Manufacturer: Cascade Sciences
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KIT A: Integrated Mechanically Refrigerated Cold Traps:
There are a number of different distillation systems on the market. Cascade’s PUREPATH 100 + KIT A has a few marked differences.
1) Temperature Delta Of Asahi Glass Helps Minimize Breakage
The truth is – glass breaks and the distillation glassware is expensive to replace. The Asahi glass on the PUREPATH has an industry leading 110°C temperature delta. This means the Asahi glass on the PUREPATH can withstand the temperature shocks associated with rapid, hot to cold temperature changes that could occur with extreme temperature ranges – or when cold ethanol is introduced into the system to clean.
2) Keep It Clean! The Vacuum Integrity Of The Asahi Glass Is Exceptional – Seals And Joints Do Not Require Grease
Many products manufactured in a distillation system are destined for human consumption. The PUREPATH seals and joints are super smooth, which not only means exceptional vacuum integrity, but that you won’t have to introduce grease into the system in order to maintain vacuum. Lesser quality glass will often slightly leak – reducing performance/output and increase labor efforts chasing down small vacuum leaks.
3) The Vacuum Pumping System – Deep, Protected From Contamination & Real Time Graphical Data
The vacuum system features a UL Listed Agilent DS302 Rotary Vane Pump Since the vacuum integrity of the AGI Glass is so strong, it clears the way for the vacuum pump to get deeper to its ultimate pressure of 2×10-3 mbar. We protect and keep processing clean with a foreline trap on the inlet and an oil mist return.
4) Rodaviss® Couplings For Easy, Safe Disconnect Of Receiving Flasks
Cascade’s PUREPATH minimizes another potential glass break point by utilizing Rodaviss couplings.
5) Professional on-site installation and training. Our installation and training crew is a team of technicians from Cascade Sciences, Asahi Glass and seasoned industry veterans.
There are many variables that dictate thru put of any wiped film system. Crude oil will run through at different rates. Depending on initial potency test numbers, expect 2-3 Liters per hour.
To produce quality distillate, crude oil typically must run through the system twice.
• 1st Run strips terpenes and volatiles (Heads)
• 2nd Run distills heavy flower (Body)
• High Evaporation Efficiency
• Minimum Thermal Decomposition
• Gas and Vacuum Tight
• Uniform Thin Film
• Jacketed Evaporator for Easy Viewing
• Uniform Rotating Wiper System (Up to 300°C Option)
• Grease-less Magnetic Sealed Bearing, Valve and Joints
• Perfect for Heat Sensitive Materials
• Short Residence Time
| Precision Glass by Asahi | |
|---|---|
| Jacketed Evaporator ID 100mm with evaporation surface area of 0.1m2 | |
| Receiver 2000ml, Borosilicate Glass 3.3 | |
| Temperature range of glass –90°C to +230°C | |
| Delta of Glass 110°C (the temperature change the glass can withstand without breaking) | |
| External Condenser: Thermal transfer area 0.2m2 with 2 water connectors | |
| Magnetic Seal with Cover –torque 1.1Nm / Cover SS316 | |
| Wiper PTFE Wiper +200°C | |
| Overall Design Operating Pressure 0.1 mbar | |
| Cold Finger: Dry Ice capacity of up to 475ml | |
| Temperature Control by Huber | |
| Huber 202 Heating Feed Vessel with Temperature Probe | |
| General information & temperature controller | |
| Temperature range | 45°C to 200 °C |
| Temperature stability | ±0.02 °C |
| Temperature control | TAC, self-optimizing (True Adaptive Control) |
| Controller | Pilot ONE (E-grade “Basic”) |
| Safety class | III / FL |
| Protection class | IP20 |
| Dimensions: | (W x D x H) 178 x 260 x 355 mm |
| Weight | 8 kg |
| Heating / cooling capacity | |
| Heating capacity | 2 kW |
| Circulation pump | |
| Pressure pump max. | 27 l/min ; 0,7 bar |
| Suction pump max. | 22 l/min ; 0,4 bar |
| Pump connection | M16x1 AG male |
| Connections | |
| Pt100 connection | Pt100 |
| Digital interface | RS232, Ethernet, USB Device, USB Host |
| Operating data | |
| Permissible ambient temp. | 5°C to 40°C |
| Bath opening WxD/BD | Ø = 25 / 150 mm |
| Bath volume | 2L |
| Power supply | 230V 1~ 50/60Hz |
| Current max. | 10A |
| Huber 125 Ministat Cooling Main Body Condenser General information & temperature controller |
|
| Temperature range | -25°C to 150°C |
| Temperature stability | ±0.02°C |
| Temperature control | TAC, self-optimizing (True Adaptive Control) |
| Controller | Pilot ONE (E-grade “Basic”) |
| Safety class | III / FL |
| Protection class | IP20 |
| Dimensions (W x D x H) | 225 x 370 x 429 mm |
| Weight | 25kg |
| Heating / cooling capacity | |
| • Heating capacity | 1.5 kW |
| • Cooling capacity | 100 20 0 -10 -20 °C 0.3 0.3 0.21 0.15 0.05 kW |
| • Cooling machine | air-cooled |
| • Refrigerant | R290 (0.1 kg) |
| Circulation pump | |
| • Pressure pump max. | 22 lpm ; 0.7 bar | 5.81 gpm ; 10.15 psi |
| Suction pump max. | 16 lpm ; 0.4 bar | 4.23 gpm ; 5.8 psi |
| Pump connection | M16x1 AG male |
| Permissible viscosity | 50 mm²/s |
| Connections | |
| Pt100 connection | Pt100 |
| Digital interface | RS232, Ethernet, USB Device, USB Host |
| Operating data | |
| Permissible ambient temp. | 5°C to 35°C |
| Noise Level | 47dB(A) |
| Bath opening W x D / BD | 178 x 80 / 120 mm |
| Bath volume | 2.75 Liters |
| Filling volume min. | 2 Liters |
| Power supply | 115V 1~ 50/60Hz |
| Current max. | 11.5 A |
| Huber 304 Heating Main Body Jacket | |
| General information & temperature controller | |
| Temperature range | 28°C to 300 °C |
| Temperature stability | ±0.02 °C |
| Temperature control | TAC, self-optimizing (True Adaptive Control) |
| Controller | Pilot ONE (E-grade “Basic”) |
| Safety class | III / FL |
| Protection class | IP20 |
| Dimensions | (W x D x H) 210 x 335 x 392 mm |
| Weight | 14kg |
| Heating / cooling capacity | |
| Heating capacity | 3kW |
| Circulation pump | |
| Pressure pump max. | 25 l/min ; 0,7 bar |
| Suction pump max. | 18.5 l/min ; 0,4 bar |
| Pump connection | M16x1 AG male |
| Permissible viscosity | 50 mm²/s |
| Connections | |
| Pt100 connection | Pt100 |
| Digital interface | RS232, Ethernet, USB Device, USB Host |
| Operating data | |
| Permissible ambient temp. | 5°C to 40 °C |
| Bath opening WxD/BD | 130 x 100 / 155mm |
| Bath volume | 5 Liters |
| Filling volume minimum | 3.2 litres |
| Power supply | 230V 1~ 50/60Hz |
| Current max. | 14A |
| Fusing | 16A |
| Vacuum Power by Agilent | |
| Agilent DS302 8.2 CFM | |
| Pump Type | Oil, Rotary Vane |
| Pumping Speed | 8.2 CFM |
| Ultimate Pressure | 2 × 10-3 mbar |
| Power | 120V / 1ph (220V available) |
| Intake Connection | KF-25 |
| Dimensions | (L x W x H) 19.33” x 5.27” x 8.34” |
| Weight | 53 lbs |
| Vacuum Gauges, Connection Hardware included | |
| KIRK-1 FEATURES | |
| ● Auto Off | |
| ● On/Off soft switch | |
| ● Battery level indication | |
| ● Good/Bad sensor (tube) indication | |
| ● Self test mode | |
| ● Field replaceable sensor | |
| ● 3 different graphical displays of vacuum pressure (pump-down, line, or bar graph) | |
| ● Vacuum analytics for leak, outgassing and pump-down | |
| Unit Size | |
| • Length | 28″ |
| • Width | 83″ |
| • Height | 83″ |
| KIT A Equipment | |
| Huber Minichiller 600 OLÉ General Information & Temperature Controller |
|
| Temperature Range | -20°C to 40°C |
| Temperature Stability | ±0,5°C |
| Temperature Display | OLED Display |
| Display Resolution | 0.1°C |
| Alarm Message | optical, acoustical |
| Controller | OLÉ |
| Safety Class | I / NFL |
| Protection Class | IP20 |
| Dimensions | (W x D x H) 280 x 490 x 424 mm |
| Weight | 35 kg |
| Heating / Cooling Capacity | |
| Cooling Capacity | 15 0 -10 -20 °C 0.6 0.5 0.35 0.15 kW |
| Cooling | machine air-cooled |
| Refrigerant | R290 (0,085 kg) |
| Circulation Pump | |
| Pressure Pump Max. | 24 l/min ; 0,7 bar |
| Suction Pump Max. | 18 l/min ; 0,4 bar |
| Pump Connection | M16x1 AG male |
| Connections | |
| Digital Interface | USB, RS232 |
| Operating Data | |
| Permissible Ambient Temp. | 5°C to 40°C |
| Noise Level | 63 dB(A) |
| Filling Volume Min. | 2.8 Liters |
| Volume of Expansion | 2.2 Liters |
| Power Supply | 230V 1~ 50/60Hz |
| Current max. | 4 A |
| Huber TC100 | |
| Temperature Range | -100°C to 40°C |
| Controller | ON-OFF-Regler |
| Safety Class | I / NFL |
| Dimensions | (W x D x H) 295 x 500 x 570 mm |
| Weight | 61 kg |
| Heating / Cooling Capacity | |
| Cooling Capacity | 0 -20 -50 -60 -80 -90 -100 °C 0.16 0.15 0.13 0.12 0.12 0.07 0.01 kW |
| Cooling | machine air-cooled |
| Refrigerant 1. Stage | R1270 (0,114 kg) |
| Refrigerant 2. Stage | R1150 |
| Operating Data | |
| Permissible Ambient Temp. | 5°C to 40°C |
| Power Supply | 230V 1~ 50/60Hz |
| Current Max. | 6.5 A |
Download PUREPATH Power Requirements
Magnetic Stir Bearing Maintenance
