vacuum pump and circulator. Recommended Vacuum Pumps: Pro Series 5.6CFM Corrosion Resistant Two Stage Vacuum Pump (premium option) Just Better 6 CFM 2 Stage Deep Vacuum Pump (USA made economy option) Best Value Vacs VE280 9CFM Two Stage Vacuum Pump (economy option) Recommended Circulator: Polyscience 7 Liter MX Heated Circulator (economy option) Polyscience 7 Liter MX Refrigerated Circulator (premium option with chilling capability) Recommended Add-Ons: Glass Dewar Style Cold Trap (recommended cold trap) Bullseye Precison Vacuum Gauge (premium vacuum gauge for measuring depth) CT40 or CT80 Electronic Cold Trap (electronic cold trap, dry ice replacement) Specifications: Boiling Flask Size: 1L Receveiving Flask Size: 250ml Batch Capacity approximate: 200-400 grams Run time: 4 to 8 hours dependent upon material composition and throughput Distillation Temperature Range: 140-250C (Do not exceed 250C) Recommended Condenser Temperature: 40-50C This Kit Includes: Glass Components: 1L 2-Neck Boiling Flask Short Path Head Triple Neck Cow Receiving Flask 3x 250ml Single Neck Round Bottom Flask 14/20 Thermometer Adapter 24/40 Thermometer Adapter 120mm Glass Funnel 14/20 Stopper 24/40 Stopper Accessories: Magnetic PTFE Stirring Bar Retriever 5 Pack of Metal Keck Clips Dow Corning High Vacuum Silicone Grease Tripod Stand 1L Analog Heating and Stirring Mantle 3 Finger Clamp Adjustable 0-70mm Boss Head -13mm 6" x 6" Scissor Jack 250-500ml Cork Stand 10ft of Vacuum Hose 10ft of Chiller Hose 1/4" Vacuum Manifold Traceable Kangaroo Thermometer - Digital 10 Pack of Adjustable Stainless Steel Tubing Clamps Fiberglass Insulation Rope 10 Feet 1.5 Gallon Cold Trap (2QT Tank) Dry Ice, Liquid Nitrogen w/ 2x 1/4" Barb Adapters Distillation Quick Start Guide This guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs, Before beginning distillation, ensure the following steps have been taken: Vacuum Pump is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed. All glass components are in good working order and ready to be assembled A winterization and degassing procedure has been done to prepare oil for distillation Once all three of these steps have been completed, you are ready to begin distilling. Begin by placing stir bar in boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer. Assemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware Attach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation. Connect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system. Connect receiving cow to cold trap. Connect cold trap to manifold. Connect vacuum gauge to manifold. At this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process. Turn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability. Start stir slower and increase speed with temperature. Once you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C. You will see your first fraction somewhere between 180C and 190C or slightly before. This is the “heads” fraction. You will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to “self-clean” the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your “main body” fraction. You will see temps between 190-220C during this fraction. Continue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed. The final “tails” fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The “tails” fraction has an obvious color change and will be darker than the “main body” fraction. You will see temps between 200-250C during this fraction. As fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well. Once process is complete, stop heat, stop stir, and stop vacuum. Let atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation. *Notice to Customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. BVV™ is not responsible for the failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail, which can cause bodily harm or damage to the surrounding area.
$1,387.43
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Distillation Head
BVV™ Distillation Head BVV™ Brand Distillation head is made out of 3.3 Boro and comes with (2) 24/40 Ground Male Joints and a 14/20 Female thermometer joint at the top of the head. This head features 2x GL-14 barbs for the condenser and an extended drip tip for the receiving cow. The head measures 8.5" from the bottom 24/40 joint to the top of the head and the condenser is 3.5" long. The head has 2 sets of quad Vigreux and is bent at a 20-degree angle. *Notice to customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. **Glassware Safety Disclaimer: BVV™ is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.**
$277.49
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475L Centrifuge Bags
This nylon bag is designed to fit in our BVV brand centrifuges to contain material and be easily swappable after runs to speed up processing times. These bags come with 2 zippers and come in 1, 10, 50, 100, and 200 micron filtration levels. For use with 475L Centrifuges Appx. Size : 47.25" Diameter x 16.75" Height Specifications SKU Appx. Diameter In. Appx. Height in. CFB-45L-XXX 17.5" 11.75" CFB-160L-XXX 32.25" 13" CFB-280L-XXX 39.25" 14" CFB-475L-XXX 47.25" 16.75"
$339.92 - $692.33
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Valved Vacuum Adapter 2.0 - Made in USA
Valved Vacuum Adapter 2.0 This Valved Vacuum Adapter allows the user to isolate the vacuum in a short path distillation system from the cow or receiving flasks of the system to allow the easy swap of the flasks and allows for a full bore vapor flow. These adapters have a 24/40 male joint having a grease-less Viton O-ring seal which reduces the grease mess for each fraction. It also includes GL-14 Cap for venting vacuum and also comes with a PTFE threaded valve with Viton Seals. Sizes: 24/40 Joint - All 3 Joints are 24/40 with GL-14 Cap 34/45 Joint - 2 34/45 Joints and 24/40 lower O-ring Joint with GL-14 Cap *Notice to customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. **Glassware Safety Disclaimer: BVV™ is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.**
$624.35
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Cold Trap 2" Stainless Steel
Cold Trap 2" Stainless Steel This Stainless Steel Cold is designed and intended for use with the Polyscience IP60 Cold Finger (Can also be used with dry Ice) to create a cold trap that can achieve extremely frigid temperatures. These cold traps have 2 1/4" FNPT ports with one having a dip tube to the bottom of the trap to achieve higher vapor condensing rates with the 2" Diameter Center opening for the IP60. This Cold trap also has an insulating vacuum jacket around the entire container to maintain the subzero temperatures and help achieve the maximum minimal temperature of the IP60. Unlike many cold Traps on the market, this one is also made out of 304 Stainless steel and the internal parts are resistant to most chemicals and easily cleaned due to the Tri-Clamp lid design. Specifications Material 304 Stainless Steel Temperature Rating -200 to 200°C Ultimate Vacuum <100millitorr / microns Cold Finger Internal Dimensions 1.85" x 11.75" (Fits Polyscience IP60) Trap Internal Dimensions 5.85" x 10" Outside Dimensions 8" x 14" x 15" (Includes jacket gauge and valve hardware) Weight 28LBS
$645.16 - $704.82
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DigiVac Bullseye Precision Gauge | Portable Vacuum Gauge | .001 to 2 Torr Accuracy
Bullseye Precision Gauge | Portable Vacuum Gauge | .001 to 2 Torr Accuracy The Bullseye Precision Gauge is the ideal portable vacuum gauge to serve many applications. This patented vacuum gauge offers Graphical Displays and graphics supporting real-time analytics (Leak, Pump, Outgas, Stable) Visual graphing feature right on the display Display pinpoints the root of the problem so you get it right the first time Put it anywhere with its magnet and kickstand Options: Rugged carrying case designed for instrument, back-up sensor and these adapters that can change the NPT to a KF25 or KF16 vacuum interface adapters Sensor (Probe) Replacements: This gauge is paired with the Thermocouple Plus/531 Equivalent Sensor, but works with Agilent 531 or 536 sensors as well if you are looking for a more robust sensor option Numeric & Graphical Displays See vacuum readings in either numbers or easy-to-read graphs Calibrated & Precise Delivered pretested and calibrated with thermocouple sensor under actual vacuum against a NIST standard. Extended Battery Lifespan Solid state electronics are built into the Bullseye Precision Gauge. The portable vacuum gauge operates using AA batteries and lasts 70 hours. Applications Vacuum pump monitoring, vacuum pump testing, baseline vacuum pump performance, & transformer dry-out, distillation monitoring Bullseye Precision Gauge Accuracy Remember to choose your vacuum gauge that gives you the accuracy you need for your application. This Bullseye comes with a thermocouple sensor, which has better accuracy in the millitorr up to 6 Torr. If you need your Bullseye Gauge to have CE rating then choose either the Bullseye with 531 or Bullseye with 536 KF25 1 to 99 millitorr +/- 2 millitorr or 20% 100 to 2000 millitorr +/- 10% 2 to 6 Torr +/- 25% Above 6 Torr Continuous and monotonic (increasing reading indicates increasing pressure) Units Torr, mbar, bar, kPa, inHg, mm Hg, millitorr, microns, inches of water, PSI, Pa Control Range 1E-4 – 1000 Torr Range with Accuracy .001 – 5 Torr Sensor Type SEN-VGT500, Thermocouple Plus Dimensions 6.2”H x 3.7”W x 1.3”D Certifications ROHS and CE
$772.56
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Analog Heating and Stirring Mantle
Analog Heating and Stirring Mantle is used to heat up a glass round bottom flask and stir the contents inside. Heating and stirring functions are analog and sizes range from 500ml to 2000ml. (Mantle's are tested in house and may show slight discoloration on the heating surface.) Certifications: CE Approval Warranties: 500ml - 30 Day Limited Warranty 1000/2000ml - 90 Day Limited Warranty.
$187.30 - $270.55
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Glass Cold Trap - Ribbed (Made in USA)
BVV™ Glass Cold Trap - Ribbed This dewar style glass is designed to increase surface area for maximum vapor condensation and it also has 24/40 or 34/45 jointed connections to increase vapor flow. Note: The bottom joint will always be 24/40. *Notice to customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement.
$693.72
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4" Stainless Steel Buchner Funnel
4 Inch Stainless Steel Buchner Funnel 4” Buchner Funnel Kit: This buchner funnel kit adapts to any vessel with a 24/40 joint. The included adapter makes it possible to pull vacuum and use large vessels as a collection. Max internal volume of the buchner funnel is 0.82L, but can be adapted with a larger spool for higher capacity. This kit features: 4” x 4” 304SS spool with a capacity of 0.82L 4” Tri-Clamp Single Hinge Clamp 4”x1.5” 304SS Hemispherical Reducer 1.5” Tri-Clamp Double Hinged Clamp 4” 5 Micron 304SS Sintered Disc Filter 4” 304SS Filter Plate V2 1.5”x24/40 304SS Adapter 24/40 Glass Inlet Straight Adapter with hose connection Recommended items: 110MM sized filter paper, 24/40 jointed glass conical flask. For additional information or questions regarding this kit contact our customer support line.
$513.35
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5L Premium Short Path Distillation Turnkey Setup
5L Premium Distillation Kit This unit carries a 2 day lead time. The 5L Premium Short Path Distillation Turnkey Setup features our 5L Distillation Kit with P5 Distillation Head and USA made glass. Every component in this turnkey is made for precision, throughput, and repeatable results. Also included is our Pro Series 11.3CFM Corrosion Resistant Two Stage Vacuum Pump giving you extreme power and depth with a long lifespan, the Bullseye Precision Vacuum Gauge from Digivac which is the most rugged and dependable vacuum gauge on the market, and a BVV 19L Heated Circulator for maximum condensation of vapors. You will also receive a Dewar Style Glass Cold Trap to keep all volatiles and solvents out of your vacuum system. This Turnkey Setup gives you everything needed to perform distillation at the highest level. The Premium Short Path Distillation Turnkey Kit Includes: 5L Distillation Kit with P5 Distillation Head KF-25 x 1/4" Barb Adapter Dewar Style Glass Cold Trap Bullseye Precision Vacuum Gauge Polyscience 7L MX Heated Circulator Pro Series 14.1CFM Corrosion Resistant Two Stage Vacuum Pump Short Path Distillation Quick Start Guide This guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs, Before beginning distillation, ensure the following steps have been taken: Vacuum Pump is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed. All glass components are in good working order and ready to be assembled A winterization and degassing procedure has been done to prepare oil for distillation Once all three of these steps have been completed, you are ready to begin distilling. Begin by placing stir bar in boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer. Assemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware Attach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation. Connect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system. Connect receiving cow to cold trap. Connect cold trap to manifold. Connect vacuum gauge to manifold. At this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process. Turn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability. Start stir slower and increase speed with temperature. Once you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C. You will see your first fraction somewhere between 180C and 190C or slightly before. This is the “heads” fraction. You will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to “self-clean” the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your “main body” fraction. You will see temps between 190-220C during this fraction. Continue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed. The final “tails” fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The “tails” fraction has an obvious color change and will be darker than the “main body” fraction. You will see temps between 200-250C during this fraction. As fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well. Once the process is complete, stop heat, stop stir, and stop vacuum. Let atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation. ***Note: This entire setup will ship via motor freight.*** ***Note: All units are inspected for broken glass or parts before unit is shipped. If unit arrives damaged or glass is broken (this does not include minor imperfections or scuffs in glassware), Customer MUST contact BVV™ within 3 days of delivery to file a claim and receive a replacement part. If customer DOES NOT contact BVV™ within 3 days of delivery responsibility for replacement parts falls on the customer and they must pay for replacement pieces.*** ***Glassware Safety Disclaimer: BVV™ is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.***
$7,630.89
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2L Short Path Distillation Kit
Short Path Distillation Setup Short path distillation is used for compounds that are not stable at high temperatures. It can also be used to purify small amounts of a compound. For those new to this type of distillation, our Short Path Kit includes everything you will need as you get started. All stands, clamps, clips, and tubing are included, which means it’s ready to start working straight out of the box. The cold trap, cow and vacuum grease can all be customized to meet your needs. The 2L Distillation Kit builds upon the same principal as the 1L Distillation Kit, giving users an easy to use system that will get them up and running at an affordable price. It includes all stands, clamps, clips, and tubing needed to begin distilling immediately. This Kit Does NOT include a vacuum pump or circulator. Please see the below recommendations for both as well as recommended add-ons. Or check out our 2L Standard Distillation Turnkey Setup which includes vacuum pump and circulator. Crossbar pictured is not included. We recommend purchasing multiple lab stands to accommodate your specific needs. Recommended Vacuum Pumps: Pro Series 5.6CFM Corrosion Resistant Two Stage Vacuum Pump (recommended option) Just Better 6 CFM 2 Stage Deep Vacuum Pump (economy option) Best Value Vacs VE280 9CFM Two Stage Vacuum Pump (economy option) Recommended Circulators: Polyscience 7 Liter MX Heated Circulator (economy option) Polyscience 7 Liter MX Refrigerated Circulator (premium option with chilling capability) Recommended Add-Ons: Glass Dewar Style Cold Trap (recommended cold trap) Bullseye Precison Vacuum Gauge (premium vacuum gauge for measuring depth) CT40 or CT80 Electronic Cold Trap (electronic cold trap, dry ice replacement) Short Path Distillation Kit Specifications: Boiling Flask Size: 2L Recieving Flask Size: 250ml Batch Capacity approximate: 2L = 400-1000 grams Run time: 4 to 8 hours dependent upon material composition and throughput Distillation Temperature Range: 140-250C (Do not exceed 250C) Recommended Condenser Temperature: 40-50C This Kit Comes Standard With The Following: Glass Components: 2L 2-Neck Boiling Flask Short Path Head Triple Neck Cow 3x 250mL Single Neck Receiving Flask 1/8" 14/20 PTFE Thermometer Adapter 1/4" 24/40 PTFE Thermometer Adapter 120mm Glass Funnel Accessories: Magnetic PTFE Stirring Bar Retriever 5 Pack of Metal Keck Clips Dow Corning High Vacuum Silicone Grease Tripod Stand 2L Digital Heating and Stirring Mantle 3 Finger Clamp Adjustable 0-70mm 6" x 6" Scissor Jack 250-500ml Cork Stand 10ft of Vacuum Hose 10ft of Chiller Hose 1/4" Vacuum Manifold Traceable Kangaroo Thermometer - Digital 10 Pack of Adjustable Stainless Steel Tubing Clamps Fiberglass Insulation Rope 10 Feet 1.5 Gallon Cold Trap (2QT Tank) Dry Ice, Liquid Nitrogen w/ 2x 1/4" Barb Adapters Distillation Quick Start Guide This guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs. Before beginning distillation, ensure the following steps have been taken: Vacuum Pump is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed. All glass components are in good working order and ready to be assembled A winterization and degassing procedure has been done to prepare oil for distillation The unit's max internal temperature cannot exceed 380C. The recommended max set temperature should not exceed 250C Once all three of these steps have been completed, you are ready to begin distilling. Begin by placing stir bar in boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer. Assemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware Attach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation. Connect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system. Connect receiving cow to cold trap. Connect cold trap to manifold. Connect vacuum gauge to manifold. At this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process. Turn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability. Start stir slower and increase speed with temperature. Once you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C. You will see your first fraction somewhere between 180C and 190C or slightly before. This is the “heads” fraction. You will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to “self-clean” the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your “main body” fraction. You will see temps between 190-220C during this fraction. Continue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed. The final “tails” fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The “tails” fraction has an obvious color change and will be darker than the “main body” fraction. You will see temps between 200-250C during this fraction. As fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well. Once process is complete, stop heat, stop stir, and stop vacuum. Let atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation. Learn more about short path distillation components and FAQs with this distillation guide. *Notice to Customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. BVV™ is not responsible for the failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail, which can cause bodily harm or damage to the surrounding area.
$1,768.98
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Diamond Sauce Separator for 1.9 ft³ Ovens and Larger
BVV Diamond Sauce Separator The BVV diamond sauce separator is a good compliment to any diamond miner. With this vessel you can easily strain and separate your diamonds from the sauce using the internal basket. You can clean your diamonds like never before with less work. DSS-9 12.25" Exact Height (Fits 1.9 ft³ Vacuum Ovens) 6" Deep Basket (100 micron mesh Dutch Weave) 3"x9" Main Body Spool DSS-12 15.25" Exact Height (Fits larger than 1.9 ft³ Vacuum Ovens) 9" Deep Basket (100 micron mesh Dutch Weave) 3"x12" Main Body Spool Replacement Top Gasket around the basket can be found Here.
$221.99 - $249.74
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160L Centrifuge Bags
This nylon bag is designed to fit in our BVV brand centrifuges to contain material and be easily swappable after runs to speed up processing times. These bags come with 2 zippers and come in 1, 10, 50, 100, and 200 micron filtration levels. For use with 160L Centrifuges Appx. Size : 31.25" Diameter x 13" Height Specifications SKU Appx. Diameter In. Appx. Height in. CFB-45L-XXX 17.5" 11.75" CFB-160L-XXX 32.25" 13" CFB-280L-XXX 39.25" 14" CFB-475L-XXX 47.25" 16.75"
$259.45 - $485.60
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20L Digital Heating Mantle
20L DIGITAL HEATING AND STIRRING MANTLE Digital Heating and Stirring Mantles give the operator the most precise temperatures and readouts during distillations. These mantles autotune to specific user input to provide consistent results. Each mantle is equipped with large digital display that will give you readouts for both set temperature, actual temperature, and stirring speed. Each mantle also comes with a vertical brace bar and boss head as well as a temperature probe which plugs directly into the mantle. For first time use, the mantle should have an initial burn out done. This will burn off any residual oils used in the production of the insulation rope. The unit's max internal temperature cannot exceed 380C. The recommended max set temperature should not exceed 250C Specifications: Capacity: 20L (20000mL) Power Supply: 220V 60Hz (NEMA 6-20 plug) Adjustable Rotation Speed: 50-1800 RPM Motor Power: 40W, DC14-24V Heating Power 180-2200W Temperature Control Accuracy: +/- 1C Intelligent Temperature Control: Yes Temperature Range: RT+10-380C Insulation Material: Alkali-free Glass Fiber, temperature resistant up to 450C Shipping Dimensions: 25 x 25 x 18 in. Weight: 35 lbs
$1,942.41
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Dewar Glass Cold Trap
BVV™ Dewar Glass Cold Trap This dewar style glass is designed for maximum vapor condensation and it also has a 24/40 bottom joint and (2) GL-14 8mm Hose Barbs *Notice to customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement.
$346.86 $291.36
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Diamond Sauce Separator Basket Dutch Weave 100 Micron
BVV Diamond Sauce Separator Baskets for your Diamond Sauce Separator sold "A la Carte" The 6" long basket fit the BVV DSS-9 The 8.25" long basket fit the BVV DSS-12 The basket is a Dutch Weave all 304 Stainless Steel basket, and fits inside a 3" tri-clamp spool. The lip perfectly fits the tri clamp flange and works with our Dutch Weave product line gaskets.
$41.62 - $48.56
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Neocision P5V6 Neocision Distillation Head - USA Made
P5V6 Distillation Head P5V6 Distillation Head has 6 sets of vigreux in the distillation column with 34/45 lower joint and 24/40 upper and side joints and includes GL-14 barb connections. MADE IN THE USA Designed for 5 Liter Flasks Set of 6 vigreux to allow for packing media Larger vacuum jacket allows for less heat loss during distillations Larger vapor path to allow for gas/vapor phase flow Increased internal diameter for faster, more efficient fractioning as well as packing and unpacking of media Increased condenser length and diameter for more efficient condensation of vapor with zero clogging *Notice to customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. **Glassware Safety Disclaimer: BVV™ is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.**
$763.09
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2L Short Path Distillation Kit with P2 Distillation Head
2L Short Path Distillation Kit with P2 Distillation Head The 2L Distillation Kit w/ P2 Distillation Head includes everything needed to perform distillation excluding the vacuum pump and chiller. This kit features our USA made P2 Distillation Head as well as USA made glass. It is designed with ease of use in mind and includes the highest quality components to ensure results are repeatable time and again. **This Kit Does NOT include a vacuum pump or circulator. Please see the below recommendations for both as well as recommended add-ons. Or check out our 2L Premium Turnkey Setup which includes vacuum pump and circulator.** Crossbar pictured is not included. We recommend purchasing multiple lab stands to accomodate your specific needs. Recommended Vacuum Pumps: Pro Series 5.6CFM Corrosion Resistant Two Stage Vacuum Pump (recommended option) Just Better 6 CFM 2 Stage Deep Vacuum Pump (USA made economy option) Welch 1400 DuoSeal 0.9 cfm 0.1 Micron Belt Drive Dual-Stage Pump Recommended Circulators: Polyscience 7 Liter MX Heated Circulator (economy option) Polyscience 7 Liter MX Refrigerated Circulator (premium option with chilling capability) Recommended Add-Ons: Glass Dewar Style Cold Trap (recommended cold trap) Bullseye Precison Vacuum Gauge (premium vacuum gauge for measuring depth) CT40 or CT80 Electronic Cold Trap (electronic cold trap, dry ice replacement) J-KEM Digital Vapor Temp Monitor (digital vapor temp monitor with data-logging capabilities) Specifications: Boiling Flask Size: 2L Receveiving Flask Size: 250mL Batch Capacity approximate: 2L = 400-1000 grams Run time: 4 to 8 hours dependent upon material composition and throughput Distillation Temperature Range: 140-250C (Do not exceed 250C) Recommended Condenser Temperature: 40-50C This Kit Includes: Glass components: 2L USA Made 2-Neck Boiling Flask P2 USA Made Distillation Head Triple Neck Cow 3x 250mL Receiving Flask 2x 24/40 Chemglass Thermometer Inlet Adapter 120mm Glass Funnel Accessories: Magnetic PTFE Stirring Bar Retriever 5 Pack of Metal Keck Clips Dow Corning High Vacuum Silicone Grease Tripod Stand 2L Digital Heating and Stirring Mantle 3 Finger Clamp Adjustable 0-70mm 6" x 6" Scissor Jack 250-500ml Cork Stand 10ft of Vacuum Hose 10ft of Chiller Hose 1/4" Vacuum Manifold Traceable Kangaroo Thermometer - Digital 10 Pack of Adjustable Stainless Steel Tubing Clamps Fiberglass Insulation Rope 10 Feet 1.5 Gallon Cold Trap (2QT Tank) Dry Ice, Liquid Nitrogen w/ 2x 1/4" Barb Adapters Distillation Quick Start Guide This guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs, Before beginning distillation, ensure the following steps have been taken: Vacuum Pump is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed. All glass components are in good working order and ready to be assembled A winterization and degassing procedure has been done to prepare oil for distillation The unit's max internal temperature cannot exceed 380C. The recommended max set temperature should not exceed 250C Once all three of these steps have been completed, you are ready to begin distilling. Begin by placing stir bar in boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer. Assemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware Attach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation. Connect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system. Connect receiving cow to cold trap. Connect cold trap to manifold. Connect vacuum gauge to manifold. At this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process. Turn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability. Start stir slower and increase speed with temperature. Once you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C. You will see your first fraction somewhere between 180C and 190C or slightly before. This is the “heads” fraction. You will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to “self-clean” the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your “main body” fraction. You will see temps between 190-220C during this fraction. Continue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed. The final “tails” fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The “tails” fraction has an obvious color change and will be darker than the “main body” fraction. You will see temps between 200-250C during this fraction. As fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well. Once process is complete, stop heat, stop stir, and stop vacuum. Let atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation. *Notice to Customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. BVV™ is not responsible for the failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail, which can cause bodily harm or damage to the surrounding area.
$3,052.35
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280L Centrifuge Bags
This nylon bag is designed to fit in our BVV brand centrifuges to contain material and be easily swappable after runs to speed up processing times. These bags come with 2 zippers and come in 1, 10, 50, 100, and 200 micron filtration levels. For use with 280L Centrifuges Appx. Size : 39.25" Diameter x 14" Height Specifications SKU Appx. Diameter In. Appx. Height in. CFB-45L-XXX 17.5" 11.75" CFB-160L-XXX 32.25" 13" CFB-280L-XXX 39.25" 14" CFB-475L-XXX 47.25" 16.75"
$221.99 - $577.17
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Color Remediation Column CRC w/ Bypass
Color Remediation Column w/ Bypass The CRC is a secondary column used as a filtration cartridge for hydrocarbon and ethanol extraction systems. Filter medias are packed in the column above a triple filtration stack, which aids in the removal of impurities from extracted oils. The CRC features a bypass path, allowing the operator to skip the column in case of a clog. The color remediation process is made simple by bundling the cartridge with the needed filter medias. We have paired the unit with suggested media, supplied in the proper ratio, and a standard operating procedure. The included procedure takes all the guesswork out of filtration, delivering the desired results the first try. Our CRC comes available with 1/4",3/8", and 1/2" MJIC connections, your choice of a 3",4", and 6" diameter spool with a 12" height, and rack mounting brackets standard to accommodate systems of any size. This Kit Includes: Color Remediation Column Rack Mounting Brackets 100 pack of 8 and 20-micron filter papers 1000g of Activated Alumina 1000g of Silica 60A 1000g of Pure-Flo® B80 (81, 5000, 6000 or Color Bleach)*Substitutes 1000g of Celite®545 Instruction Manual
$1,179.32 - $1,873.04
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P2 Distillation Head - USA Made
P2 Distillation Head P2 Packable Distillation Head with 24/40 Joints. Includes GL-14 Barb Connections. Recommended packing media: Raschig Rings, Porcelain Berl Saddles, Glass Beads, Pro-Pak, or Stainless Steel Wool. Key Features: MADE IN THE USA Designed for 1 & 2 Liter Flasks Single set of lowered vigreaux to allow for packing media Larger vacuum jacket allows for less heat loss during distillations Larger vapor path to allow for gas/vapor phase flow Increased internal diameter for faster, more efficient fractioning as well as packing and unpacking of media Increased condenser length and diameter for more efficient condensation of vapor with zero clogging *Notice to customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. **Glassware Safety Disclaimer: BVV™ is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.**
$832.46
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2L Premium Short Path Distillation Turnkey Setup with P2 Distillation Head
2L Premium Short Path Distillation Turnkey Setup with P2 Distillation Head The 2L Premium Distillation Turnkey Setup features our 2L Distillation Kit with P2 Distillation Head and USA made glass. Every component in this turnkey is made for precision, throughput, and repeatable results. Also included is our Pro Series 11.3CFM Corrosion Resistant Two Stage Vacuum Pump giving you extreme power and depth with long lifespan, the Bullseye Precision Vacuum Gauge from Digivac which is the most rugged and dependable vacuum gauge on the market, and a Polyscience 7L MX Heated Circulator for maximum condensation of vapors. You will also receive a Dewar Style Glass Cold Trap to keep all volatiles and solvents out of your vacuum system. This Turnkey Setup gives you everything needed to perform distillation at the highest level. The Premium Turnkey Kit Includes: 2L Distillation Kit w/ P2 Distillation Head KF-25 x 1/4" Barb Adapter Dewar Style Glass Cold Trap Bullseye precision Vacuum Gauge Polyscience 7L MX Heated Circulator Pro Series 14.1CFM Corrosion Resistant Two Stage Vacuum Pump Distillation Quick Start Guide This guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs, Before beginning distillation, ensure the following steps have been taken: Vacuum Pump is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed. All glass components are in good working order and ready to be assembled A winterization and degassing procedure has been done to prepare oil for distillation Once all three of these steps have been completed, you are ready to begin distilling. Begin by placing stir bar in boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer. Assemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware Attach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation. Connect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system. Connect receiving cow to cold trap. Connect cold trap to manifold. Connect vacuum gauge to manifold. At this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process. Turn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability. Start stir slower and increase speed with temperature. Once you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C. You will see your first fraction somewhere between 180C and 190C or slightly before. This is the “heads” fraction. You will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to “self-clean” the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your “main body” fraction. You will see temps between 190-220C during this fraction. Continue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed. The final “tails” fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The “tails” fraction has an obvious color change and will be darker than the “main body” fraction. You will see temps between 200-250C during this fraction. As fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well. Once the process is complete, stop heat, stop stir, and stop vacuum. Let the atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation. ***Note: This entire setup will ship via motor freight.*** ***Note: All units are inspected for broken glass or parts before unit is shipped. If unit arrives damaged or glass is broken (this does not include minor imperfections or scuffs in glassware), Customer MUST contact BVV™ within 3 days of delivery to file a claim and receive a replacement part. If customer DOES NOT contact BVV™ within 3 days of delivery responsibility for replacement parts falls on the customer and they must pay for replacement pieces.*** ***Glassware Safety Disclaimer: BVV™ is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.***
$8,324.60 - $10,613.87
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5L Short Path Distillation Kit with P5 Distillation Head
5L Short Path Distillation Kit with P5 Distillation Head This unit carries a 2 day lead time. The 5L Distillation Kit includes everything needed to perform distillation excluding the vacuum pump and chiller. This kit features our USA made P5 Distillation Head, as well as USA, made glass. This Kit is designed for high volume production with the highest quality components for precise, repeatable results time and again. This Kit Does NOT include a vacuum pump or chiller. Please see the below recommendations for both as well as recommended add-ons. Recommended Vacuum Pumps: Pro Series 11.3CFM Corrosion Resistant Two Stage Vacuum Pump (recommended option) Just Better 6 CFM 2 Stage Deep Vacuum Pump (economy option) Recommended Chillers: Polyscience 7 Liter MX Heated Circulator (economy option) Polyscience 7 Liter Refrigerated Circulator (premium option with chilling capability) Recommended Add-Ons: Bullseye Precision Vacuum Gauge (premium vacuum gauge for measuing depth) CT40 or CT80 Electronic Cold Trap (electronic cold trap, dry ice replacement) J-KEM Digital Vapor Temp Monitor (digital vapor temp monitor with data-logging capabilites) Specifications: Boiling Flask Size: 5L Receiving Flask Size: 2x 500mL, 1000mL Batch Capacity approximate: 1000-2500 grams Run time: 4 to 8 hours dependent upon material composition and throughput Distillation Temperature Range: 140-250C (Do not exceed 250C) Recommended Condenser Temperature: 40-50C This Kit Includes: Glass components: 5L Boiling Flask P5V6 Distillation Head Triple Neck Cow 2x 500mL Receiving Flask 1L Receiving Flask 120mm Glass Funnel Dewar cold trap Accessories: PTFE Magnetic Stir Bar Retriever 5 Pack of Metal Keck Clips Dow Corning High Vacuum Silicone Grease Tripod Stand 5L Digital Heating and Stirring Mantle 3-Finger Adjustable Clamp 0-77mm 6" x 6" Scissor Jack 500-1000mL Cork Stand 2x 24/40 ChemglassPTFE Thermometer Inlet Adapter 10ft of Gum Rubber Vacuum Hose 10ft of Silicone Chiller Hose 1/4" Vacuum Manifold Traceable Kangaroo Thermometer - Digital 10 Pack of Adjustable Stainless Steel Tubing Clamps Fiberglass Insulation Rope 10 Feet Distillation Quick Start Guide This guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs, Before beginning distillation, ensure the following steps have been taken: Vacuum Pump is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed. All glass components are in good working order and ready to be assembled A winterization and degassing procedure has been done to prepare oil for distillation The unit's max internal temperature cannot exceed 380C. The recommended max set temperature should not exceed 250C Once all three of these steps have been completed, you are ready to begin distilling. Begin by placing stir bar in boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer. Assemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware Attach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation. Connect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system. Connect receiving cow to cold trap. Connect cold trap to manifold. Connect vacuum gauge to manifold. At this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process. Turn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability. Start stir slower and increase speed with temperature. Once you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C. You will see your first fraction somewhere between 180C and 190C or slightly before. This is the “heads” fraction. You will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to “self-clean” the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your “main body” fraction. You will see temps between 190-220C during this fraction. Continue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed. The final “tails” fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The “tails” fraction has an obvious color change and will be darker than the “main body” fraction. You will see temps between 200-250C during this fraction. As fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well. Once process is complete, stop heat, stop stir, and stop vacuum. Let atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation. *Notice to Customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. BVV™ is not responsible for the failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail, which can cause bodily harm or damage to the surrounding area.
$3,052.35
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Neocision 20L Neocision Dual Short Path Distillation Turnkey System
20L Neocision Dual Short Path Distillation Turnkey System This unit carries a 2 day lead time. (Note: This kit does NOT include the stainless steel table.) The 20L Neocision Distillation Turnkey Setup features our Dual USA made P10V6 Distillation Heads. Every component in this distillation kit is made for precision, throughput, and repeatable results. You will also receive Dual Dewar Style Ribbed Glass Cold Traps to keep all volatiles and solvents out of your vacuum system. This Turnkey Setup gives you everything needed to perform distillation at the highest level. The 20L Neo Kit Includes: 20L Neocision Kit with glassware, labware, and Dual P10V6 Distillation Heads. BVV 15 Liter Advanced Digital Heated Circulator Choice of Vacuum Pump KF-25 Bellow Y Manifold Dual Ribbed Dewar Style Glass Cold Trap Non-Mercury Glass Thermometers 20L Digital Heating and Stirring Mantle Distillation Quick Start Guide This guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs, Before beginning distillation, ensure the following steps have been taken: Vacuum Pump is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed. All glass components are in good working order and ready to be assembled A winterization and degassing procedure has been done to prepare oil for distillation The unit's max internal temperature cannot exceed 380C. The recommended max set temperature should not exceed 250C Once all three of these steps have been completed, you are ready to begin distilling. Begin by placing stir bar in the boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer. Assemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware Attach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation. Connect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system. Connect receiving cow to cold trap. Connect cold trap to manifold. Connect vacuum gauge to manifold. At this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process. Turn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability. Start stir slower and increase speed with temperature. Once you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C. You will see your first fraction somewhere between 180C and 190C or slightly before. This is the “heads” fraction. You will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to “self-clean” the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your “main body” fraction. You will see temps between 190-220C during this fraction. Continue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed. The final “tails” fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The “tails” fraction has an obvious color change and will be darker than the “main body” fraction. You will see temps between 200-250C during this fraction. As fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well. Once process is complete, stop heat, stop stir, and stop vacuum. Let atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation. ***Note: This entire setup will ship via motor freight.*** *Notice to Customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. BVV™ is not responsible for the failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail, which can cause bodily harm or damage to the surrounding area.
$18,036.64 - $23,586.38
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ChemTek ChemTek Large Fuge Bags - 50 Pack
ChemTek Large Fuge Bags - 50 Pack Centrifuge bags used for separations. Specifications: Size: 50-Pack Dimensions: H: 7” W: 6.5” Micron Size: 25 Micron Material: Food Grade Nylon
$69.37
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