Distillation
1L Standard Distillation Turnkey Setup
1L Standard Distillation Turnkey Setup The Standard Distillation Turnkey Setup includes all the components necessary to successfully perform distillation at an entry level price point. The Standard Turnkey Setup Includes: 1L Distillation Kit 1/4" Flare x 1/4" Barb Adapter BVV™ 5L Heated Circulator BVV™ V9D 9CFM Two Stage Vacuum Pump Distillation Quick Start Guide This guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs, Before beginning distillation, ensure the following steps have been taken: Vacuum Pump is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed. All glass components are in good working order and ready to be assembled A winterization and degassing procedure has been done to prepare oil for distillation Once all three of these steps have been completed, you are ready to begin distilling. Begin by placing stir bar in boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer. Assemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware Attach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation. Connect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system. Connect receiving cow to cold trap. Connect cold trap to manifold. Connect vacuum gauge to manifold. At this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process. Turn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability. Start stir slower and increase speed with temperature. Once you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C. You will see your first fraction somewhere between 180C and 190C or slightly before. This is the “heads” fraction. You will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to “self-clean” the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your “main body” fraction. You will see temps between 190-220C during this fraction. Continue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed. The final “tails” fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The “tails” fraction has an obvious color change and will be darker than the “main body” fraction. You will see temps between 200-250C during this fraction. As fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well. Once process is complete, stop heat, stop stir, and stop vacuum. Let atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation. ***Note: This entire setup will ship via motor freight.*** *Notice to Customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. BVV™ is not responsible for the failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail, which can cause bodily harm or damage to the surrounding area.
$2,974.85 - $3,329.00
1L Distillation Kit
1L Distillation Kit The 1L Distillation Kit is a simple, easy to use system designed for small personal use. It includes all stands, clamps, clips, and tubing needed to begin distilling immediately. This Kit Does NOT include a vacuum pump or circulator. Please see the below recommendations for both as well as recommended add-ons. Or check out our 1L Standard Distillation Turnkey Setup which includes vacuum pump and circulator. Recommended Vacuum Pumps: Pro Series 5.6CFM Corrosion Resistant Two Stage Vacuum Pump (premium option) Just Better 6 CFM 2 Stage Deep Vacuum Pump (USA made economy option) Best Value Vacs VE280 9CFM Two Stage Vacuum Pump (economy option) Recommended Circulator: Polyscience 7 Liter MX Heated Circulator (economy option) Polyscience 7 Liter MX Refrigerated Circulator (premium option with chilling capability) Recommended Add-Ons: Glass Dewar Style Cold Trap (recommended cold trap) Bullseye Precison Vacuum Gauge (premium vacuum gauge for measuring depth) CT40 or CT80 Electronic Cold Trap (electronic cold trap, dry ice replacement) Specifications: Boiling Flask Size: 1L Receveiving Flask Size: 250ml Batch Capacity approximate: 200-400 grams Run time: 4 to 8 hours dependent upon material composition and throughput Distillation Temperature Range: 140-250C (Do not exceed 250C) Recommended Condenser Temperature: 40-50C This Kit Includes: Glass Components: 1L 2-Neck Boiling Flask Short Path Head Triple Neck Cow Receiving Flask 3x 250ml Single Neck Round Bottom Flask 14/20 Thermometer Adapter 24/40 Thermometer Adapter 120mm Glass Funnel 14/20 Stopper 24/40 Stopper Accessories: Magnetic PTFE Stirring Bar Retriever 5 Pack of Metal Keck Clips Dow Corning High Vacuum Silicone Grease Tripod Stand 1L Analog Heating and Stirring Mantle 3 Finger Clamp Adjustable 0-70mm Boss Head -13mm 6" x 6" Scissor Jack 250-500ml Cork Stand 10ft of Vacuum Hose 10ft of Chiller Hose 1/4" Vacuum Manifold Traceable Kangaroo Thermometer - Digital 10 Pack of Adjustable Stainless Steel Tubing Clamps Fiberglass Insulation Rope 10 Feet 1.5 Gallon Cold Trap (2QT Tank) Dry Ice, Liquid Nitrogen w/ 2x 1/4" Barb Adapters Distillation Quick Start Guide This guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs, Before beginning distillation, ensure the following steps have been taken: Vacuum Pump is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed. All glass components are in good working order and ready to be assembled A winterization and degassing procedure has been done to prepare oil for distillation Once all three of these steps have been completed, you are ready to begin distilling. Begin by placing stir bar in boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer. Assemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware Attach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation. Connect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system. Connect receiving cow to cold trap. Connect cold trap to manifold. Connect vacuum gauge to manifold. At this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process. Turn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability. Start stir slower and increase speed with temperature. Once you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C. You will see your first fraction somewhere between 180C and 190C or slightly before. This is the “heads” fraction. You will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to “self-clean” the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your “main body” fraction. You will see temps between 190-220C during this fraction. Continue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed. The final “tails” fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The “tails” fraction has an obvious color change and will be darker than the “main body” fraction. You will see temps between 200-250C during this fraction. As fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well. Once process is complete, stop heat, stop stir, and stop vacuum. Let atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation. *Notice to Customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. BVV™ is not responsible for the failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail, which can cause bodily harm or damage to the surrounding area.
$1,274.94
2L Short Path Distillation Kit
Short Path Distillation Setup Short path distillation is used for compounds that are not stable at high temperatures. It can also be used to purify small amounts of a compound. For those new to this type of distillation, our Short Path Kit includes everything you will need as you get started. All stands, clamps, clips, and tubing are included, which means it’s ready to start working straight out of the box. The cold trap, cow and vacuum grease can all be customized to meet your needs. The 2L Distillation Kit builds upon the same principal as the 1L Distillation Kit, giving users an easy to use system that will get them up and running at an affordable price. It includes all stands, clamps, clips, and tubing needed to begin distilling immediately. This Kit Does NOT include a vacuum pump or circulator. Please see the below recommendations for both as well as recommended add-ons. Or check out our 2L Standard Distillation Turnkey Setup which includes vacuum pump and circulator. Crossbar pictured is not included. We recommend purchasing multiple lab stands to accommodate your specific needs. Recommended Vacuum Pumps: Pro Series 5.6CFM Corrosion Resistant Two Stage Vacuum Pump (recommended option) Just Better 6 CFM 2 Stage Deep Vacuum Pump (economy option) Best Value Vacs VE280 9CFM Two Stage Vacuum Pump (economy option) Recommended Circulators: Polyscience 7 Liter MX Heated Circulator (economy option) Polyscience 7 Liter MX Refrigerated Circulator (premium option with chilling capability) Recommended Add-Ons: Glass Dewar Style Cold Trap (recommended cold trap) Bullseye Precison Vacuum Gauge (premium vacuum gauge for measuring depth) CT40 or CT80 Electronic Cold Trap (electronic cold trap, dry ice replacement) Short Path Distillation Kit Specifications: Boiling Flask Size: 2L Recieving Flask Size: 250ml Batch Capacity approximate: 2L = 400-1000 grams Run time: 4 to 8 hours dependent upon material composition and throughput Distillation Temperature Range: 140-250C (Do not exceed 250C) Recommended Condenser Temperature: 40-50C This Kit Comes Standard With The Following: Glass Components: 2L 2-Neck Boiling Flask Short Path Head Triple Neck Cow 3x 250mL Single Neck Receiving Flask 1/8" 14/20 PTFE Thermometer Adapter 1/4" 24/40 PTFE Thermometer Adapter 120mm Glass Funnel Accessories: Magnetic PTFE Stirring Bar Retriever 5 Pack of Metal Keck Clips Dow Corning High Vacuum Silicone Grease Tripod Stand 2L Digital Heating and Stirring Mantle 3 Finger Clamp Adjustable 0-70mm 6" x 6" Scissor Jack 250-500ml Cork Stand 10ft of Vacuum Hose 10ft of Chiller Hose 1/4" Vacuum Manifold Traceable Kangaroo Thermometer - Digital 10 Pack of Adjustable Stainless Steel Tubing Clamps Fiberglass Insulation Rope 10 Feet 1.5 Gallon Cold Trap (2QT Tank) Dry Ice, Liquid Nitrogen w/ 2x 1/4" Barb Adapters Distillation Quick Start Guide This guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs. Before beginning distillation, ensure the following steps have been taken: Vacuum Pump is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed. All glass components are in good working order and ready to be assembled A winterization and degassing procedure has been done to prepare oil for distillation The unit's max internal temperature cannot exceed 380C. The recommended max set temperature should not exceed 250C Once all three of these steps have been completed, you are ready to begin distilling. Begin by placing stir bar in boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer. Assemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware Attach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation. Connect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system. Connect receiving cow to cold trap. Connect cold trap to manifold. Connect vacuum gauge to manifold. At this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process. Turn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability. Start stir slower and increase speed with temperature. Once you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C. You will see your first fraction somewhere between 180C and 190C or slightly before. This is the “heads” fraction. You will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to “self-clean” the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your “main body” fraction. You will see temps between 190-220C during this fraction. Continue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed. The final “tails” fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The “tails” fraction has an obvious color change and will be darker than the “main body” fraction. You will see temps between 200-250C during this fraction. As fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well. Once process is complete, stop heat, stop stir, and stop vacuum. Let atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation. Learn more about short path distillation components and FAQs with this distillation guide. *Notice to Customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. BVV™ is not responsible for the failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail, which can cause bodily harm or damage to the surrounding area.
$1,806.16
2L Short Path Parts Kit with Dry Ice Cold Trap
2L Short Path Parts Kit with Dry Ice Cold Trap This kit includes all the parts and fixturing to build a distillation setup with a 2L boiling flask. No heating or cooling equipment is included.
$1,062.45
2L Full Bore Short Path Distillation Turnkey Kit with P2 Distillation Head
2L Full Bore Short Path Distillation Turnkey Kit with P2 Distillation Head This unit carries a 2-day lead time The 2L Full Bore Short Path Distillation Turnkey Kit with P2 Distillation Head is a great setup for smaller scale processors that want a budget friendly system without sacrificing quality on the main components that make a short path great. We understand that as an operator our customers want to be able to start their system and operate in ideal conditions run after run. That is why we paired a full-bore setup with a 14.1CFM pump that will assure the lowest vacuum depth will be pulled every time. Main components such as the distillation head, vacuum valve adapter, and cold trap are all American blown glass. These components allow us to present this system that will repeat in performance time after time. For a in depth analysis of this system please view the following videos. Here you will see the system setup, component explanation, and even see it perform in a first and second distillation pass. These runs were all performed in our lab and the data was used to help fine tune the system. The unit's max internal temperature cannot exceed 380C. The recommended max set temperature should not exceed 250C Video 1 - Setup and Component Explanation Video 2 - Setup Addendum Video 3 - Fist pass Distillation Video 4 - Second Pass Distillation The 2L Full Bore Short Path Distillation Turnkey Kit with P2 Distillation Head Includes: 1 First Pass Distillation Operating Procedure 1 P2 Distillation Kit 1 2L Double Neck Boiling Flask 1 Full Bore Vacuum Valve Adapter 1 BVV MP7H Heater 1 2L Heating Mantle 1 Ribbed Glass Cold Trap 1 Bullseye Precision Vacuum Gauge 1 BVV Pro Series 14.1CFM Rotary Vane Pump (Comes filled with oil. Recommend purchasing additional Ultra 19 Vacuum Pump Oil. SKU: INLAND19-ULTRS-1G) 1 Oil Mist Filter Trap for Rotary Vane Pump 1 24/40 250ml Single Neck Round Bottom Flask 3 24/40 500ml Single Neck Round Bottom Flask 1 24/40 Glass Funnel 1 Vacuum Manifold for Rotary Vane Pump 1 1 Meter Bellow Hose 1 PTFE Magnetic Stirring Bar Retriever 1 24/40 Metal Keck Clip 6 24/40 Plastic Keck Clips 3 250-500ml Cork Stands 2 Chain Clamps 1 Boss Head with 3 Finger Clamp 1 BVV Lab Stand 10 Fiber Glass Insulation Rope 1 Dow Corning High Vacuum Grease 1 10/30 Non-Mercury Glass Thermometers 1 24/40 – 10/30 Glass Adapter Bushing 1 24/40 – 1/8” Thermometer Adapter 1 24/40 Straight Adapter 2 6”x6” Scissor Jack 3 36” Threaded Lab Stand Rod 2 Gl14 – 8mm Barb 6 ¼” Silicone Tubing 2 PTFE Magnetic Stirring Bar 4 Hose Clamp with Butterfly Key ***Note: This entire setup will ship via motor freight.*** ***Note: All units are inspected for broken glass or parts before unit is shipped. If unit arrives damaged or glass is broken (this does not include minor imperfections or scuffs in glassware), Customer MUST contact BVV™ within 3 days of delivery to file a claim and receive a replacement part. If customer DOES NOT contact BVV™ within 3 days of delivery responsibility for replacement parts falls on the customer and they must pay for replacement pieces.*** ***Glassware Safety Disclaimer: BVV™ is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.***
$10,624.46
2L Short Path Distillation Kit with P2 Distillation Head
2L Short Path Distillation Kit with P2 Distillation Head The 2L Distillation Kit w/ P2 Distillation Head includes everything needed to perform distillation excluding the vacuum pump and chiller. This kit features our USA made P2 Distillation Head as well as USA made glass. It is designed with ease of use in mind and includes the highest quality components to ensure results are repeatable time and again. **This Kit Does NOT include a vacuum pump or circulator. Please see the below recommendations for both as well as recommended add-ons. Or check out our 2L Premium Turnkey Setup which includes vacuum pump and circulator.** Crossbar pictured is not included. We recommend purchasing multiple lab stands to accomodate your specific needs. Recommended Vacuum Pumps: Pro Series 5.6CFM Corrosion Resistant Two Stage Vacuum Pump (recommended option) Just Better 6 CFM 2 Stage Deep Vacuum Pump (USA made economy option) Welch 1400 DuoSeal 0.9 cfm 0.1 Micron Belt Drive Dual-Stage Pump Recommended Circulators: Polyscience 7 Liter MX Heated Circulator (economy option) Polyscience 7 Liter MX Refrigerated Circulator (premium option with chilling capability) Recommended Add-Ons: Glass Dewar Style Cold Trap (recommended cold trap) Bullseye Precison Vacuum Gauge (premium vacuum gauge for measuring depth) CT40 or CT80 Electronic Cold Trap (electronic cold trap, dry ice replacement) J-KEM Digital Vapor Temp Monitor (digital vapor temp monitor with data-logging capabilities) Specifications: Boiling Flask Size: 2L Receveiving Flask Size: 250mL Batch Capacity approximate: 2L = 400-1000 grams Run time: 4 to 8 hours dependent upon material composition and throughput Distillation Temperature Range: 140-250C (Do not exceed 250C) Recommended Condenser Temperature: 40-50C This Kit Includes: Glass components: 2L USA Made 2-Neck Boiling Flask P2 USA Made Distillation Head Triple Neck Cow 3x 250mL Receiving Flask 2x 24/40 Chemglass Thermometer Inlet Adapter 120mm Glass Funnel Accessories: Magnetic PTFE Stirring Bar Retriever 5 Pack of Metal Keck Clips Dow Corning High Vacuum Silicone Grease Tripod Stand 2L Digital Heating and Stirring Mantle 3 Finger Clamp Adjustable 0-70mm 6" x 6" Scissor Jack 250-500ml Cork Stand 10ft of Vacuum Hose 10ft of Chiller Hose 1/4" Vacuum Manifold Traceable Kangaroo Thermometer - Digital 10 Pack of Adjustable Stainless Steel Tubing Clamps Fiberglass Insulation Rope 10 Feet 1.5 Gallon Cold Trap (2QT Tank) Dry Ice, Liquid Nitrogen w/ 2x 1/4" Barb Adapters Distillation Quick Start Guide This guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs, Before beginning distillation, ensure the following steps have been taken: Vacuum Pump is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed. All glass components are in good working order and ready to be assembled A winterization and degassing procedure has been done to prepare oil for distillation The unit's max internal temperature cannot exceed 380C. The recommended max set temperature should not exceed 250C Once all three of these steps have been completed, you are ready to begin distilling. Begin by placing stir bar in boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer. Assemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware Attach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation. Connect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system. Connect receiving cow to cold trap. Connect cold trap to manifold. Connect vacuum gauge to manifold. At this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process. Turn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability. Start stir slower and increase speed with temperature. Once you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C. You will see your first fraction somewhere between 180C and 190C or slightly before. This is the “heads” fraction. You will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to “self-clean” the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your “main body” fraction. You will see temps between 190-220C during this fraction. Continue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed. The final “tails” fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The “tails” fraction has an obvious color change and will be darker than the “main body” fraction. You will see temps between 200-250C during this fraction. As fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well. Once process is complete, stop heat, stop stir, and stop vacuum. Let atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation. *Notice to Customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. BVV™ is not responsible for the failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail, which can cause bodily harm or damage to the surrounding area.
$3,116.51
2L Standard Short Path Distillation Turnkey Setup
2L Standard Short Path Distillation Turnkey Setup The Standard Distillation Turnkey Setup includes all the components necessary to successfully perform distillation at an entry-level price point. Crossbar pictured is not included. We recommend purchasing multiple lab stands to accommodate your specific needs. The Standard Turnkey Setup Includes: 2L Distillation Kit 1/4" Flare x 1/4" Barb Adapter BVV™ 5L Heated Circulator BVV™ V9D 9CFM Two Stage Vacuum Pump High quality and durable Borosilicate 3.3 glass Vacuum-jacketed distillation adapter 3-way cow adapter, accommodating up to 3 pcs of 500mL flasks GCT-01 cold trap guarding from damage of vapors Kangaroo Traceable Digital Thermometer Flexible Gum Rubber Vacuum Tubing and Silicone Tubing for Flow Distillation Quick Start Guide This guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs, Before beginning distillation, ensure the following steps have been taken: Vacuum Pump is in good working order. The pump should be run against the dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed. All glass components are in good working order and ready to be assembled A winterization and degassing procedure has been done to prepare oil for distillation The unit's max internal temperature cannot exceed 380C. The recommended max set temperature should not exceed 250C Once all three of these steps have been completed, you are ready to begin distilling. Begin by placing stir bar in boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer. Assemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware Attach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation. Connect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system. Connect receiving cow to cold trap. Connect cold trap to manifold. Connect vacuum gauge to manifold. At this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process. Turn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability. Start stir slower and increase speed with temperature. Once you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C. You will see your first fraction somewhere between 180C and 190C or slightly before. This is the “heads” fraction. You will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to “self-clean” the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your “main body” fraction. You will see temps between 190-220C during this fraction. Continue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed. The final “tails” fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The “tails” fraction has an obvious color change and will be darker than the “main body” fraction. You will see temps between 200-250C during this fraction. As fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well. Once the process is complete, stop heat, stop stir, and stop vacuum. Let the atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation. ***Note: This entire setup will ship via motor freight.*** *Notice to Customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. BVV™ is not responsible for the failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail, which can cause bodily harm or damage to the surrounding area.
$3,683.15
2L Premium Short Path Distillation Turnkey Setup with P2 Distillation Head
2L Premium Short Path Distillation Turnkey Setup with P2 Distillation Head The 2L Premium Distillation Turnkey Setup features our 2L Distillation Kit with P2 Distillation Head and USA made glass. Every component in this turnkey is made for precision, throughput, and repeatable results. Also included is our Pro Series 11.3CFM Corrosion Resistant Two Stage Vacuum Pump giving you extreme power and depth with long lifespan, the Bullseye Precision Vacuum Gauge from Digivac which is the most rugged and dependable vacuum gauge on the market, and a Polyscience 7L MX Heated Circulator for maximum condensation of vapors. You will also receive a Dewar Style Glass Cold Trap to keep all volatiles and solvents out of your vacuum system. This Turnkey Setup gives you everything needed to perform distillation at the highest level. The Premium Turnkey Kit Includes: 2L Distillation Kit w/ P2 Distillation Head KF-25 x 1/4" Barb Adapter Dewar Style Glass Cold Trap Bullseye precision Vacuum Gauge Polyscience 7L MX Heated Circulator Pro Series 14.1CFM Corrosion Resistant Two Stage Vacuum Pump Distillation Quick Start Guide This guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs, Before beginning distillation, ensure the following steps have been taken: Vacuum Pump is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed. All glass components are in good working order and ready to be assembled A winterization and degassing procedure has been done to prepare oil for distillation Once all three of these steps have been completed, you are ready to begin distilling. Begin by placing stir bar in boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer. Assemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware Attach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation. Connect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system. Connect receiving cow to cold trap. Connect cold trap to manifold. Connect vacuum gauge to manifold. At this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process. Turn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability. Start stir slower and increase speed with temperature. Once you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C. You will see your first fraction somewhere between 180C and 190C or slightly before. This is the “heads” fraction. You will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to “self-clean” the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your “main body” fraction. You will see temps between 190-220C during this fraction. Continue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed. The final “tails” fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The “tails” fraction has an obvious color change and will be darker than the “main body” fraction. You will see temps between 200-250C during this fraction. As fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well. Once the process is complete, stop heat, stop stir, and stop vacuum. Let the atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation. ***Note: This entire setup will ship via motor freight.*** ***Note: All units are inspected for broken glass or parts before unit is shipped. If unit arrives damaged or glass is broken (this does not include minor imperfections or scuffs in glassware), Customer MUST contact BVV™ within 3 days of delivery to file a claim and receive a replacement part. If customer DOES NOT contact BVV™ within 3 days of delivery responsibility for replacement parts falls on the customer and they must pay for replacement pieces.*** ***Glassware Safety Disclaimer: BVV™ is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.***
$8,499.57 - $10,836.95
5L Premium Short Path Distillation Turnkey Setup
5L Premium Distillation Kit This unit carries a 2 day lead time. The 5L Premium Short Path Distillation Turnkey Setup features our 5L Distillation Kit with P5 Distillation Head and USA made glass. Every component in this turnkey is made for precision, throughput, and repeatable results. Also included is our Pro Series 11.3CFM Corrosion Resistant Two Stage Vacuum Pump giving you extreme power and depth with a long lifespan, the Bullseye Precision Vacuum Gauge from Digivac which is the most rugged and dependable vacuum gauge on the market, and a BVV 19L Heated Circulator for maximum condensation of vapors. You will also receive a Dewar Style Glass Cold Trap to keep all volatiles and solvents out of your vacuum system. This Turnkey Setup gives you everything needed to perform distillation at the highest level. The Premium Short Path Distillation Turnkey Kit Includes: 5L Distillation Kit with P5 Distillation Head KF-25 x 1/4" Barb Adapter Dewar Style Glass Cold Trap Bullseye Precision Vacuum Gauge Polyscience 7L MX Heated Circulator Pro Series 14.1CFM Corrosion Resistant Two Stage Vacuum Pump Short Path Distillation Quick Start Guide This guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs, Before beginning distillation, ensure the following steps have been taken: Vacuum Pump is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed. All glass components are in good working order and ready to be assembled A winterization and degassing procedure has been done to prepare oil for distillation Once all three of these steps have been completed, you are ready to begin distilling. Begin by placing stir bar in boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer. Assemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware Attach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation. Connect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system. Connect receiving cow to cold trap. Connect cold trap to manifold. Connect vacuum gauge to manifold. At this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process. Turn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability. Start stir slower and increase speed with temperature. Once you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C. You will see your first fraction somewhere between 180C and 190C or slightly before. This is the “heads” fraction. You will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to “self-clean” the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your “main body” fraction. You will see temps between 190-220C during this fraction. Continue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed. The final “tails” fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The “tails” fraction has an obvious color change and will be darker than the “main body” fraction. You will see temps between 200-250C during this fraction. As fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well. Once the process is complete, stop heat, stop stir, and stop vacuum. Let atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation. ***Note: This entire setup will ship via motor freight.*** ***Note: All units are inspected for broken glass or parts before unit is shipped. If unit arrives damaged or glass is broken (this does not include minor imperfections or scuffs in glassware), Customer MUST contact BVV™ within 3 days of delivery to file a claim and receive a replacement part. If customer DOES NOT contact BVV™ within 3 days of delivery responsibility for replacement parts falls on the customer and they must pay for replacement pieces.*** ***Glassware Safety Disclaimer: BVV™ is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.***
$7,791.27
5L Short Path Distillation Kit with P5 Distillation Head
5L Short Path Distillation Kit with P5 Distillation Head This unit carries a 2 day lead time. The 5L Distillation Kit includes everything needed to perform distillation excluding the vacuum pump and chiller. This kit features our USA made P5 Distillation Head, as well as USA, made glass. This Kit is designed for high volume production with the highest quality components for precise, repeatable results time and again. This Kit Does NOT include a vacuum pump or chiller. Please see the below recommendations for both as well as recommended add-ons. Recommended Vacuum Pumps: Pro Series 11.3CFM Corrosion Resistant Two Stage Vacuum Pump (recommended option) Just Better 6 CFM 2 Stage Deep Vacuum Pump (economy option) Recommended Chillers: Polyscience 7 Liter MX Heated Circulator (economy option) Polyscience 7 Liter Refrigerated Circulator (premium option with chilling capability) Recommended Add-Ons: Glass Dewar Style Cold Trap (recommended cold trap) Bullseye Precision Vacuum Gauge (premium vacuum gauge for measuing depth) CT40 or CT80 Electronic Cold Trap (electronic cold trap, dry ice replacement) J-KEM Digital Vapor Temp Monitor (digital vapor temp monitor with data-logging capabilites) Specifications: Boiling Flask Size: 5L Receiving Flask Size: 2x 500mL, 1000mL Batch Capacity approximate: 1000-2500 grams Run time: 4 to 8 hours dependent upon material composition and throughput Distillation Temperature Range: 140-250C (Do not exceed 250C) Recommended Condenser Temperature: 40-50C This Kit Includes: Glass components: 5L Boiling Flask P5V6 Distillation Head Triple Neck Cow 2x 500mL Receiving Flask 1L Receiving Flask 120mm Glass Funnel Accessories: PTFE Magnetic Stir Bar Retriever 5 Pack of Metal Keck Clips Dow Corning High Vacuum Silicone Grease Tripod Stand 5L Digital Heating and Stirring Mantle 3-Finger Adjustable Clamp 0-77mm 6" x 6" Scissor Jack 500-1000mL Cork Stand 2x 24/40 ChemglassPTFE Thermometer Inlet Adapter 10ft of Gum Rubber Vacuum Hose 10ft of Silicone Chiller Hose 1/4" Vacuum Manifold Traceable Kangaroo Thermometer - Digital 10 Pack of Adjustable Stainless Steel Tubing Clamps Fiberglass Insulation Rope 10 Feet 1.5 Gallon Cold Trap (2QT Tank) Dry Ice, Liquid Nitrogen w/ 2x 1/4" Barb Adapters Distillation Quick Start Guide This guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs, Before beginning distillation, ensure the following steps have been taken: Vacuum Pump is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed. All glass components are in good working order and ready to be assembled A winterization and degassing procedure has been done to prepare oil for distillation The unit's max internal temperature cannot exceed 380C. The recommended max set temperature should not exceed 250C Once all three of these steps have been completed, you are ready to begin distilling. Begin by placing stir bar in boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer. Assemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware Attach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation. Connect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system. Connect receiving cow to cold trap. Connect cold trap to manifold. Connect vacuum gauge to manifold. At this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process. Turn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability. Start stir slower and increase speed with temperature. Once you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C. You will see your first fraction somewhere between 180C and 190C or slightly before. This is the “heads” fraction. You will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to “self-clean” the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your “main body” fraction. You will see temps between 190-220C during this fraction. Continue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed. The final “tails” fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The “tails” fraction has an obvious color change and will be darker than the “main body” fraction. You will see temps between 200-250C during this fraction. As fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well. Once process is complete, stop heat, stop stir, and stop vacuum. Let atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation. *Notice to Customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. BVV™ is not responsible for the failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail, which can cause bodily harm or damage to the surrounding area.
$3,116.51
5L Neocision Short Path Distillation Kit
5L Neocision Short Path Distillation Kit This unit carries a 2 day lead time. The 5L Neocision Short Path Distillation Kit features our 5L Distillation Kit with P5 Distillation Head and USA made glass. Every component in this turnkey is made for precision, throughput, and repeatable results. You will also receive a Dewar Style Glass Cold Trap to keep all volatiles and solvents out of your vacuum system. The Premium Turnkey Kit Includes: 5L Neocision Kit with P5 Distillation Head KF-25 x 1/4" Barb Adapter Dewar Style Glass Cold Trap Distillation Quick Start Guide This guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs, Before beginning distillation, ensure the following steps have been taken: Vacuum Pump is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed. All glass components are in good working order and ready to be assembled A winterization and degassing procedure has been done to prepare oil for distillation Once all three of these steps have been completed, you are ready to begin distilling. Begin by placing stir bar in boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer. Assemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware Attach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation. Connect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system. Connect receiving cow to cold trap. Connect cold trap to manifold. Connect vacuum gauge to manifold. At this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process. Turn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability. Start stir slower and increase speed with temperature. Once you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C. You will see your first fraction somewhere between 180C and 190C or slightly before. This is the “heads” fraction. You will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to “self-clean” the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your “main body” fraction. You will see temps between 190-220C during this fraction. Continue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed. The final “tails” fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The “tails” fraction has an obvious color change and will be darker than the “main body” fraction. You will see temps between 200-250C during this fraction. As fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well. Once process is complete, stop heat, stop stir, and stop vacuum. Let atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation. ***Note: This entire setup will ship via motor freight.*** *Notice to Customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. BVV™ is not responsible for the failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail, which can cause bodily harm or damage to the surrounding area.
$9,845.33
5L Neocision Short Path Distillation Turnkey Kit
5L Neocision Short Path Distillation Turnkey Kit This unit carries a 2 day lead time. The 5L Premium Distillation Turnkey Setup features our 5L Distillation Kit with P5 Distillation Head and USA made glass. Every component in this turnkey is made for precision, throughput, and repeatable results. Also included is our Pro Series Corrosion Resistant Two Stage Vacuum Pump giving you extreme power and depth with a long lifespan, the Bullseye Precision Vacuum Gauge from Digivac which is the most rugged and dependable vacuum gauge on the market, and a BVV 19L Heated Circulator for maximum condensation of vapors. You will also receive a Dewar Style Glass Cold Trap to keep all volatiles and solvents out of your vacuum system. This Turnkey Setup gives you everything needed to perform distillation at the highest level. The Premium Turnkey Kit Includes: 5L Neocision Kit with P5 Distillation Head KF-25 x 1/4" Barb Adapter Dewar Style Glass Cold Trap Bullseye Precision Vacuum Gauge BVV 19L MX Heated Circulator Pro Series 21.2CFM Corrosion Resistant Two Stage Vacuum Pump Distillation Quick Start Guide This guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs, Before beginning distillation, ensure the following steps have been taken: Vacuum Pump is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed. All glass components are in good working order and ready to be assembled A winterization and degassing procedure has been done to prepare oil for distillation Once all three of these steps have been completed, you are ready to begin distilling. Begin by placing stir bar in boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer. Assemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware Attach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation. Connect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system. Connect receiving cow to cold trap. Connect cold trap to manifold. Connect vacuum gauge to manifold. At this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process. Turn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability. Start stir slower and increase speed with temperature. Once you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C. You will see your first fraction somewhere between 180C and 190C or slightly before. This is the “heads” fraction. You will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to “self-clean” the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your “main body” fraction. You will see temps between 190-220C during this fraction. Continue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed. The final “tails” fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The “tails” fraction has an obvious color change and will be darker than the “main body” fraction. You will see temps between 200-250C during this fraction. As fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well. Once process is complete, stop heat, stop stir, and stop vacuum. Let atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation. ***Note: This entire setup will ship via motor freight.*** ***Note: All units are inspected for broken glass or parts before unit is shipped. If unit arrives damaged or glass is broken (this does not include minor imperfections or scuffs in glassware), Customer MUST contact BVV™ within 3 days of delivery to file a claim and receive a replacement part. If customer DOES NOT contact BVV™ within 3 days of delivery responsibility for replacement parts falls on the customer and they must pay for replacement pieces.*** ***Glassware Safety Disclaimer: BVV™ is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.***
$14,874.25 - $20,894.77
10L Neocision Dual Head Short Path Distillation Turnkey System
10L Neocision Dual Head Short Path Distillation Turnkey System This unit carries a 2 day lead time. The 10L Neocision Distillation Turnkey Setup features our Dual 10L P5 Distillation Heads and USA made glass. Every component in this turnkey is made for precision, throughput, and repeatable results. Also included is a KF-25 Vacuum Pump giving you extreme power and depth with a long lifespan, the Bullseye Precision Vacuum Gauge from Digivac which is the most rugged and dependable vacuum gauge on the market, and a BVV 19L Heated Circulator for maximum condensation of vapors. You will also receive a Dual Dewar Style Glass Cold Trap to keep all volatiles and solvents out of your vacuum system. This Turnkey Setup gives you everything needed to perform distillation at the highest level. The Premium Turnkey Kit Includes: 10L Neocision Kit with Dual P5 Distillation Heads KF-25 2 Meter Bellows Dual Dewar Style Glass Cold Trap Bullseye Precision Vacuum Gauge BVV 19L Heated Circulator Your Choice Of KF-25 Vacuum Pump Distillation Quick Start Guide This guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs, Before beginning distillation, ensure the following steps have been taken: Vacuum Pump is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed. All glass components are in good working order and ready to be assembled A winterization and degassing procedure has been done to prepare oil for distillation Once all three of these steps have been completed, you are ready to begin distilling. Begin by placing stir bar in boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer. Assemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware Attach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation. Connect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system. Connect receiving cow to cold trap. Connect cold trap to manifold. Connect vacuum gauge to manifold. At this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process. Turn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability. Start stir slower and increase speed with temperature. Once you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C. You will see your first fraction somewhere between 180C and 190C or slightly before. This is the “heads” fraction. You will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to “self-clean” the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your “main body” fraction. You will see temps between 190-220C during this fraction. Continue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed. The final “tails” fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The “tails” fraction has an obvious color change and will be darker than the “main body” fraction. You will see temps between 200-250C during this fraction. As fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well. Once process is complete, stop heat, stop stir, and stop vacuum. Let atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation. ***Note: This entire setup will ship via motor freight.*** ***Note: All units are inspected for broken glass or parts before unit is shipped. If unit arrives damaged or glass is broken (this does not include minor imperfections or scuffs in glassware), Customer MUST contact BVV™ within 3 days of delivery to file a claim and receive a replacement part. If customer DOES NOT contact BVV™ within 3 days of delivery responsibility for replacement parts falls on the customer and they must pay for replacement pieces.*** ***Glassware Safety Disclaimer: BVV™ is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.***
$18,769.88 - $25,144.56
10L Neocision Dual Head Short Path Distillation Kit
10L Neocision Dual Head Short Path Distillation Kit This unit carries a 2 day lead time. The 10L Neocision Distillation Turnkey Setup features our Dual 10L P5 Distillation Heads and USA made glass. Every component in this turnkey is made for precision, throughput, and repeatable results. Also included the Bullseye Precision Vacuum Gauge from Digivac which is the most rugged and dependable vacuum gauge on the market. You will also receive a Dual Dewar Style Glass Cold Trap to keep all volatiles and solvents out of your vacuum system. This Turnkey Setup gives you everything needed to perform distillation at the highest level. The 10L Neo Kit Includes: 10L Neocision Kit with Dual P5 Distillation Heads KF-25 90 Degree Long Manifold and Metering Valve Dual Dewar Style Glass Cold Trap Bullseye Precision Vacuum Gauge Distillation Quick Start Guide This guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs, Before beginning distillation, ensure the following steps have been taken: Vacuum Pump is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed. All glass components are in good working order and ready to be assembled A winterization and degassing procedure has been done to prepare oil for distillation Once all three of these steps have been completed, you are ready to begin distilling. Begin by placing stir bar in boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer. Assemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware Attach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation. Connect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system. Connect receiving cow to cold trap. Connect cold trap to manifold. Connect vacuum gauge to manifold. At this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process. Turn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability. Start stir slower and increase speed with temperature. Once you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C. You will see your first fraction somewhere between 180C and 190C or slightly before. This is the “heads” fraction. You will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to “self-clean” the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your “main body” fraction. You will see temps between 190-220C during this fraction. Continue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed. The final “tails” fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The “tails” fraction has an obvious color change and will be darker than the “main body” fraction. You will see temps between 200-250C during this fraction. As fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well. Once process is complete, stop heat, stop stir, and stop vacuum. Let atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation. ***Note: This entire setup will ship via motor freight.*** *Notice to Customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. BVV™ is not responsible for the failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail, which can cause bodily harm or damage to the surrounding area.
$13,032.67
10L Premium Short Path Distillation Turnkey System
10L Premium Short Path Distillation Turnkey System This unit carries a 2 day lead time. (Note: Stainless Steel Table NOT Included.) The 10L Premium Short Path Distillation Turnkey System features our USA made P10 Distillation Head. Every component in this turnkey is made for precision, throughput, and repeatable results. Also included the Kangaroo digital thermometer which is very rugged and reliable. You will also receive a Ribbed Dewar Style Glass Cold Trap to keep all volatiles and solvents out of your vacuum system. This Turnkey Setup gives you everything needed to perform distillation at the highest level. The 10L Neo Kit Includes: 10L Short Path Distillation Kit including glassware, labware, and P10 Distillation Head. 10L Digital Heating and Stirring Mantle. Polyscience 15 Liter Advanced Digital Heated Circulator BVV™ 21.2CFM Pro Series Corrosion Resistant Vacuum Pump Valved Vacuum Adapter. Ribbed Dewar Style Glass Cold Trap. Kangaroo Digital Thermometer. Distillation Quick Start Guide This guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs, Before beginning distillation, ensure the following steps have been taken: Vacuum Pump is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed. All glass components are in good working order and ready to be assembled A winterization and degassing procedure has been done to prepare oil for distillation The unit's max internal temperature cannot exceed 380C. The recommended max set temperature should not exceed 250C Once all three of these steps have been completed, you are ready to begin distilling. Begin by placing stir bar in boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer. Assemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware Attach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation. Connect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system. Connect receiving cow to cold trap. Connect cold trap to manifold. Connect vacuum gauge to manifold. At this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process. Turn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability. Start stir slower and increase speed with temperature. Once you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C. You will see your first fraction somewhere between 180C and 190C or slightly before. This is the “heads” fraction. You will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to “self-clean” the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your “main body” fraction. You will see temps between 190-220C during this fraction. Continue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed. The final “tails” fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The “tails” fraction has an obvious color change and will be darker than the “main body” fraction. You will see temps between 200-250C during this fraction. As fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well. Once process is complete, stop heat, stop stir, and stop vacuum. Let atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation. ***Note: This entire setup will ship via motor freight.*** ***Note: All units are inspected for broken glass or parts before unit is shipped. If unit arrives damaged or glass is broken (this does not include minor imperfections or scuffs in glassware), Customer MUST contact BVV™ within 3 days of delivery to file a claim and receive a replacement part. If customer DOES NOT contact BVV™ within 3 days of delivery responsibility for replacement parts falls on the customer and they must pay for replacement pieces.*** ***Glassware Safety Disclaimer: BVV™ is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.***
$16,290.84
10L Premium Short Path Distillation Kit with P10 Distillation Head
10L Short Path Distillation Kit with P10 Distillation Head This unit carries a 2 day lead time. (Note: Stainless Steel Table NOT Included.) The 10L Short Path Distillation Kit features our USA made P10 Distillation Head. Every component in this turnkey is made for precision, throughput, and repeatable results. Also included the Kangaroo digital thermometer which is very rugged and reliable. You will also receive a Ribbed Dewar Style Glass Cold Trap to keep all volatiles and solvents out of your vacuum system. This Kit gives you the basic necessities of a short path distillation system and allows you to add on a temperature control system and vacuum pump to fit your needs. The 10L Neo Kit Includes: 10L Short Path Distillation Kit including glassware, labware, and P10 Distillation Head. 10L Digital Heating and Stirring Mantle. Valved Vacuum Adapter. Ribbed Dewar Style Glass Cold Trap. Kangaroo Digital Thermometer. Distillation Quick Start Guide This guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs, Before beginning distillation, ensure the following steps have been taken: Vacuum Pump is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed. All glass components are in good working order and ready to be assembled A winterization and degassing procedure has been done to prepare oil for distillation The unit's max internal temperature cannot exceed 380C. The recommended max set temperature should not exceed 250C Once all three of these steps have been completed, you are ready to begin distilling. Begin by placing stir bar in boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer. Assemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware Attach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation. Connect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system. Connect receiving cow to cold trap. Connect cold trap to manifold. Connect vacuum gauge to manifold. At this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process. Turn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability. Start stir slower and increase speed with temperature. Once you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C. You will see your first fraction somewhere between 180C and 190C or slightly before. This is the “heads” fraction. You will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to “self-clean” the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your “main body” fraction. You will see temps between 190-220C during this fraction. Continue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed. The final “tails” fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The “tails” fraction has an obvious color change and will be darker than the “main body” fraction. You will see temps between 200-250C during this fraction. As fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well. Once process is complete, stop heat, stop stir, and stop vacuum. Let atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation. ***Note: This entire setup will ship via motor freight.*** *Notice to Customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. BVV™ is not responsible for the failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail, which can cause bodily harm or damage to the surrounding area.
$5,808.04
20L Neocision Dual Head Short Path Distillation Kit
20L Neocision Dual Head Short Path Distillation Kit This unit carries a 2 day lead time. (Note: This kit does NOT include the stainless steel table.) The 20L Neocision Distillation Kit Setup features our Dual P10V6 Distillation Heads and USA made glass. Every component in this distillation kit is made for precision, throughput, and repeatable results. You will also receive Dual Dewar Style Ribbed Glass Cold Traps to keep all volatiles and solvents out of your vacuum system. This kit gives you the essentials of a short path distillation system and allows you to add a pump and temperature control system of your choosing. The 20L Neo Kit Includes: 20L Neocision Kit with glassware, labware, and Dual P10V6 Distillation Heads. KF-25 Bellow Y Manifold Dual Ribbed Dewar Style Glass Cold Trap Non-Mercury Glass Thermometers 20L Digital Heating and Stirring Mantle Distillation Quick Start Guide This guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs, Before beginning distillation, ensure the following steps have been taken: Vacuum Pump is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed. All glass components are in good working order and ready to be assembled A winterization and degassing procedure has been done to prepare oil for distillation The unit's max internal temperature cannot exceed 380C. The recommended max set temperature should not exceed 250C Once all three of these steps have been completed, you are ready to begin distilling. Begin by placing stir bar in the boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer. Assemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware Attach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation. Connect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system. Connect receiving cow to cold trap. Connect cold trap to manifold. Connect vacuum gauge to manifold. At this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process. Turn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability. Start stir slower and increase speed with temperature. Once you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C. You will see your first fraction somewhere between 180C and 190C or slightly before. This is the “heads” fraction. You will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to “self-clean” the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your “main body” fraction. You will see temps between 190-220C during this fraction. Continue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed. The final “tails” fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The “tails” fraction has an obvious color change and will be darker than the “main body” fraction. You will see temps between 200-250C during this fraction. As fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well. Once process is complete, stop heat, stop stir, and stop vacuum. Let atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation. *Note: This entire setup will ship via motor freight.*** *Notice to Customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. BVV™ is not responsible for the failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail, which can cause bodily harm or damage to the surrounding area.
$9,632.85 - $9,916.16
20L Neocision Dual Short Path Distillation Turnkey System
20L Neocision Dual Short Path Distillation Turnkey System This unit carries a 2 day lead time. (Note: This kit does NOT include the stainless steel table.) The 20L Neocision Distillation Turnkey Setup features our Dual USA made P10V6 Distillation Heads. Every component in this distillation kit is made for precision, throughput, and repeatable results. You will also receive Dual Dewar Style Ribbed Glass Cold Traps to keep all volatiles and solvents out of your vacuum system. This Turnkey Setup gives you everything needed to perform distillation at the highest level. The 20L Neo Kit Includes: 20L Neocision Kit with glassware, labware, and Dual P10V6 Distillation Heads. BVV 15 Liter Advanced Digital Heated Circulator Choice of Vacuum Pump KF-25 Bellow Y Manifold Dual Ribbed Dewar Style Glass Cold Trap Non-Mercury Glass Thermometers 20L Digital Heating and Stirring Mantle Distillation Quick Start Guide This guide gives basic quick start instructions for distillation systems. It is intended to provide a starting point for learning the process. Parameters should be adjusted to suit specific needs, Before beginning distillation, ensure the following steps have been taken: Vacuum Pump is in good working order. Pump should be run against dry load to allow internals to warm up. Oil should be clear. Cloudy or dark oil should be changed. All glass components are in good working order and ready to be assembled A winterization and degassing procedure has been done to prepare oil for distillation The unit's max internal temperature cannot exceed 380C. The recommended max set temperature should not exceed 250C Once all three of these steps have been completed, you are ready to begin distilling. Begin by placing stir bar in the boiling flask and then load your material. This should be done using a funnel. A small amount of alcohol in the oil will give it a thinner consistency making it easier to transfer. Assemble all glassware and ensure each joint is properly greased. Do not use too much, as the vacuum pressure might pull some grease into the system. To ensure a full seal, spread grease in a circular motion by rotating glassware Attach circulator to condenser and set temperature to 50C. Allow circulator to reach temperature before beginning distillation. Connect vacuum pump to manifold. The manifold will allow you to isolate each individual component as well as let atmosphere into and out of the system. Connect receiving cow to cold trap. Connect cold trap to manifold. Connect vacuum gauge to manifold. At this point, ensure all connections are correct. Also ensure receiving cow is positioned to collect the first fraction in the far-left receiving flask. Circulator should be at its set temperature. Turn on vacuum pump to begin process. Turn on heat and set to 60C. Vacuum pump will begin to pull down and temperature will begin to rise. Watch the gauge to monitor vacuum pressure and stability. Start stir slower and increase speed with temperature. Once you are close to 60C, increase the temperature 20 degrees. Continue to raise the heat incrementally in 20-degree steps, increasing the set temperature as you near your set point. Increase temperatures incrementally until you reach 220C. You will see your first fraction somewhere between 180C and 190C or slightly before. This is the “heads” fraction. You will move to your second fraction when you see an increased reaction in the head, a slight color change toward golden, as well as a thickening of distillate. When this fraction hits, allow the distillate to “self-clean” the head for a minute or two then, rotate the cow to the middle receiving flask. Collect your “main body” fraction. You will see temps between 190-220C during this fraction. Continue to increase stirring speed as necessary. Reaction in the head may vary but it should never stop. As fluid level in the boiling flask decreases, increase stir speed. The final “tails” fraction is a mixture of the first and second fractions and should be saved for re-distillation later. Ideally, you want to turn the cow to the final flask before the tails fraction hits. The “tails” fraction has an obvious color change and will be darker than the “main body” fraction. You will see temps between 200-250C during this fraction. As fluid level in the boiling flask decreases even more, set stirring RPM higher (1000+ RPM). You may need to compensate with a bit more heat to finish of the final fraction as well. Once process is complete, stop heat, stop stir, and stop vacuum. Let atmosphere into the system. Be sure to properly store your distillate as exposure to air and light can cause oxidation. ***Note: This entire setup will ship via motor freight.*** *Notice to Customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. BVV™ is not responsible for the failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail, which can cause bodily harm or damage to the surrounding area.
$18,415.73 - $24,082.11
4" Wiped Film Evaporator (WFE) Distillation Turn Key System - USA MADE
4" BVV Wiped Film Evaporator This system has a 1-2 week lead time. The BVV™ 4" Wiped Film Evaporator (WFE) is a full turnkey distillation kit that will will allow anyone to run a molecular distillation. With the magnetically driven wiper and high vacuum seals this system is able to achieve vacuum levels below 10 mtorr. The system has multiple temperature control apparatuses that allow the user to dial in specific settings that works best for their application. The maximum operating temperature of the outer jacket is 200°C with the standard circulators shown below. The maximum feed rate is up to 7LPH. On average, you can expect to flow 500-1000ml per hour. All heated circulators can be tailored to your specific needs, just ask our team of experienced account representatives! The temperature controlled circulators will need thermal fluid that corresponds with the temperatures needed. Click here to browse fluids. *Heating and Chilling Fluids are not included* Duratherm S - 7 Gallons - Bottom heater (wiper body) Therminol XP Heat Transfer Fluid - 5 Gallons - Top and middle heater *Propylene Glycol - 5 Gallons - Fluid for the diffusion pump option chiller. Ethanol 99% or Isopropyl 99% - 2 Gallons - Cold Trap / Cold Finger. For a full list of ancillary equipment included in the kits please see the table below: KIT Part of System Component Electrical Requirements (V / Ph / A) WFE04-TK-01 Standard Model Wiper Assembly BVV™ Stirring motor 120V / 1Φ Vacuum System BVV™ Pro Series 35.3CFM Rotary Vane Vacuum Pump* DigiVac Bullseye Precision Vacuum Gauge 220V / 3Φ AA Batteries (4x) Temperature Controlled Circulators Polyscience 7L Polyscience 15L (2x) 120V / 1Φ / 10A 220V / 1Φ / 10A Injection Beaker and Wrench 7LPH Peristaltic Heated Hose 120V / 1Φ 120V / 1Φ WFE04-TK-02 Upgraded Vacuum System Upgraded Cold Trap Wiper Assembly BVV™ Stirring motor 120V / 1Φ Vacuum System BVV™ Pro Series 35.3CFM Rotary Vane Vacuum Pump* Summit Research Diffusion Pump (SR-DP04A)** DigiVac Bullseye Precision Vacuum Gauge 220V / 3Φ 180/264V / 1Φ / 10.5A AA Batteries (4x) Temperature Controlled Circulators Polyscience 7L Polyscience 15L (2x) 120V / 1Φ / 10A 220V / 1Φ / 10A Injection Beaker and Wrench 7LPH Peristaltic Heated Hose 120V / 1Φ 120V / 1Φ Cold Trap Polyscience IP100 120V / 1Φ / 11.5A WFE04-TK-03 Upgraded Vacuum System Upgraded Cold Trap Outlet Pumps Wiper Assembly BVV™ Stirring motor 120V / 1Φ Vacuum System BVV™ Pro Series 35.3CFM Rotary Vane Vacuum Pump* Summit Research Diffusion Pump (SR-DP04A)** DigiVac Bullseye Precision Vacuum Gauge 220V / 3Φ 180/264V / 1Φ / 10.5A AA Batteries (4x) Temperature Controlled Circulators Polyscience 7L Polyscience 15L (2x) 120V / 1Φ / 10A 220V / 1Φ / 10A Injection Beaker and Wrench 7LPH Peristaltic Heated Hose 120V / 1Φ 120V / 1Φ Cold Trap Polyscience IP100 120V / 1Φ / 11.5A Outlet Pumps Beaker and Wrench Gear Pump (2x) Beaker and Wrench Heat Pad PID Controller 120V / 1Φ 120V / 1Φ Notes: *The Rotary vane vacuum pump paired with this kit uses 3Φ power, a smaller single phase pump can be substituted if needed. Substitution will have an impact the performance versus the standard unit. **The Summit Research diffusion pump must be water cooled, if facility water cooling is not an option an additional chiller may be needed, a Polyscience 1HP Durachill is recommended. An air cooled diffusion pump can be provided as a substitute. Substitution will have an impact the performance versus the standard unit.
$63,746.77 - $107,661.21
Beaker & Wrench Turn-key System 6"
Beaker & Wrench Turn-key System Please Note: Lead time 0-4 weeks Get greater consistency, purity, and confidence in every Flower oil distillation when you use our system to monitor and optimize flow rate, temperature, pressure, and wiper speed (RPM) in real time. Fully continuous flow leaves behind less advanced methods with a dependable output of 3-5 liters per hour; maximizing efficiency and minimizing complications. Be assured of the quality of your system. Each system is 6 inch and constructed with fully compliant USA NRTL-certified components, including a display unit and two sensors to track the contents of both streams of fluid as it continuously travels through the glassware. Your system arrives ready to use immediately with all components primed for use. Just roll it off the lift gate and let it get to work. Meet demand and feel confident in the quality of your output with this turn-key system. 6” Stainless Steel Wiped-Film Evaporator Delivers greater consistency, purity, and confidence in every Flower oil distillation. Continuous flow leaves behind less advanced and efficient methods with a dependable input up to 7 liters per hour. Throughput capability Up to 7.0 L/hr Average 3.0-5.0 L/hr True Continuous Feed Peristaltic Inlet pump allows addition of oil while machine is still under vacuum Outlet pumps allow dispensing of products directly into vessel of choice Feed rates adjustable from 10mL to 10L/hr Jacketed body Thermal fluid circulating through jacketed body for consistent temperature Precise temperature control PID temperature controllers on body and all heated lines for creation of precise SOPs Expert On-Site Training and Installation Validation with YOUR oil on the day of install Consultation on how to generate the best SOP for your lab Sample SOP provided for internal use Potency up to 99.8% total Flower content Feed 20L stainless steel feed flask with vacuum inlet line Peristaltic dosing pump for precise, vacuum-held dosing Feed line to evaporator is jacketed and PID controlled Short-Path Evaporator Max evaporator temperature: 200 °C 316 Stainless Steel 316 Stainless Steel Internal condenser (cold finger) 6 rollers Easy to adjust drive system speed Distillate & Residue Discharge Pumps (2 pumps) Gear pump in PID controlled heated design (design temperature 100°C), digitally displayed pump speed. Calibration and secret menu options for optimal SOP development Check valves used as a pressure lock against the atmosphere Vacuum System 21 to 36 CFM Rotary Vane Vacuum pump equipped with vacuum pump oil Diffusion vacuum pump for achieving stable vacuum conditions at low pressures (oil included) Flanged cold trap & collection vessel for cold trap Heating & Cooling by Beaker & Wrench/ Polyscience 1 independent heating unit for the evaporator (oil circulator) 1 independent heating unit (silicone pad) for the residue & distillate line 1 independent heating unit for the feed tank (silicone pad) 1 independent cooling unit for the cold trap (immersion probe) 1 independent chilling unit for the internal condenser (water circulator) Rack/Frame Frame constructed of 80/20 aluminium extrusion and equipped with 4 wheels Power supply & power distribution system 1. Voltage: 120V or 220V Frequency: 60 Hz 3. Number of Phases: 1 (two hot wires) • Power distribution panel Control panel for pumps. Included spare parts. 1 set of rollers 1 set of static gaskets 1 set of shaft sealing for rotary transmission • 1 set of bearings for rotary transmission 1 set of O-rings Documentation Operating instructions Component Certifications See Below Heaters & Chillers CE/ISO9001 Vacuum Pumps Gear Pumps Wiper Drive Power Box Frequency Box Pressure Gauge
$262,070.06
Beaker & Wrench 40L Complete Dosing System
Beaker & Wrench 40L Complete Dosing System Please note: This Product has 1 week lead time For Wiped Film Evaporators The 40L Complete Dosing System by Beaker & Wrench® is a continuous feed system that connects to any Wiped Film Evaporator effortlessly. Optimize your time and end results by dialing into your feed system. The Feed Gear Pump by Beaker & Wrench® gives the operator control over flow rate and freedom to load material into the flask without breaking deep vacuum. Once attuned with the flow rate, calculations become less of a guessing game and more of a formula. Distill as slow or as fast as needed! The contents of this system include: Heated 40L feed flask Crude Cozy™ Digitally operated, heated Feed Gear Pump 4″ tri-clamp port on feed lid Inlet adapter (for your still) 6′ Heated Transfer Line (not pictured) Wattage: 90/ft, 120 Volts Maximum Temp: 150°C UL Listed 3 Channel PID Temperature Controller UL: E510826 How does it work?Crude is loaded into a heated feed flask, which then flows through the heated Gear Pump. The Gear Pump moves fluid through the gears while maintaining vacuum. Oil is then pulled towards the still body, ready for distillation! Cleaning:Every Operator has their own preference in how they clean their Wiped Film Evaporator. Ethanol, Isopropyl alcohol or vegetable oil are viable options when looking to clean your Wiped Film. Step-by-step instructions are included in the manual! Installation: Are you interested in having a Beaker & Wrench® technician install your Complete Dosing System? Click here for a quote! The advantage with having a technician perform installation is you can ask any and all questions necessary on how to process with your Wiped Film Evaporator! What is the warranty?1 year manufacturer’s warranty on parts for exchange. Customer has 5 days from day of delivery to inspect equipment for breakages or damage. ** Please indicate the inlet size of your still in the Notes section of your purchase. This will help us adapt to your set-up.
$17,707.44
Steam Distillation Kit
Steam Distillation Steam distillation is the separation of organic compounds at low temperatures by boiling water. It is widely used for essential oils and terpenes because it does not degrade the organic material as a traditional fractional distillation does. Alternatively, steam distillation can extract a diverse array of immiscible substances. You can use steam distillation for “steam stripping” in petroleum refineries and separate commercially important organic compounds, including fatty acids. Our system is composed of a 6-piece glass distillation set up paired with a separatory funnel. Simply fill the boiling flask with water and the material flask with your organic material, then use the heating mantle to boil the water and pass the steam through the material flask. There is a port above the material flask on the U-Tube to insert a thermometer to more closely monitor the process. The steam passing around the material will lower the boiling point on the surface of the plant material and cause the terpenes to boil off at low temperatures. After moving through the U-Tube the steam and terpenes will condense in the graham condenser and drain into the flask below. After filling the flask, simply swap it and drain the contents into the separatory funnel to remove all water. Steam Distillation is beneficial due to the lower boiling point being able to reduce the decomposition of temperature-sensitive compounds. Here’s a look at the key benefits of steam distillation. Key Benefits of Steam Distillation: Streamlined method produces organic solvent-free products Possesses large capacity for processing at the industrial scale Requires no subsequent separation steps Requires less fuel for the steam boiler for extraction of oils Due to its wide application and inexpensive equipment, steam distillation can be a cost-effective investment Kit Includes: 2L Analog Mantle 2L Boiling Flask 2L Material Flask U-Tube 24/40 Thermometer Adapter 24/40 Male Stopper Graham Condenser 500ml Flask 500ml Separatory Funnel BVV™ Lab Stand Three Finger Clamp Boss Head Please Note: for any replacement parts, please contact us. 2L Dual Neck Flask (SKU: STEAM-01-2000ml) 2L Material Flask (SKU: STEAM-02) U-Tube (SKU: STEAM-03) Graham Condenser (SKU: STEAM-04)
$701.21
Analog Heating and Stirring Mantle
Analog Heating and Stirring Mantle is used to heat up a glass round bottom flask and stir the contents inside. Heating and stirring functions are analog and sizes range from 500ml to 2000ml. (Mantle's are tested in house and may show slight discoloration on the heating surface.) Certifications: CE Approval Warranties: 500ml - 30 Day Limited Warranty 1000/2000ml - 90 Day Limited Warranty.
$191.24 - $247.90
2L Digital Heating and Stirring Mantle
2L Digital Heating and Stirring Mantle Digital Heating and Stirring Mantles give the operator the most precise temperatures and readouts during distillations. These mantles autotune to specific user input to provide consistent results. Each mantle is equipped with large digital display that will give you readouts for both set temperature, actual temperature, and stirring speed. Each mantle also comes with a vertical brace bar and boss head as well as a temperature probe which plugs directly into the mantle. For first time use, the mantle should have an initial burn out done. This will burn off any residual oils used in the production of the insulation rope. The unit's max internal temperature cannot exceed 380C. The recommended max set temperature should not exceed 250C Specifications: Capacity: 2L (2000mL) Power Supply: 110V 60Hz Adjustable Rotation Speed: 50-1800 RPM Motor Power: 40W, DC14-24V Heating Power 180-2200W Temperature Control Accuracy: +/- 1C Intelligent Temperature Control: Yes Temperature Range: RT+10-380C Insulation Material: Alkali-free Glass Fiber, temperature resistant up to 450C Shipping Dimensions: 20 x 14 x 13 in. Weight: 8 lbs
$814.54
5L Digital Heating and Stirring Mantle
5L Digital Heating and Stirring Mantle Digital Heating and Stirring Mantles give the operator the most precise temperatures and readouts during distillations. These mantles autotune to specific user input to provide consistent results. Each mantle is equipped with large digital display that will give you readouts for both set temperature, actual temperature, and stirring speed. Each mantle also comes with a vertical brace bar and boss head as well as a temperature probe which plugs directly into the mantle. For first time use, the mantle should have an initial burn out done. This will burn off any residual oils used in the production of the insulation rope. The unit's max internal temperature cannot exceed 380C. The recommended max set temperature should not exceed 250C Features: PID Temperature control Brushless magnetic magnetic stirrer motor Temperature protector Specifications: Capacity: 5L (5000mL) Power Supply: 110V 60Hz Adjustable Rotation Speed: 50-1800 RPM Motor Power: 40W, DC14-24V Heating Power 180-2200W Temperature Control Accuracy: +/- 1C Intelligent Temperature Control: Yes Temperature Range: RT+10-380C Insulation Material: Alkali-free Glass Fiber, temperature resistant up to 450C Shipping Dimensions: 20 x 15 x 14 in. Weight: 12 lbs
$1,133.28
10L Digital Heating and Stirring Mantle
10L Digital Heating and Stirring Mantle Digital Heating and Stirring Mantles give the operator the most precise temperatures and readouts during distillations. These mantles autotune to specific user input to provide consistent results. Each mantle is equipped with large digital display that will give you readouts for both set temperature, actual temperature, and stirring speed. Each mantle also comes with a vertical brace bar and boss head as well as a temperature probe which plugs directly into the mantle. For first time use, the mantle should have an initial burn out done. This will burn off any residual oils used in the production of the insulation rope. The unit's max internal temperature cannot exceed 380C. The recommended max set temperature should not exceed 250C Specifications Capacity: 10L (10000mL) Power Supply: 220V 60Hz Adjustable Rotation Speed: 50-1800 RPM Motor Power: 40W, DC14-24V Heating Power 180-2200W Temperature Control Accuracy: +/- 1C Intelligent Temperature Control: Yes Temperature Range: RT+10-380C Insulation Material: Alkali-free Glass Fiber, temperature resistant up to 450C Shipping Dimensions: 23 x 23 x 16 in. Weight: 20 lbs
$1,770.74
20L Digital Heating Mantle
20L DIGITAL HEATING AND STIRRING MANTLE Digital Heating and Stirring Mantles give the operator the most precise temperatures and readouts during distillations. These mantles autotune to specific user input to provide consistent results. Each mantle is equipped with large digital display that will give you readouts for both set temperature, actual temperature, and stirring speed. Each mantle also comes with a vertical brace bar and boss head as well as a temperature probe which plugs directly into the mantle. For first time use, the mantle should have an initial burn out done. This will burn off any residual oils used in the production of the insulation rope. The unit's max internal temperature cannot exceed 380C. The recommended max set temperature should not exceed 250C Specifications: Capacity: 20L (20000mL) Power Supply: 220V 60Hz Adjustable Rotation Speed: 50-1800 RPM Motor Power: 40W, DC14-24V Heating Power 180-2200W Temperature Control Accuracy: +/- 1C Intelligent Temperature Control: Yes Temperature Range: RT+10-380C Insulation Material: Alkali-free Glass Fiber, temperature resistant up to 450C Shipping Dimensions: 25 x 25 x 18 in. Weight: 35 lbs
$1,983.23
Glas-Col Stirmantle
Glas-Col Stirmantle Glas-Col offers two types of StirMantles: Electromagnetic (50 to 750 rpm) and Motor Driven (100 to 1850 rpm). The maximum rpms available for each type depends on the viscosity of the solution being heated. Electromagnetic StirMantles are typically used with aqueous solutions like water, while the Motor Driven units use a powerful magnet for higher viscous solution like oils. StirMantles withstands 400°C internal operating temperature. EMS series include the heating mantle, speed control and stir-bar. TEM series only includes the heating mantle and allows the customer in select different speed control options or combined speed/temperature packages like the 104A HS112. WARNING: chemical spillage, overheating, overloading, and general misuse will greatly reduce service life! Note: The temperature probe this mantle comes with can only be used with a thermowell. If you are using it with BVV™ glassware you will need to add SKU: TK1/4-12 or TK1/4-18 depending on what mantle size is selected.
$1,416.59 - $2,054.06
Glas-Col 2 L Stir Mantle
Glas-Col 2 L Stir Mantle Specifications Material aluminum housed Max temperature C 400 Height (in) 6 Outside Diameter (od)(in) 12 Capacity 2 L Volts 115 Watts 500 Includes: Separable 4-ft., 2-wire cord and locking connector.
$2,116.39
Glas-Col 12L Stir Mantle
Glas-Col 12L Stir Mantle Specifications Body Material Material Max temperature C 400 Height (in) 9 Outside Diameter (od)(in) 16.5 Capacity 12 L Volts 115 Watts 1 @ 1300 Includes: Separable 4-ft., 2-wire cord and locking connector.
$2,532.87
Glas-Col 22L Stir Mantle
Glas-Col 22L Stir Mantle Safely and accurately heat solutions used in various distillations in laboratory and scientific applications Apply heat directly and uniformly to containers, such as round bottom flasks More accurate than hot plates and safer than Bunsen burners Controllers can be purchased individually Accommodates 22L spherical flasks Specifications & Description Max Flask Size (mL) 22000 Min Stirrer Speed (rpm) 100 Max Stirrer Speed (rpm) 1850 Max temperature (° F) 752 Max temperature (° C) 400 Power (VAC) 115 Power (watts) 1540 Height (in) 14 Diameter (in) 6.875 Outside Diameter (OD) (in) 19 Description Stirring/Heating Mantle, 22L Spherical Flask; 115V
$2,691.53
Glas-Col Mantle and Controller
Glas-Col Mantle and Controller Specifications Material Aluminum Housed Max Temperature C 400 Height (in) 10 Outside Diameter (od)(in) 13.66 Capacity 22L Volts 115 Watts 2 @ 770 Includes: Separable 4-2ft., 2-wire cord and locking connector
$4,608.18
Glas-Col Vapor Monitor
Glas-Col Vapor Monitor motor vapor temperature or other processes audible alarm - high, low, t/c break digital display Specifications TC Type "J" MUST BE ORDERED SEPARATELY Range 0 - 999 C Dimensions 4" W x 4" D x 4" H Volts 120 Includes: 6' attached power cord and grid support bracket
$396.65
Glas-Col Thermocouple Type "J" Mini Plug
Glas-Col Thermocouple Type "J" Mini Plug D x L : 1/4" x 4" Lead Length: 72"
$99.16
Glas-Col K Type Thermocouple
Glas-Col K Type Thermocouple Glas-Col K Type thermocouple is used to measure temperatures from -50°C to 1000°C with a lead length of 72" and probe length of either 12" or 18".
$349.90
Fiberglass Insulation Rope 10 Feet
Fiberglass Insulation Rope 10 Feet ***Caution: Always use proper protection when working with fiberglass. Avoid skin and eye contact.*** Ten feet of white 1/2" fiberglass insulation rope. Used to wrap the upper half of boiling flasks. Specifications: Width: 1/2" Material: Fiberglass Maximum Temperature: 1000F Resistant to solvents, acids, and bleach Color: White Length: 10 ft. (20ft needed for 5L Flask.)
$39.66
5L Glas-Col Fabric Insulating Top
5L Glas-Col Fabric Insulating Top This mantle helps prevent vapor condensation in the upper half of a flask during distillation of high-boiling materials. The tops are designed for use with Series M, TM, or STM mantles. They protect the flask, the solutions, and the laboratory from drafts, which would disturb the reflux ration during fractionation, from flying glass of flask implosions in high vacuum distillations, from falling objects; and, from thermal strain between top and lower half of flask during high-temperature operations. With a glass-fabric construction and laced-side opening, the elliptical hole accommodates 1-, 2-, and 3-neck flasks.
$495.81
Glas-Col 12L Heating Insulation Top - 115V, 590W
Glas-Col 12L Heating Insulation Top - 115V, 590W Glas-Col invented the Electric Heating Mantle in 1939 and has continued to be the industry leader for Laboratory and Industrial heating ever since. Our products are known for exceptional performance, reliability and durability. Specifications Capacity 12 L Volts 115 Watts 590
$1,171.52
Glas-Col 50L Heating Insulation Top - 1000W, 115V
Glas-Col 50L Heating Insulation Top - 1000W, 115V Glas-Col invented the Electric Heating Mantle in 1939 and has continued to be the industry leader for Laboratory and Industrial heating ever since. Our products are known for exceptional performance, reliability and durability. Specifications Capacity 50 L Volts 115 Watts 1,000
$2,085.23
Arometrix Fraction Finder
Arometrix Fraction Finder Overview Description The FRACTION FINDER is Arometrix’s real-time molecular monitoring system for refinement processes, such as fractional distillation and isolation. This patented technology is essential for getting the highest-quality, most consistent oils possible. Forget the old ways of relying on experience, guesswork, and eyesight alone – now you can identify fractions in-line with this novel approach to real-time molecular tracking. DON’T JUST DO YOUR PROCESS. KNOW YOUR PROCESS. Features & Details Arometrix Sensor Uniquely built to attach directly to glassware in seconds Connects and transmits to the high-quality monitor Plug and play – instantaneously analyzes the mixture flowing through the processing machine Available in two sizes: size 29 (fits 28-30mm OD glass) and size 34 (fits 31-34mm OD glass) Available with ultra-sensitivity as an add-on (10X increase in sensitivity) Arometrix Monitor Collects and displays real-time molecular data in-line throughout the process High-quality, high-resolution touch screen Compatible with all Arometrix sensors Key Software Features Molecular Viewing – View up to 3 molecules simultaneously via two different graphing options Intensity Values – Observe numeric molecular intensity levels that correlate with potency Data Logging – Record run data for traceability in our data review app Software Updates – Upgrade to new software releases easily from the field Lack of objectivity during fractional distillation Botanical processors don’t know their product’s quality until after the process is over. This is because traditional molecular analyzers are hardware-hungry and can’t be utilized in-line, but rather, after the process for sample testing. During the process, processors are forced to rely on subjective techniques, such as eyesight, experience, and guesswork, and indirect techniques like temperature. This lack of analytical tools during the processing leads to human error and “bad” batches. Now, you can forget the old ways of manually ‘finding fractions’. The FRACTION FINDER product line will improve the quality, consistency, and value of processed botanicals. Make smarter decisions based on data Arometrix’s disruptive solution is the patented FRACTION FINDER. Processors refer to it while they are operating to view current process status and undertake corrective actions if needed. By using the Fraction Finder in tandem with existing laboratory and processing techniques, you’ll have a wealth of additional information on which to base decisions. For example, the data will tell you when to change your distillation collection flasks so that the different fractions are more optimally separated. The main fractions are “heads”, “bodies”, and “tails”. Knowing exactly when each fraction starts helps you to determine optimal flask transfers for precise and repeatable separation of fractions. Additionally, this technology is great for rapidly training novice technicians on the process, or standardizing distillations across a large facility. Applicable processes for this model includes small, benchtop, and industrial distillation process, including short path distillation, thin film distillation, and wiped film evaporation / distillation, and chromatography / isolation. Powered by fluorescence spectroscopy The AROMETRIX technology utilizes a principle known as fluorescence spectroscopy, a branch of science concerned with measuring molecules based on how they interact with light. The technology uses a spectrum of wavelengths over time to determine the relative purity of oils flowing through a glass condenser or sight glass. This technique paves the way for precision and repeatability, which will yield a more consistent product over time. Product Details Included in this package: Arometrix Monitor Arometrix Fraction Finder Sensor Light-Blocking Tape Power Supply 3″ Sensor Cable Pole-Mounting Clamp User Manual Quick Start Guide 1-Year Warranty Compliance: ROHS CE
$7,366.29 - $8,734.72
Bullseye Precision Gauge | Portable Vacuum Gauge | .001 to 2 Torr Accuracy
Bullseye Precision Gauge | Portable Vacuum Gauge | .001 to 2 Torr Accuracy The Bullseye Precision Gauge is the ideal portable vacuum gauge to serve many applications. This patented vacuum gauge offers Graphical Displays and graphics supporting real-time analytics (Leak, Pump, Outgas, Stable) Visual graphing feature right on the display Display pinpoints the root of the problem so you get it right the first time Put it anywhere with its magnet and kickstand Options: Rugged carrying case designed for instrument, back-up sensor and these adapters that can change the NPT to a KF25 or KF16 vacuum interface adapters Sensor (Probe) Replacements: This gauge is paired with the Thermocouple Plus/531 Equivalent Sensor, but works with Agilent 531 or 536 sensors as well if you are looking for a more robust sensor option Numeric & Graphical Displays See vacuum readings in either numbers or easy-to-read graphs Calibrated & Precise Delivered pretested and calibrated with thermocouple sensor under actual vacuum against a NIST standard. Extended Battery Lifespan Solid state electronics are built into the Bullseye Precision Gauge. The portable vacuum gauge operates using AA batteries and lasts 70 hours. Applications Vacuum pump monitoring, vacuum pump testing, baseline vacuum pump performance, & transformer dry-out, distillation monitoring Bullseye Precision Gauge Accuracy Remember to choose your vacuum gauge that gives you the accuracy you need for your application. This Bullseye comes with a thermocouple sensor, which has better accuracy in the millitorr up to 6 Torr. If you need your Bullseye Gauge to have CE rating then choose either the Bullseye with 531 or Bullseye with 536 KF25 1 to 99 millitorr +/- 2 millitorr or 20% 100 to 2000 millitorr +/- 10% 2 to 6 Torr +/- 25% Above 6 Torr Continuous and monotonic (increasing reading indicates increasing pressure) Units Torr, mbar, bar, kPa, inHg, mm Hg, millitorr, microns, inches of water, PSI, Pa Control Range 1E-4 – 1000 Torr Range with Accuracy .001 – 5 Torr Sensor Type SEN-VGT500, Thermocouple Plus Dimensions 6.2”H x 3.7”W x 1.3”D Certifications ROHS and CE
$750.80
KF-25 x KF-25 x 1/8" FNPT Adapter
KF-25 x KF-25 x 1/8" FNPT Adapter This 304 stainless steel KF-25 adapter is specifically designed for adapting Digivac Bullseye Precision Vacuum Gauges to systems with reducing and minimizing connect / leak points on the system.
$38.25
Wireless Digital Vacuum Gauge 1~19,000 Microns
VGW-mini Wireless micron vacuum gauge measures vacuum via just one service port and with no loss of refrigerant. Its compact, robust and smart design support HVAC technicians with numerous intelligent features like the graphic display of measurement data in the Elitech Tools App. Its smart Bluetooth integration allows for data to be stored and evaluated reliably and efficiently, thus saving precious time and resources. Product Features High Accuracy The digital vacuum gauge achieves precise deep vacuum measurements down to single digit resolutions and provides notifications when the evacuation target is met. Smart APP Control Control your micron tester remotely and navigate through all measurement data via Smartphone or Tablet. Quickly and conveniently document your job, finalize your report and export - directly from the job site. Intelligent Judgement of H2O Status The vacuum meter automatically judges physical state of H2O by comparing ambient temperature and water saturation temperature corresponding to the vacuum in the system. Large, Easy-to-Read Display Continual digital readout of evacuation process can be viewed easily on the large, full-view LCD screen. Rechargeable Lithium Battery Built-in rechargeable lithium battery can work up to 20 hours per single full charge, saving troubles of frequent battery change. Product Specifications Measuring Range: 0-19000 micron Operating Temperature: -4℉~140℉ (-20°C~60°C) Interface: 1/4 SAE Accuracy: 1~10,000 microns: ±10% of readings ±10 microns10,000~19,000 microns: ±20% of readings Resolution: 0-400 1 Micron400-3000 10 Micron3000-10000 100 Micron10000-19000 250 Micron Vacuum Units microns, mTorr, in/hg, Pa, Torr, KPa, mbar and psia Battery rechargeable lithium battery (1,000mAh) Overload 27.5 bar Certification CE
$240.82
J-KEM Digital Temperature Monitor
J-KEM Digital Temperature Monitor Monitors and displays the temperature of an attached piece of equipment on a bright LED display. Built-in USB and free KEM-Net software provide remote temperature monitoring and data logging to a GLP/GMP compliant file. Audible alarm. Specifications: 120 or 230Vac, 50 watts.Warranty: 2 Years The temperature range desired determines the probe/thermocouple type: J [black] (0 – 800° C) K [yellow] (-50 – 1200° C) T [blue] (-200 – 250° C)
$815.96
J-KEM DVR-200-EV Digital Vacuum Regulator
J-KEM DVR-200-EV Digital Vacuum Regulator The DVR-200-EV has the same stainless steel pressure transducer inside, but the vacuum valve is outside of the controller. The value of this design is that the vacuum valve can be cleaned or replaced much easier than the valve in the classic DVR-200. Some applications, like distillations or stripping large volumes of solvent, can leave residues inside the valve which causes it to fail. Replacing the vacuum valve is the most frequent repair that J-KEM performs on the DVR-200. Replacing the valve in the classic DVR-200 is difficult and must be returned to J-KEM for repair. With the EV version, the user can disassembled the valve and wash it out, or even replace it in under 5 minutes. For large distillations or botanical applications, J-KEM recommends the DVR-200-EV. No Mercury 100% digital pressure entry and control Wetted parts are 100% stainless steel and Teflon Vacuum ramping feature eliminates bumping Resists: All organic solvents Acids Bases Water Specifications: 100 watts. Vacuum fittings: 1/8″ NPTM. Warranty: Electronics 2 Years, Vacuum Valve 6 months (void if damaged by chemical buildup)
$2,320.38
Traceable Kangaroo Thermometer - Digital
Digital Thermometer Traceable Kangaroo™ Thermometer comes equipped with the 42-inch probe cable in a reel-compartment pouch in the back of the unit. As a perfect “carry-around” unit, this thermometer can fit easily in any pocket, or you can use the convenient flip-open stand to place upright. The dual-range digital thermometer measures temperature in test tubes, beakers, and other scientific laboratory equipment and is especially effective for rugged applications with high-impact ABS cases. Additionally, digital thermometers can measure the temperature of many substances from air to liquids to surfaces—all electronically. The best thing about this thermometer? It’s easy to use! Any user can record identical results with this intuitive unit. The range is –58.0 to 572°F and –50.0 to 300°C with a resolution of 0.1° (between –19.9 to 199.9°) otherwise 1° and an accuracy of ±1°C (between –30 and 250°C) otherwise ±2°C. This unit automatically captures and recalls minimum and maximum temperature readings over any time period. Its high and low alarm may be programmed in 1° increments. The alarm sounds every minute until temperature returns to non-alarm condition. Pressing the HOLD key freezes the display to record a current reading. To assure accuracy, an individually serial-numbered Traceable® Certificate is provided from its ISO 17025 calibration laboratory accredited by A2LA. It indicates traceability to standards provided by NIST (National Institute of Standards and Technology). The stainless-steel probe has a diameter of 0.14 inches x 7-1/2 inch length and is resistant to most chemicals. The supplied silver-oxide battery runs continuously for one year. Large 3/4-inch digits are readable from 20 feet. Compact size is 2-1/2 x 4-3/4 x 1/2 inches, and weight is 2-3/4 ounces. Each product goes through an intense vetting process before carrying the Traceable name, which means you’ll save both time and money by not having to calibrate separately. The Traceable Kangaroo Thermometer applies to various unique applications such as the storage, laboratory, and medical industries. Specifications: Temperature Range F: -58 - 572F Temperature Range C: -50 - 300C Temperature Resolution: 0.1C Temperature Accuracy: +/-1C Programmable High and Low Alarm ISO 17025 Calibration Stainless Steel Probe Diameter of Probe: 0.14 in Length of Probe: 7.5 in Size: 2.5x4.75x.5 in Weight: 2.75 ounces
$92.08
Flat Bottom Flask
Flat Bottom Flask Flat Bottom Flasks are used to capture and store material when used with a glass funnel. These flasks are flat bottomed and come with a non-jointed opening. Sizes Available: 500ml 1000ml *Notice to customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. **Glassware Safety Disclaimer: BVV™ is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.**
$21.25 - $24.08
Single Neck Round Bottom Flask
Single Neck Round Bottom Flask Single neck round bottom flasks can be used for a variety of applications such as capturing and collecting material and also used for boiling off material through distillation. These flasks are single neck with a ground 24/40 joint and require the application of vacuum grease to the ground surface when using the flasks in a vacuum application. When laying these flasks down it is always recommended to use a cork stand for the flask to prevent breakage and keep the flask upright. Sizes Available: 50ml - 24/40 Ground Joint 100ml - 24/40 Ground Joint 125ml - 24/40 Ground Joint 250ml - 24/40 Ground Joint 500ml - 24/40 Ground Joint 1000ml - 24/40 Ground Joint 2000ml - 24/40 Ground Joint *Notice to customers: All units are inspected for broken glassware or parts before leaving BVV™. If the unit arrives damaged (this does not include minor imperfections or scuffs in glassware), the customer MUST contact BVV™ within 72 hours from carrier delivery to file a claim. If the customer DOES NOT contact BVV™ within 72 hours from carrier delivery, then BVV™ cannot issue any replacement(s) or compensation for the item; a new purchase will need to be made for a replacement. **Glassware Safety Disclaimer: BVV™ is not responsible for failure of glassware which must be inspected before and after every use because it may eventually develop imperfections or damage through normal usage, mishandling, and stress caused by temperature variations. If an imperfection or damage is noted while inspecting the glassware DO NOT use the glassware because it can fail causing bodily harm or damage to the surrounding area.**
$7.08 - $53.83
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